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Comparing with the result of methyl iodide in intense laser field, some differences are observed:(1) at the same laser field intensity, the highest charged fragment ion of methyl bromide was Br(superscript 3+), lower than I(superscript 6+) of methyl iodide;(2) the dehydrogenation channel was observed in the multiphoton dissociation or Coulomb explosion of methyl bromide, but was not observed in the case of methyl iodide;(3) HBr(superscript +) was observed, but there was no similar channel in the case of methyl iodide;(4) for methyl bromide, the valid charge distance of Coulomb explosion increases with the product of p and q; while in the case of methyl iodide, the distance remained almost the same;(5) the producing channel of CH(superscript + subscript m)(m=0, 1, 2) is different from the ionization-dissociation of methyl iodide in which the stepwise dissociation of CH3(superscript +) was thought to be the main channel, CH(superscript + subscript m)(m=0, 1, 2) of methyl bromide are mainly from the products of the direct dissociation of the dehydrogenated parent ions instead of the stepwise dissociation of CH3(superscript +).

与碘甲烷在强场中的实验结果对比发现:(1)在相同的激光场强下,碘甲烷电离解离的最高价碎片离子为I(上标 6+)而溴甲烷为Br(上标 3+);(2)溴甲烷质谱中存在母体离子的脱氢产物CHBr和CHBr(上标 2+),而对于碘甲烷,没有检测到这些通道,C-I键首先断开;(3)质谱中存在H^79Br和H^81Br,而碘甲烷的电离解离中不存在HI产物;(4)溴甲烷库仑两体爆炸的有效电荷间距随着两碎片电荷乘积的增大而增大,而对于碘甲烷此间距几乎不随电荷乘积变化;(5)CH(m=0, 1, 2)的主要生成通道可能与碘甲烷不同,不是来自CH3的顺序脱氢,而是来自脱氢母体离子的直接解离。

Wo hydrogen-adsorped peaks of TPR, namely α and β peaks, which can be ascribed to Mo(superscript 6+)→Mo(superscript 5+) and Mo(superscript 5+)→Mo(superscript n+)(n=4, 3, 2) reduction processes respectively, appear both at sulfured state and functioning state. The experiment results indicate that there is a close relation between the altitude of the peaks and the activity of the catalyst at low temperature.

PR表征结果示出,硫化态及工作态催化剂皆出现α、β2个吸氢峰,可分别归属Mo(上标 6+)→Mo(上标 5+)和Mo(上标 5+)→Mo(n=4, 3, 2)的还原过程;工作态催化剂α峰峰温较硫化态低,β峰为宽峰带低价钼混合峰;吸氢峰的大小与催化剂低温活性密切相关。

Different alkaline earth metal ions, such as Ca(superscript 2+), Mg(superscript 2+) and Zn(subscript 2+), were introduced and their influences on the working characteristics, crystalline behavior as well as the electrical properties were studied.

通过引入Ca(上标 2+),Mg(上标 2+),Zn(上标 2+)等不同的二价金属离子,重点讨论了它们对玻璃的特征温度、分相析晶行为以及膨胀系数、电学性质的影响。

Methods The pyrogllol auto-oxidation was adopted to produce superoxide anion O(superscript - subscript 2; the system H2O2/Fe(superscript 2+) was used to produce hydroxy radical through Fenton reaction; and spectrophotometry was used to detect the clearing functions of drugs with different concentrations against O(superscript - subscript 2) and OH.

采用邻苯三酚自氧化法产生超氧阴离子自由基O(上标-下标 2,采用H2O2/Fe(上标 2+)体系通过Fenton反应产生羟自由基,用分光光度法分别测定不同浓度的药物对O(上标-下标 2)是和OH的清除作用。

Methods IO(superscript - subscript 3) was prepared by quantitative oxidation of bromine water, with the excessive bromine removed with formic acid. In the presence of excessive iodide, I(superscript -) would be oxidized by I(superscript - subscript 3) to form 3 times of I(superscript - subscript 3) in mol, displaying maximal absorption at 286nm in ultraviolet zone and a slightly low apex at 345nm.ε286=1.3×10^5 Lmol^(-1)cm^(-1),ε345=8.1×10^4 Lmol^(-1)cm^(-1), with both showing high sensitivity.

利用溴水定量氧化I生成IO(上标-下标 3),再用甲酸除去过量的溴,IO(上标-下标 3)在过量碘化物存在下氧化I产生3倍摩尔量的I(上标-下标 3),在紫外光区的286nm具有最大吸收,并在345nm处另有一略低的吸收峰,ε286=1.3×10^5 Lmol^(-1)cm^(-1),ε345=8.1×10^4 Lmol^(-1)cm^(-1),均具有很高的灵敏度。

The amount of Na(superscript +), NH4(superscript +), K(superscript +), Mg(superscript 2+), Ca(superscript 2+), Zn(superscript 2+) in fruits and juice (sports water, green tea , pear juice, carrot juice and carrot and orange juice) were respectively separated and detected by non-suppressed ion chromatography. And pyridine-2, 6-dicarbexylic was used as mobile phase to separated monovalent cations and pyridine-2, 6-dicarbexylic-ethylenedi-amine-oxalic acid was used as mobile phase to separated divalent cations.

采用非抑制型离子色谱法测定了水果以及饮料(运动型饮料、绿茶、水蜜桃汁、胡萝卜汁和胡萝卜橙汁)中Na、NH4、K、Mg(上标 2+)、Ca(上标 2+)、Zn(上标 2+)的含量,其中一价阳离子以吡啶-2,6-二羧酸为淋洗液测定,二价阳离子以吡啶-2,6-二羧酸+乙二胺+草酸为淋洗液测定。

When pH is 8.0, the flocculation rate can reach 91%. The experiment indicates that the evaluation system of kaoline is affected by PO(superscript 3- subscript 4) and Ca(superscript 2+) when the concentration of PO(superscript 3- subscript 4) is high in the substrate. As the real flocculation efficiency cannot be achieved, the evaluation system needs to be modified.

实验表明,培养基中PO(上标 3-下标 4)浓度较高时,现有的微生物絮凝剂高岭土评价体系会受到PO(上标 3-下标 4)与Ca(上标 2+)的影响,不能真实地表示微生物絮凝剂的絮凝效果,需要对现有评价体系进行修改。

Templating agent could not be sufficiently removed at temperature below 500℃, while temperature exceeding 600℃ might result in collapse of the framework. The conversion from Co(superscript 2+) to Co(superscript 2+) was a gradual time-consuming process. Calcination at 550℃ in a muffle furnace for 10 hours could remove the templating agent and bond water and give a satisfactory result.

焙烧温度和时间决定CoAPO-5分子筛最终的物化性能,焙烧温度低于500℃不能有效去除模板剂,而高于600℃将导致分子筛骨架的破坏,Co(上标 2+)向Co(上标 3+)转化是一个逐渐转化的过程,550℃下焙烧10h,能较好地去除模板剂和结合水及实现Co(上标 2+)的转化。

Results Colifrom bacterium, staphylococcus albus, cerea bacillus, bacillus aeruginosus and yeast fungus can resist to arsenite.

结果 绿脓杆菌可耐受100 mg/L的As(上标 3+)浓度,大肠埃希菌、白色葡萄球菌、蜡样芽孢杆菌和酵母菌均可耐受1000 mg/L的As(上标 3+)浓度;大肠埃希菌对As(上标 3+)有一定的富集能力。

The judge's total reduced score was significantly correlating with those reduced score of push-off r=0.733(superscript *, second fly phaser=0.871(superscript *, and landing r=0.707(superscript *.

四、裁判之总扣分与推撑部分r=0.733(上标*,第二飞程部分r=0.871(上标*,及著地部分r=0.707(上标*之扣分达显著相关。

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