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The coordination process and structure between amidoxime modified polyacrylonitrile fiber and FeCl3 in aqueous solution were studied by using X-ray photoelectron spectroscopy, Fourier transforminfrared spectrometer, dynamic thermal mechanical analyzer, and electrical conductivity method, respectively.

在室温条件下应用偕胺肟改性聚丙烯腈纤维与FeCl3反应制备了聚丙烯腈纤维铁配合物,并分别使用X射线光电子能谱、傅立叶红外光谱、动态热机械分析和电导法对Fe-AO-PAN进行了表征以确定其组成结构。

Polyacrylonitrile fiber was modified into a chelating fiber containing amidoxime group by adding hydroxylamine, resulting from that nitrile group was transformed into amidoxime group.

以聚丙烯腈纤维为原料,加入羟胺试剂,将腈基转变为偕胺肟基团,使聚丙烯腈纤维改性成含有偕胺肟基团的螫合纤维。

An acid dyeable polyacrylonitrile blend fiber was prepared by blending polyacrylontrile and a copolymer syn-thesized from trihydroxy methyl-aminomethane containing basic groups and acrylonitrile raonomr via wet spinning process.

用含有碱性基团的丙烯酸氨基酯与丙烯腈单体共聚,其共聚物与聚丙烯腈共混,经湿法纺丝制备酸性染料可染PAN共混纤维。

Activity ratio of acrylonitrile-ammonium itaconic acid copolymerization system and the changes of AIA content in two methods of comnonomer adding were studied in this paper.

研究了丙烯腈-衣康酸铵共聚体系的竞聚率和不同加料方式下聚丙烯腈树脂中衣康酸铵含量的变化规律。

In the second section, with ketone and hydroxylamine hydrochloride as the starting materials, 3-aminopropanol is prepared via three steps including reaction of ketone and hydroxylamine hydrochloride , condensation of ketoxime and acrylonitrile, and hydrogenation cracking of condensation product.

第二是3-氨基丙醇的制备,由酮肟丙烯睛缩合物催化氢化裂解制得:即先以酮、盐酸羟胺为起始原料在碱性条件下合成酮肟,再与丙烯腈反应生成酮肟丙烯腈缩合物后经催化氢化裂解制得3-氨基丙醇。

In order to compare with normal wet spinning PAC fibre, the morphological characteristics, including void siz, distribution, volume, shape, location, surface crevices etc. of the polyblend fibre and their change during stretching, was studied by SEM, SAXS, porosimeter and water retention methods.

用SEM、SAXS和保水率测定等方法,在与普通湿纺法聚丙烯腈纤维对比的基础上,对丙烯腈共混纤维在拉伸前后的形态特性,包括孔穴大小、体积、形状、位置和表面裂缝等进行了研究。

The results showed the pyrolytic process of polyacrylonitrile film can be divided into three stages.

用非等温热重法分析了聚丙烯腈薄膜的热解过程,探讨了升温速率对聚丙烯腈薄膜热重曲线和失重速率峰值的影响。

The desalting rate decreases with the rise of flow rate, and increases with the rise of voltage.

为了去除丙烯腈废水中的硫酸铵,采用电渗析法对丙烯腈废水进行脱盐处理。

Using the proposed vertical rotating packed bed,the acrylonitrile monomer removal efficiency from polyacrylonitrile can be achieved to over 99% upon twice devolatilized.

采用该技术对丙烯腈系聚合物进行两次循环脱挥处理,丙烯腈脱除率达到99%以上。

The content of SF in this polymerizing system does not affect the rates of the said homopolymerization and copolymerization,but causes a drastic change of the average molecular weights of the polyacry...

聚合体系中SF的含量在一定范围内变化时,对AN均聚和AN-MA-SMAS共聚的反应速度均无影响,但引起聚丙烯腈和丙烯腈共聚物的平均分子量的急剧变化。

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