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丙二醇

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Molybdenum-glycol complexes synthesized with different alkylene glycols and Mo/alcohol ratios have different acidity and catalytic activity. For the topic reaction, the catalytic activity of Mo-1, 2-ethandiol or Mo-1, 2-propanediol is higher than that of Mo-butanediol.

结果表明,用不同的二醇和不同醇/钼比制备的钼醇催化剂具有不同的催化性能和酸性,用乙二醇和丙二醇制备的催化剂,催化性能优于丁二醇制备的催化剂。

Using butyraldehyde and 1,2-propanediol as raw materials, H3PW6Mo6O 40 /TiO2 as catalyst, butyraldehyde 1,2-propanediol acetal is synthesized.

以二氧化钛负载磷钨钼杂多酸为催化剂,通过丁醛和1,2-丙二醇反应合成了丁醛1,2-丙二醇缩醛。

Water,glycerin,rosa centifolia flower water,butylene glycol,centaurea cyanus flower water,peg-40 hydrogenated castor oil,propylene glycol,ppg-26-buteth-26,phenoxyethanol,methylparaben,sorbic acid,benzophenone-4,pentadecalactone,citrus aurantium dulcisoil,panthenol,menthyl lactate,sodium hydroxide,glycyrrhiza glabraroot extract,aesculus hippocastanumseed extract,citrus aurantium amaraoil,allantoin,limonnene,linalool,blue 1(ci 42090),yellow 5ci 19140

水,甘油,千叶蔷薇花水,丁烯二醇,矢车菊花水,PEG-40氢化蓖麻油,丙二醇,PPG-26-丁醇聚醚-26,苯氧乙醇,对羟基苯甲酸甲酯,山梨酸,二苯甲酮-4,环十五内酯,甜橙油,泛醇,乳酸孟酯,氢氧化钠,甘草根萃取,七叶树籽萃取,苦橙油,尿囊素,柠檬精油,芳樟醇,蓝,黄水:几乎所有护肤品成分第一位都是水。

By using ethanol precipitative pretreatment and rectification patent technology,the product 1,3-propanediol with purity of 99% had been harvested,the seperation yield of 1,3-propa...

采用发酵液醇沉预处理、再精馏的专利技术可分离得到纯度大于99%的1,3-丙二醇产品,分离收率大于85%,产品质量达到了聚对苯二甲酸丙二酯聚合反应的要求。

Propanediol (1,3-PD) is an important intermediate in the production of polyesters propylene terephthalate.

1,3-丙二醇是合成聚对苯二甲酸丙二醇酯的重要原料。

The project to be built with an annual output of 20,000 tons a polyethylene terephthalate plant. Adopting advanced and mature direct esterification process for the production of raw materials for purified terephthalic acid and 1,3-propanediol.

本项目拟建设一套年产2万吨聚对苯二甲酸丙二醇酯生产装置,采用国内先进成熟的直接酯化法生产工艺,主要原料为精对苯二甲酸和1,3-丙二醇

The effect of reagents, reaction temperature, dinitrogen tetroxide and nitric acid on the yield and purity of 1,2-propanediol dinitrate were also investigated.

结果表明,N_2O_5和环氧丙烷硝化的主产物是1,2-丙二醇二硝酸酯,副产物是1,2-丙二醇单硝酸酯。

The results indicated that CHCl3 was optimum reagent and the reaction temperature was better controlled at 10~15℃. Dinitrogen tetraoxide and nitric acidhad a detrimental effect on the yield and purity of 1,2-propanediol dinitrate. When the concentrations of dinitrogen tetroxide and nitric acid were below 1.00% and 5.53% respectively, these detrimental effects could be neglected. Under the optimum conditions, the yields and the purity of 1,2-propanediol dinitrate were 99.01% and 95.89%, respectively.

同时考察了反应溶剂、反应温度、N_2O_5中N_2O_4和HNO_3杂质对1,2-丙二醇二硝酸酯收率和纯度的影响,结果表明,适宜的溶剂是CHCl3;适宜的反应温度为10~15℃;在适宜条件下,1,2-丙二醇二硝酸酯的收率和纯度可分别达到99.01%和95.89%;N_2O_4和HNO_3对产物的收率和纯度均有不利影响,但当N_2O_5中N_2O_4含量小于1.00%,HNO_3含量小于5.53%时,对产物收率和纯度的影响不大。

In this paper, the acetalization of benzylaldehyde and 1,3-propanediol in the presence of vanadium phosphorus oxide catalyst was studied.

研究了苯甲醛与1,3-丙二醇在钒磷氧催化剂作用下的缩醛化反应,考察了反应时间、醇醛比、催化剂用量、带水剂种类和用量等因素对苯甲醛1,3-丙二醇缩醛收率的影响。

The results showed that the suitable condition for the reaction are as follows: benzaldehyde/1, 2-propylene molar ratio is 1:1.4, the mount of potassium dodecatungstocobaltate trihydrate (K5CoW12O403H2O) is 0.5g, the volume of cyclohexane is 9 mL, and reaction time is 70 min.

实验结果表明,杂多化合物K5CoW12O403H2O是合成环己酮l, 2-丙二醇缩酮的良好催化剂,在酮醇物质的量比为l:1.4、催化剂质量为0.5g、带水剂环己烷体积为9mL、反应时间为70min的最佳条件下,环己酮l, 2-丙二醇缩酮的收率最高可达94.2%。

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