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丙酮

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As an important organic intermediate, methylglyoxal is widely used in producing imidazole and furanone, and also has important applications in medicine, agricultural pesticide, textile and so on.

丙酮醛是一种重要的有机合成中间体,被广泛应用于生产药物中间体4-甲基咪唑和食品增香剂呋喃酮,并在医药、农药、纺织等领域也有很重要的应用。

It was detected by DSC that the temperature of imide and crosslinking reaction are differentiated by the catalysis of acetyl acetone copper and rare earth.

DSC研究表明乙酰丙酮铜催化剂和稀土催化剂可以分开低聚物的亚胺化和交联反应温度。

The effects of different solvents on impregnation and properties of silica /phenolic composites were compared and studied,i.

对比研究乙醇、丙酮和四氢呋喃溶剂对RTM成型石英/酚醛复合材料溶液浸润过程和性能的影响。

Use indene respectively solution of 3 ketone acetone, indene solution of 3 ketone Freon, indene solution of aether of 3 ketone oil, solution of alkyl of 3 ketone age makes indene the experiment is compared.

分别采用茚三酮丙酮溶液,茚三酮氟利昂溶液,茚三酮石油醚溶液,茚三酮庚烷溶液作试验比较。

The Diels-Alder cycloadditions of [60] fullerene for preparation of optical limitingmaterials are discussed in chapter 3 and 6. Soluble cycloaddition derivatives of 〓aresynthesized by the reaction of 〓 with indene,1,1'-biindene andcyclopentadiene derivatives.〓Particular, the Diels-Alder cycloaddition of 〓 with1,1'-biindene under controlled conditions affords the stable monoadduct 〓〓of novel structure, which was confirmed by HPLC, FTIR, FD-MS,〓NMR,〓 NMR, HMQC and HMBC spectra, Its two bridgehead cage carbons resonate at70.91ppm, The 〓 NMR spectra showed 38 lines consistent with the 〓 symmetryassociated with [6,6] addition. The 〓 shows similar optical limitingproperties to that of 〓 in toluene for 8ns laser at wave length 532nm. Moreover, thehigh solubility of this adduct in polar solvents such as THF, acetone enables itsincorporation into sol-gel glass matrix. The thin films prepared via the sol-gel methodshow improved OL behaviour compared to those of 〓. The langmuir-Blodgett filmformation and uv-visible absorption of 〓 are also investigated. LBmonolayer of this compound is prepared on the air-water interface at 〓 mol/l. In chapter 4, three water-soluble derivatives of [60] fullerene: fullerol(1), theaddition product (2)of fullerol (1)with polyvinylpyrrolidone and fumaric acidderivative of 〓(3) are synthesized and characterized.

通过Diels-Alder环加成反应,用茚〓和1,1'-联茚〓及取代茂合成了一系列可溶性的〓环加成衍生物,发现可控制反应条件,使1,1'-联茚与〓反应,并高产率地得到具有新颖结构的单加成物,用HPLC、FTIR、FD-MS 及〓、HMQC、HMBC等多种波谱技术对其结构进行表征,测得它的两个〓杂化的桥头碳的化学位移为〓ppm,证明生成的衍生物为6∶6闭式环加成,〓NMR谱中共给出38个信号,表明〓联茚衍生物分子具有〓对称性;在波长532nm,脉冲宽度8ns的激光下,〓联茚衍生物的甲苯溶液的光限幅性能与〓的甲苯溶液相近,由于〓联茚单加成衍生物熱稳定性好,在四氢呋喃,丙酮等极性溶剂中溶解性好,能分别均匀地掺入溶胶-凝胶中,已发现它的溶胶(so1)光限幅性能优于纯〓的光限幅性能;使用Langmuir-Blodgett技术将〓联茚衍生物在空气和水的界面进行了LB单层膜和多层膜实验以及UV-Vis吸收谱研究,通过等温压缩曲线测试,证明浓度为〓〓时,〓联茚衍生物能够形成单层膜。

Properties White powder, inodorous, non-toxic, soluble in dilute alkali solution, carbon disulfide, benzene, acetone, dichloromethane and a little soluble in chloroform, insoluble in alcohol, carbon tetrachloride and ethyl acetate.

性质 白色粉末。无毒、无味。溶于稀碱、二硫化碳、苯、丙酮和二氯甲烷,微溶于氯仿,难溶于乙醇、四氯化碳、醋酸乙酯。

Methods: the model of acute eczema were induced by 5%DNCB. The model was then treated with Zihuang ointment by inunction for 4 weeks. Benyang oinmentand Gingeli were used in the control groups.

用5%的DNCB丙酮溶液诱发豚鼠急性湿疹模型,再用紫黄油膏外涂治疗4周,以苯氧膏及麻油外涂作为对照。

Microwave heating ; numerical methods ; empirical formula ; acetone iodation reaction

微波加热;数值模拟;经验公式;丙酮碘化反应

During the reaction, a by- product, shown as formula below, is formed at the same time as the pseudo-ionone, because of an impurity in the citral, thereby resulting in a mixture of pseudo- ionone and formula, referred to herein as a pseudo- ionone mixture or as crude pseudo-ionone.

假性紫罗兰酮的制备柠檬醛和丙酮的下列反应:这种反应通常是进行的温度面向对象之间的1000长在反应,1分产品,如公式所示以下,在形成同时,伪酮,因为有一个杂质在柠檬,从而在一个假性和公式混合物产生的,下称一假性混合物或原油伪紫罗兰。

Methods: According to the refe-rence of new traditional Chinese medicine study, maximal dosage of drug was given to rabbits to do the acute toxicological and irritative test on skin. The guinea pig was used to do the skin hypersensitive test with excipient as negative control and 1% 2,4-dinitrochlorobenzene as the positive control.

参照中药新药研究指导原则,采用最大给药剂量法对大白兔进行皮肤用药急性毒性和刺激性试验;以赋形剂为阴性对照,1%的2,4-二硝基氯苯丙酮溶液为阳性对照,对豚鼠进行皮肤过敏性试验。

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47:5 法老对约瑟说,你父亲和你弟兄们到你这里来了。

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