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丙酮

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The effects of different entrainers(methanol,acetone,ethyl acetate,petroleum ether and ethanol of different concentrations) on the diosgenin extraction rate were studied.

探讨了乙醇、甲醇、丙酮、乙酸乙酯、石油醚作为夹带剂以及在无夹带剂的条件下,对薯蓣皂素收率的影响。

Storage tanks developed by the introduction of new special plastic material, containing acetone, ethyl ether and other chloro-organic chemicals Fang operation, there are anti-corrosion and dissolution.

储水箱采用新研制的特种塑料材质,对含有丙酮、乙醚氯钫等有机化学物质的作业,有耐腐蚀而溶解作用。

It is easily soluble in water, acetone and alcohol, slightly soluble in ether, ethyl acetate, chloroform, and pyridine, unsoluble in benzene.

熔点151℃~154℃。易溶于水、丙酮与醇,微溶于醚、乙酸乙酯、氯仿和吡啶,不溶于苯。

The invention relates to synthesis of an organic matter, in particular to a method for preparing ethyl pyruvate.

本发明涉及有机物的合成,具体的说是一种制备丙酮酸乙酯的方法。

Objective To investigate the mutation characteristics in exon 7 of the PAH gene in phenylketonuria patients in Xinjiang.

目的研究分析新疆地区苯丙酮尿症患者中苯丙氨酸羟化酶基因外显子7的突变特征。

A full factorial experiment method and a second-order orthogonal design were used in the study.

研究内容主要包括: 1、以膏状大豆磷脂为原料,用丙酮为溶剂制备了粉状磷脂。

RESULTS: Image analysis of two-dimensional map revealed 72 differentially expressed proteins between MHCC97-H and MHCC97-L cells, and 9 protein peaks (including M2 pyruvate kinase,α-subunit of ATP synthase, heat shock protein 60, Toll-like receptor 9, flavoprotein oxygenase, pro-calreticulin, manganese superoxide dismutase, nm23-H1, and G-protein-coupled receptor kinase 5) were further identified by tryptic digestion, peptide mass fingerprinting and mass spectrometry.

结果: 2D图谱显示共有72个差异蛋白条带,共鉴定出了9个差异蛋白,分别为M2型丙酮酸激酶、ATP合成酶α亚单位、热休克蛋白60、Toll样受体9、含黄素单加氧酶、钙网硬蛋白前体、锰超氧化物岐化酶、nm23-H1、G-蛋白偶连受体激酶5;其中4个蛋白在高转移细胞株MHCC97-H中表达升高, 5个蛋白在低转移细胞株MHCC97-L表达升高。

They were named respectively as muramidase-released protein; succinate dehydrogenase/fumarate reductase flavoprotein subunit (SDHFp/FRDFP, extracellular); bacterial trigger factor; elongation factor G (EF-G, extracellular); PTS system sorbose subfamily I (PTS/MAN-ⅡAB, cytoplasmic); pyruvate kinase; phosphofructokinase, PK.

经MALDI-TOF-MS鉴定,这8个蛋白分别为溶菌酶释放蛋白、琥珀脱氢酶/延胡索酸还原酶黄素蛋白亚单位(SDHFp/FRDFp)、触发因子、延长因子G、细菌糖磷酸转移酶系统甘露糖特异ⅡAB亚单位、丙酮酸激酶、6-磷酸果糖激酶(6-PFK)、色氨酸-tRNA合成酶。

The factors included the type of extractant, the amount and the extraction times, the type of purified column, the type and dosage of eluviatant about the pre-treatment of the samples. The extraction was 3 minutes (13500rpm) of high speed homogenize extraction. 50mL acetonitrile as an extractant was acted on one time extraction. The florin silicon column was taken as the purified column. The extraction was eluted by 30ml 3:2 acetone - hexane and concentrated by nitrogen blowing under 50 °C water bath.The chromatographic separated conditions were studied applied the Agilent 6890 gas chromatographic apparatus and DB-17 capillary column(30m×0.25mm×0.25μm).

研究了提取剂种类、用量与提取次数,净化柱种类,淋洗剂种类与用量,提取方式与提取时间,柱温和柱流量等因素对油菜籽中有机磷农药残留提取、分离净化和色谱分离的影响,建立了采用高速匀浆提取方式提取3min13500rpm.min~(-1,以50mL乙腈为提取剂一次提取,以弗罗里硅柱为样品液净化柱,以30mL 3:2丙酮-正己烷为淋洗剂,在50℃水浴条件下用氮吹浓缩,气相色谱检测的油菜籽有机磷农药多种残留检测技术。

The effect of different second ligand on the flourescent properties of polymers were studied. Then AxByEu/HTTA/PMMA was prepared using the best second ligand HTTA.

考察了不同的第二配体(咔唑、二甲基-联吡啶、邻菲罗啉、噻吩甲酰三氟丙酮HTTA)对脂肪酸铕聚合物发光性能的影响,选择出合适的第二配体HTTA,进而合成了A3Eu/HTTA/PMMA聚合物。

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