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But the one step method that taking propene and hydrogen bromide as material synthesized 1-bromopropane was low cost, obtaining high-purity product ,and it's production process has no pollution to environment. One step method be deemed to the optimum method.

而以丙烯和HBr气体一步直接合成1-溴丙烷的方法成本较低,所得产物纯度较高,且其生产过程对环境是绿色的,可以说是生产1-溴丙烷的最佳方法。

The PECH obtained can be used to prepare energetic azide binders with top quality.

采用乳液双金属氰化物络合物代替Lewis酸类作为催化剂,使环氧氯丙烷开环聚合,制得相对分子质量较高及分子质量分布较窄的聚环氧氯丙烷,这种PECH可用于高质量的含能叠氮粘合剂中。

The solvolysis activity can be inhibited remarkably if a small amount of base was added in the medium. And the activity can be enhanced if acid was added.

原料中加入碱性物质可以显著抑制TS-1催化环氧丙烷溶剂解反应的活性;原料中添加酸性物质可以增强TS-1催化环氧丙烷溶剂解反应的活性。

The results showed that hydrogen peroxide, silanols species and TiO〓 didn't have solvolysis activity of propylene oxide. While framework Al, coordinatively unsaturated Ti〓 ions as Lewis acid sites in the framework, Ti-OH and the five member ring active titanium species formed by TS-1, hydrogen peroxide and solvent can catalyze the solvolysis of propylene oxide.

研究结果表明:原料双氧水和TS-1沸石上的SiOH和TiO〓对环氧丙烷溶剂解反应无催化活性;而下列物种对环氧丙烷溶剂解反应具有催化活性:TS-1中的骨架铝,沸石骨架中配位不饱和的Ti〓形成的L酸中心,TS-1水解产生的钛羟基和由TS-1,双氧水和溶剂相互作用所生成的五元环中间活性钛物种。

The results provide much useful information on the preparation of catalysts, the choice of reaction conditions, and the understanding of dehydrogenation process.

此外,文中还探讨了丙烷在各类负载型双组分催化剂上脱氢反应性能的差异,为进一步了解丙烷在其上脱氢过程提供了有益启示。

The preparation of grafted derivant of tertiary amine: it is prepared by the reacting of above (1) product and (2) product heated in water bath at 40℃ within 10min.

聚环氧氯丙烷乙二醇哌啶接支衍生物的制备:将上面制备的聚环氧氯丙烷乙二醇与0.25mol环氧丙基哌啶叔胺于40℃水浴条件下进行接支反应。

The preparation of esterified derivant : it is prepared by the esterifying reacting of above (3) product and 4g dodecylbenzene sulphonic acid heated in water bath at 40℃ within 30min.

聚环氧氯丙烷乙二醇哌啶接支酯化衍生物的制备:4g十二烷基苯磺酸于40℃水浴条件下聚环氧氯丙烷乙二醇哌啶接支衍生物进行酯化反应。

A small molecule core (TMP-SK3)with three terminal carboxyl groups was synthesized successfully by the reaction of 1,1,1-trihydroxymethylpropane with the excessive sebacic acid diacetic anhydride.

以1,1,1-三羟甲基丙烷与过量癸二酸二乙酸酐反应,制得了端羧基的三官能度小分子核三癸二酸三羟甲基丙烷酯(TMP-SK3)。

Epichiorohydrin was synthesized from alkali and glycerol dichlorohydrin which was synthesized from glycerol and industrial hydrochloric acid in the presence of catalyst and additive.

介绍了环氧氯丙烷合成新工艺:在催化剂和添加剂存在下,甘油与工业盐酸反应制得二氯丙醇,然后二氯丙醇与碱反应制得环氧氯丙烷产品。

Epichlorohydrin was synthesized from alkali and glycerol dichlorohydrin which was synthesized from glycerol and industrial hydrochloric acid in the presence of catalyst and additive.

摘 要:介绍了环氧氯丙烷合成新工艺:在催化剂和添加剂存在下,甘油与工业盐酸反应制得二氯丙醇,然后二氯丙醇与碱反应制得环氧氯丙烷产品。

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