不含氮的

Starting from 3-benzoyl-5-formyl-indolizine, 3-benzoyl-5-(2'2'-diacetylethenyl)-indolizines and analogs were obtained by the 〓mediated aldol condensation or Wittig reaction. These compounds,promoted by low-valent titanium, gave highly functionlizedcycl[3,2,2]azine derivatives. The coupling reaction proceeded betweenthe carbonyl group and the carbon-carbon double bond, a rare example inMcMurry reaction.

我们以3-苯甲酰基-5-甲酰基中氮茚为原料，通过三碘化钐促进的aldol反应和Wittig反应制备了3-羰基-5-羰基乙烯基中氮茚，随后经低价钛还原偶联，没有生成正常的分子内羰基-羰基偶联产物，而是得到反常的羰基与α，β-不饱羰基的双键偶联产物，较高收率地得到了含多官能团的CycI[3，2，2]azine衍生物。

First of all, this study will be multi-walled carbon nanotubes by chemical oxidation process purified so it can be modified to deal with than the purification of purity before the modified 5 wt%, more than 1.89 times the surface area to increase the surface potential decrease of about 10 ~ 20 mV and the surface functional base (-COOH and-OH) to increase 1.45 times, and then the control technology of electroless preparation parameters include: analysis of plating time, plating analysis of temperature, metal ions in solution than the (Fe2+/ Ni2+), bath pH and the added value of dispersion Agent and other research towards Fe-Ni particles to increase the iron content and Fe-Ni particles spread in the MWCNT upper fixed targets,the results found that when the parameters for the preparation of 50 ℃, pH10, do not add dispersant, metal ions than the solution (Fe2 +/ Ni2 +) 7, the highest iron content can be Fe = 40.55 at%(flat iron content 111.17 mg / g) of nanocomposites Fe-Ni/CNT, then for a series of the nature of its analysis, the final evaluation Fe-Ni/CNT nanocomposites were processed on the effectiveness of the application of mixed pollutants, the results showed that in 120 minutes at the same time when Adsorption of heavy metal ions lead nitrate 10 ppm, selenium heavy metal ion degradation of 1 ppm and orange azo dye AO7 50 ppm standard of effluents, and after a total Fe-Ni nano-particles to SEM / EDS analysis of more than 50% still remaining.

本研究首先将多壁奈米碳管以化学氧化法做纯化改质处理能使其纯度较纯化改质前提高5 wt％、比表面积提高1.89倍、表面电位下降约10~20 mV以及表面官能基提高1.45倍，再控制无电镀技术之制备参数包括：析镀时间、析镀温度，镀液中金属离子比(Fe2+/Ni2+)、镀液pH值及是否添加分散剂等，研究朝提高Fe-Ni粒子的含铁量与Fe-Ni粒子散布固定在MWCNT上等目标进行，研究结果发现当制备参数为50 ℃、pH10、不添加分散剂、镀液金属离子比(Fe2+/Ni2+)7时，可得到最高铁含量Fe = 40.55 at％(单位铁含量111.17 mg/g)之奈米复合材料Fe-Ni/CNT，接著对其作一系列性质分析，最后评估奈米复合材料Fe-Ni/CNT对共处理混合污染物之应用效益，结果显示其在120分钟时能够同时吸附重金属硝酸铅离子10 ppm、重金属硒酸根离子1 ppm及降解偶氮橘色染料AO7 50 ppm达放流水标准，且共处理后奈米Fe-Ni粒子以SEM/EDS分析仍剩余50 %以上。

The addition of MCMP had not only ensured the water quality of treated effluent to be up to first-class B of "Discharge standard of pollutants for municipal wastewater treatment plant"(GB18918-2002), but also achieved the removal of N and P effectively. Based on surveying the content of heavy metals, the T-Hg is about 81% higher, the TAs is about 110% higher, the TNi is 46% higher, the TK is 24% higher, the TP is 7% higher, the TCr is 64% lower, the TN is 29% lower. The MLVSS/MLSS is lower. The SVI value is from 19.3 to 26.23. This method needed no changes for wastewater treatment process and operation pattern, the extra consumption of power was also needlessness.

但同时发现，总汞较试验前提高81%，总砷较试验前提高110%，总镍较试验前提高46%，总钾较试验前提高24%，总磷提高7%；总铬较试验前减少64%，总氮减少29%，污泥的MLVSS/MLSS值略有降低，SVI值从19.3增加到26.23，为了保证排放的污泥中重金属含量不超标，在以后的实际生产运行中，需要定期以排泥形式排出含重金属等污染物的污泥，以保证污水处理的正常运行。

The use of benzazepin-N-acetic acid derivatives which contain an oxo group in the a position to the nitrogen atom and are substituted in the 3 position by a 1--cyclopentyl-carbonyl-amino radical, and of their salts and biolabile esters, for the prophylaxis and/or treatment of heart damage caused by cardiotoxic doses of medicaments or chemicals, in larger mammals and in particular humans.

本发明涉及苯并氮杂∴－N－乙酸衍生物及其盐和生物不稳定的酯的应用，其中苯并氮杂∴－N－乙酸衍生物在氮原子的α位置含有氧代基，且在3－位置上被1－－环戊基－羰基－氨基残基取代，用于预防和/或治疗大的哺乳动物和特别是人体的心脏损伤，其中心脏损伤是由心脏中毒剂量的药物或化学品引起的。

Amino-6-nitrobenzodifuroxan was prepared through a three-step reaction from starting material 3, 5-dinitrobenzoic acid:(1)3, 5-dinitroaniline (1) was synthesized from the reaction of DNBA and hydrazoic acid in inert solvent 1, 2-dichioroethane through Schmidt rearrangement with yield of 89.6%;(2) 1 was subjected to nitration to prepare pentanitroaniline (2) with yield of 51.1%;(3) The title compound was prepared from 2 and sodium azide in acetic acid through denitrogenation and then Schmidt rearrangement with yield of 86.8%, m.p.204℃～206℃.

以3，5-二硝基苯甲酸为原料经过3步反应合成了7-氨基6-硝基苯并二氧化吠咱：第1步反应，在二氯乙烷惰性溶剂中，DNBA与叠氮酸反应并发生Schmidt重排反应生成3，5-二硝基苯胺(1)，产率89.6%；第2步反应，1在含100%硫酸的硝硫混酸中硝化生成五硝基苯胺(2)，产率51.1%；第3步反应，2与叠氮酸反应，不经分离直接进行热解脱氮、Schmidt重排反应，得到目标化合物， m.p.204℃~ 206℃，产率86.8%。

According to the microalloying and strengthening and toughening principles of steel,a theoretical calculation method and optimum alloying design to determine titanium content in carbonizing steel were proposed.

根据钢铁材料的微合金化原理和强韧化原理，对广泛使用的含钛渗碳钢的钛含量进行了理论计算分析和优化设计，结果表明，适当降低钛含量，不影响其在渗碳过程中阻止奥氏体晶粒长大的作用，但可有效地减少或消除含钛渗碳钢中的液析氮化钛，从而提高钢材的力学性能。

The product poses a chemical risk because the dark blue thermal collar inside the sleeping bag was found to yield 75 mg/kg of the azo-colourant 3,3'- dimethoxybenzidine.The product does not comply with the REACH Regulation.

通报的理由为该睡袋不符合欧盟 REACH 法规（化学品注册、评估、授权和限制法规），深蓝色睡袋头部含偶氮着色剂3，3'-二甲氧基联苯胺75 mg/kg ，有化学风险。

It is vapour, coal, diesel oil made to take off discreditedly to the crude oil high in sulphur content, produce stench because of including sulphur alcohol.

常见的杂质有含硫，氮，氧的化合物，以及混在油中的蜡和胶质等不理想成分。它们可使油品有臭味，色泽深，腐蚀机械设备，不易保存。

Finally, according to market conditions and market products this article paper analyzes the trends in the development of camera technology, and designs a color night vision camera.

最后根据市场情况和市面上产品的情况分析了摄像机技术的发展趋势，并设计了一款彩色夜视摄像机。

Only person height weeds and the fierce looks stone idles were there.

只有半人深的荒草和龇牙咧嘴的神像。