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From FT-IR we think that the hydrogen bond between the polar oxygenous group on the thin film surface treated with plasma and acetone molecules would enlarge the distance between the carbon black particles, resulting in the addition of the electrical resistance, then the response behavior of the thin film to acetone was improved greatly.

我们通过FT-IR研究认为,等离子体处理后,薄膜表面引进的极性含氧基团与丙酮分子之间氢键的形成会增大炭黑粒子之间的距离,导致了薄膜电阻的极大增加,使薄膜对丙酮蒸气的响应得到很大改善。

4Production of chemical products from which narcotics are easily made ephedrine, 3, 4-idene dihydro phenyl-2-acctonc, phenylacetic acid, 1-phenyl-2-acetone, heliotropin, safrole, isosafrole, acetic oxide

易制毒化学品生产(麻黄素、3,4-亚基二氧苯基-2-丙酮、苯乙酸、1-苯基-2-丙酮、胡椒醛、黄樟脑、异黄樟脑、醋酸酐

Then with V∶V=11 9∶1 0,and by bubbling of air at 65-70 ℃ for 5-8 h,pyruvaldehyde was produced in 59 6% yield.

丙酮醛的总收率达 37 8%。n∶n∶n(1,2 丙二醇)=1 0∶4 0∶(1 5~ 2 5 ),以水为溶剂,在 6 0~ 70℃间歇通入氮气 1 5h ,边加原料边蒸馏,制得产率为5 0 %的丙酮醛。

The yield of pyruvaldehyde in glucose/glycine system (181□g/100ml)was3.6 folds that of galactose/glycine system (50□g/100ml)at 48 hr,We also founded that higher tmeperature promoted the change of pH, which in turn effect more significantly on Maillard reaction.

丙酮醛产量方面,45°C组葡萄系统在6084小时后才开始产生且量较少;而60°C组葡萄糖系统其产量於48小时达至最高(181□g/100ml),此时丙酮醛的产量为乳糖组(50□g/100ml )的3.6倍,之后有下降的趋势,其中浓度的效应较不明显。

Hydrothermal reactions makes water a Bronsted base-acid and act as an effective catalyst and the metal ions represent Lewis base character. The conversion process occurs in a very complex network of parallel, consecutive and equilibrium reactions, and the last step being the catalyzed Cannizzaro-type reaction of pyruvaldehyde to lactic acid.

nsted酸碱并具有一定的催化作用,金属离子在水热催化降解丙酮醛生成乳酸中表现出Lewis碱的特性,能与丙酮醛生成金属复合物,最终生成乳酸,此反应过程符合Cannizzaro反应特性。

Drying was done at ambient temperature and refluxed in acetone for hours to get rid of monomers. Finally, a vacuum oven was used to dry the product to a constant weight.

沉淀物经机械切碎后,在丙酮中浸泡24h,室温烘干再经丙酮回流数小时,除去单体,在25℃真空烘箱中烘干至恒重。

The result indicates that the best method for extracting β-carotene is to saponify the test specimen one hour with 4% NaOH methyl alcohol solution in 60-70'c and then to separate with 3:7 acetone-benzine component solvent as extraction solvent, MgO as the absorbent, the acetone-benzine as the eluent. Extracted solvent has been determined in the color dish condition (1cm) by ultraviolet spectrophotometer at 447 nm. The result shows that the β-carotene in carrotis 0.134 mgg^(-1), 0.0863mgg^(-1) in red pepper and 0.0426 mgg^(-1) in spinach.

结果表明,比较优先的β-胡萝卜素提取方法是:试样用4% NaOH甲醇溶液在60℃~70℃皂化1h,用3:7的丙酮-石油醚混合溶剂提取,以Mgo为吸附剂,丙酮-石油醚为洗脱剂分离,提取液用紫外分光光度计在波长447nm,1cm比色皿条件下测定,得出蔬菜中β-胡萝卜素含量:胡萝卜为0.134mgg^(-1),红椒为0.0863mgg^(-1),菠菜为0.426mgg^(-1)。

Alanine is formed by transamination when an amino group is donated by gutamine to pyruvic acid. It may be deaminated back to pyruvate for use in the KREBS CYCLE.

它通过转氨作用形成,氨基由谷氨酰氨提供给丙酮酸,它还可以脱去氨基重新形成丙酮酸在三羧酸循环中使用。

The functional relationship between the content of pyruvic acid and three factors,including maltose,glucose and tryptone,was fit using multi-power regression function method.

采用响应面法对丙酮酸发酵培养基成分葡萄糖、硫酸铵、蛋白胨进行优化,采用多元二次回归方程拟合3种因素与丙酮酸含量间的函数关系,并得到了最佳条件。

To 10 g of the substance being examined, coarsely powdered, add 100 ml of acetone R and allow to stand for 20 min. Add 1 ml of a solution containing 1.8 μg/ml of carbophenothion R in toluene R. Homogenise using a high-speed blender for 3 min. Filter and wash the filter cake with two quantities, each of 25 ml, of acetone R.

称取10g的检测样品,粉碎成粗粉,加入丙酮100ml,静止20min,加入1.8ug/ml的三硫磷-甲苯混合溶液1ml,高速搅拌3分钟,过滤,用丙酮洗涤滤纸两次,每次25ml。

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