下代

Alkylamine reaction with dialkyl cyanodithioiminocarbonate was catalyzed by quaternary ammonium salts at room temperature to yield 3-alkylamine-5-amino-1,2,4-triazole in good quality and high yields. After imidization and reaction with an α,β-unsaturated acid derivative, the reaction intermediate was hydrolyzed in the presence of a Lewis acid to obtain the target product.

烷基胺与氰基亚胺硫代二甲酯在季氨盐催化作用下得到质量好、收率高的3-烷氨基-5-氨基-1，2，4-三氮唑，进一步经过亚胺中间体并与α，β-不饱和酸酯作用后，中间产物在Lewis酸催化作用下水解得到三唑嘧啶酮。

In this paper, through a series of experiments, two series of quaternary-ammounium Gemini surfactants were synthesized, namely the pair alkylene double quaternary ammonium salt surfactant m-s-m·2Br and the pair the alkylene double quaternary ammonium salt surfactant -s-·2Br. We has carried on the attribute with the infrared spectrum to its structure, and to affected the factor which the synthesis pair the alkylene double quaternary ammonium salt surfactant responded to carry on the discussion. We has discovered the synthesis pair the ethylene double quaternary ammonium salt surfactant m-2-m·2Br optimum condition: The bromo alkane and a tetramethyl ethylene diamine mole of ratio is 3.0: 1.0, makes the solvent by the ethyl alcohol, 80℃ under responds for 48 hours in the backflow temperature; Synthesis pair alkylene double quaternary ammonium salt surfactant 12-S-12 ·2Br optimum condition: 12 tertiary amine and 1, 3- propylene dibromide (1, 4- two bromines butane) a mole of ratio is 2.2: 1.0, makes the solvent by the ethyl alcohol, responds for 48 hours in the constant temperature 80 ℃ under backflow.

本文通过一系列的实验，合成了两个系列的Gemini型表面活性剂，即双烷撑双季铵盐表面活性剂m-s-m·2Br和双烷撑双季铵盐表面活性剂-s-·2Br，用红外光谱对其结构进行了表征，并且对影响合成双烷撑双季铵盐表面活性剂反应的因素进行了讨论，找出了合成双乙撑双季铵盐表面活性剂m-2-m·2Br的最佳条件：溴代烷与四甲基乙二胺的摩尔比为3.0：1.0，以乙醇作溶剂，在回流温度80℃下反应48小时；合成双烷撑双季铵盐表面活性剂12-s-12·2Br的最佳条件：十二叔胺与1，3-二溴丙烷(1，4-二溴丁烷)摩尔比为2.2：1.0，以乙醇作溶剂，在恒温80℃下回流反应48小时。

The apriori and aposteriori H〓-optimal filtering question can be solved directly. L〓 Apriori and aposteriori filtering with an H〓 error bound can be solved by semidefinite programming. Robust H〓 apriori filtering and robust apriori L〓 filtering in discrete-time system are subject to a nonconvex constraint.

对这些滤波问题解法的改进同连续系统下的情况基本类似，对确定性系统的H〓验前滤波和验后滤波，本文解法可直接得出最优滤波问题的解；对H〓约束下的L〓验前滤波及验后滤波，其解可归结为一凸优化问题；但不确定性系统H〓验前滤波和鲁棒L〓验前滤波的LMI解法中有了非凸约束，因此要用迭代法求解。

The parameter adjust algorithm is also deduced. The canceling methods are discussed when the unideal factor of the device is known or unknown. The result proves that when the unideal factor of devices is unknown, the parameter solved by the iteration is convergent to that when the unideal factor is known.

本文推导了参数调节算法，并讨论了器件不理想因子已知与未知两种情况下的消除方法，证明了在器件不理想因子未知情况下采用迭代方法确定的参数最终收敛于不理想因子已知情况下的参数。

Adenosine was used as the raw material, dissolved in triethyl phosphate and then esterified with thiophosphoryl chloride under 0~5℃ for 8h without water and oxgen, in alkaline condition provided by 2,6-dimethylpyridine, introducing thiophosphoryl ester to adenosine.Then superfluous triethylamine was added and reacted under 5℃ for 1h to synthesize rough 5'-AMPS.The unpurified product was appled to a DEAE Sephadex A-25 column and eluted with triethylammonium bicarbonate.

用腺苷为起始原料，溶解于磷酸三乙脂中后，在无水无氧环境中及2，6-二甲基吡啶提供的碱性条件下与三氯硫磷以0~5℃下发生酯化反应8h，将硫代磷酸酯引入腺苷，然后再与过量三乙胺在5℃下反应1h，合成粗产品，再用碳酸氢三乙胺作洗脱液，过DEAE Sephadex A-25凝胶柱纯化。

1A series ofω-alkylmercapo acid were synthesized by two methods:one involved the reaction of the appropriateω-bromoalkyl acid with mercaptide under the presence of base;the other method was used only for the long alkyl compound by the reaction ofω-alkenyl acid and alkanethiol in the presence of AIBN.

正是基于以上考虑，本论文探索了合成下沿带有硫醚官能团，而上沿带有偶氮官能团的杯[4]芳烃衍生物的方法，进行了以下研究： 1采用ω-溴代羧酸和烃基硫醇在碱性条件下发生反应，或由ω-烯基羧酸和硫醇在AIBN的存在下反应，得到了ω-硫醚羧酸，使用氯化亚砜将羧酸转化为酰氯。

The results showed that resistant gene Ht in F1 heterozygote was the most effective on controlling spots number and size; all monogene in heterozygote could produce spore by moisture culture and resistant gene Ht1 was the most effective; resistant gene Ht1 in medium level, Ht3 in high level, and Ht in low level of vertical resistance of heterozygote, were the most effective on controlling spots spread; while Ht2 in high level of vertical resistance of heterozygote was the most ineffective on controlling spots spread; and all resistant monogene in heterozygote showed superior to their parents on controlling incubation period and gene Ht was more significant than other genes.

结果表明，抗性单基因Ht处于F1代杂合状态时，控制病斑数和病斑面积的效应最强；单基因处于杂合状态时，湿培48h病斑全部能产生分生孢子，且处于同一水平抗性杂合状态时，Ht1控制产孢量的效应最强；Ht1处于中水平、Ht3处于高水平和Ht、处于低水平垂直抗性杂合状态下，控制病斑扩展效应最强；而Ht2处于高水平垂直抗性杂合状态下，控制病斑扩展效应最弱；抗性单基因处于杂合状态下，控制潜伏期多表现超亲现象，Ht控制病害潜伏期比其它单基因显著。

When reached logarithm growth phase, it was poured or the medium was removed. 5 mL medium containing 10 mg/L mitocin-C was added , kept at 37 ℃, and then cultured in saturated humidity warm box with the CO2 of 0.05 fraction volume for 2 or 3 hours. It was coated with 0.1% gelatin in 6-hole plate, laid for over 30 minutes, and then threw away or the medium with mitocin-C was removed, washed with phosptat buffer for 5 times so as to remove the mitocin-C. 2 mL 0.05% trypsin digestive cells were added, and it was observed under microscope. When crevice appeared, cells became round (about 2－4 minutes), digestion was stopped by adding medium of the same volume, and blew up with straws repetitively to make it into monoplast suspension. Special-used cover glass was put in the center of cell counting chamber. Cells were sucked in by glass siphon, and cell suspension flew out at bucket of up or down-sides of counting chamber, until the cover glass was filled with fluid. Living cell were inoculated at concentrations of 3×108, 5×108, 1×109 L－1 after their number counted.

选取2～5代的小鼠胚胎成纤维细胞，待其至对数生长期倒掉或吸掉培养基，加入含10 mg/L丝裂霉素C的细胞全培养液5 mL，置37 ℃，体积分数0.05的CO2饱和湿度温箱中培养二三小时，在6孔板中加入0.1%明胶包被，放置30 min以上，倒掉或吸掉含丝裂霉素C的培养基，磷酸盐缓冲液清洗5遍，尽量除去丝裂霉素C，加入2 mL 0.05%的胰蛋白酶消化细胞，镜下观察，当细胞间出现裂隙，细胞变圆时（约2～4 min），立即加入等量的全培养液终止消化，并用吸管反复吹打，使之成为单细胞悬液，在细胞计数板中央放置专用的盖玻片，用玻璃虹吸管吸取细胞，让虹吸管在盖玻片上或下侧的计数板凹槽处流出悬液，至盖玻片下被液体充满为止。

Based on the date of outcrop, log and lithology, sequence stratigraphic division and correlation were made on Neopaleozoic in south of North China Basin, and high-precision geologic correlation framework was built up in the basin.2. In the term of sedimentary features of Neopaleozoic in south of North China Basin, lateral variation of sedimentary facies was studied selectively in Benxi-Taiyuan Formation, Shanxi Formation, Lower Shihezi Formation, Upper Shihezi Formation and Shiqianfeng Formation. Lithofacies paleographic features and the sedimentary evolutionary process of Late Paleozoic in south of North China Basin were worked also.3. On the basis of sand-bodies Isopach figure drawing, the distribution of major reservoir sand-bodies of Neopaleozoic in south of North China Basin was studied. Basing on the distribution of sand-bodies in sequence stratigraphic framework, combining the development and distribution features of barrier and underwater distributary channel, there is a disquisition on the distribution regularity of pay reservoir sand-bodies of Neopaleozoic in this area.

以露头、测井和岩性资料为基础，对华北盆地南部上古生界进行了层序地层的划分与对比工作，建立了盆地范围内的高精度地层对比格架。2、根据华北盆地南部上古生界的沉积特点，按本溪组—太原组、山西组、下石盒子组、上石盒子组和石千峰组5个层组分别开展了沉积相的横向变化对比研究，并以此为基础探讨了华北盆地南部晚古生代的岩相古地理特征及其沉积演化过程。3、以编制砂体等厚图的方式研究了华北盆地南部上古生界主要储集砂体的平面展布规律，并以层序地层格架下的砂体展布研究为基础，从沉积体系控制下的砂体分布特点出发，结合障壁岛与水下分流河道的发育与分布特点，系统深入地开展了区内上古生界有利储集砂体的分布规律研究。

From research,It is known that the flux of single-phase transformer would offset and exciting current of single-phase transformer would be distorted under DC current inrushing.

直流电流通过两个Y0连接的变压器中性点侵入电力系统，故针对三相三柱变压器直流入侵情况建立了直流入侵下的三相三柱变压器的电路模型和相应的方程，结合三柱磁路的麦克斯韦方程和非线性的B—H曲线方程，利用数字迭代法，在MATLAB环境下编程计算了三相三柱变压器直流入侵下的变压器励磁电流和谐波特征。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。