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Its steps include these:(1) purification of WPA;(2) neutralization reaction between purified WPA and sodium carbonate for the salt mixture of disodium hydrogen phosphate and monometallic sodium orthophosphate;(3) adjustment of the mixture's neutralizing degree with additive acid or alkali;(4) quick separation of crystal with additive organic solvent under continue stir;(5) polymerization of crystal under the high temperature for the high quality product of STPP.

其步骤为:(1)湿法磷酸净化;(2)净化后的磷酸与碳酸钠中和反应生成磷酸一氢钠和磷酸二氢钠混合盐溶液;(3)用酸、碱调节确定该混合盐溶液的中和度;(4)加入有机溶剂,通过不断地搅拌使晶体快速析出;(5)晶体经高温聚合,生成高品质的三聚磷酸钠。

In the wet-process phosphoric acid production from the Hubei phosphate ore, one of the bothersome problems is that potassium fluosilicate and sodium fluosilicate scales are liable to form on the filtration system owing to its high potassium and sodium content, which greatly restrains the application of Hubei phosphate ore.

本文首先采用人工冷却系统模拟湿法磷酸生产的真空过滤系统冷却过程,研究垢物的析出规律,实验结果得知:垢物的主要成分为氟硅酸钠和氟硅酸钾,氟硅酸钠首先析出,结构致密,其次是氟硅酸钾,最后是二水硫酸钙,氟硅酸钠对氟硅酸钾有很强的结晶诱导作用;然后在三种生产中常用的不同的材质钼二钛、聚氯乙烯和聚四氟乙烯表面进行结垢试验,发现聚四氟乙烯表面最不易结垢,而在钼二钛表面最易结垢。

Based on adequate survey to faults of sodium pump for The China Experiment Fast Reactor, in order that the advanced diagnosis methods are used in the sodium pump which is under fabrication, different methods of fault diagnosis system of sodium pump are designed and programmed; and the principal component analysis is used to fault diagnosis system of main coolant pump in a nuclear power station. The feasibility of fault diagnosis systems developed have been proved by simulation results.

本课题对中国实验快堆钠泵的故障进行了研究,把先进的珍断方法应用到正在制造中的钠泵上,设计和开发了不同方法的钠泵的故障诊断系统;同时也应用主元分析方法,建立了某核电厂的主冷却剂泵的故障诊断系统,仿真实验证明了以上三个系统的可行性。

Based on adequate survey to faults of sodium pump for The China Experiment Fast Reactor, in order that the advanced diagnosis methods are used in the sodium pump which is under fabrication, different methods of fault diagnosis system of sodium pump are designed and programmed; and the principal component analysisis used to fault diagnosis system of main coolant pump in a nuclear power station. The feasibility of fault diagnosis systems developed have been proved by simulation results.

本课题对中国实验快堆钠泵的故障进行了研究,把先进的诊断方法应用到正在制造中的钠泵上,设计和开发了不同方法的钠泵的故障诊断系统;同时也应用主元分析方法,建立了某核电厂的主冷却剂泵的故障诊断系统,仿真实验证明了以上三个系统的可行性。

Seven central depressants,including chloral hydrate,potassium bromide,sodium bromide,cal- cium bromide,alcohol,amytal and chloretone, were studied for their effects on the intraperito- neal toxicity of tartar emetic and sodium stibo- gluconate in mice.

1。关于吐酒石与葡萄糖酸锑 V 钠对小白鼠的致死作用,我们探索了一些中枢抑制药与兴奋药的影响。所试的抑制药有水合氯醛,溴化钾,溴化钠,溴化钙,酒精,安眠妥与三氯叔丁醇七种。兴奋药有苯甲酸钠咖啡硷与士的宁二种,以及溴咖合剂。2。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3,3-二甲基-4-戊烯酸-3'-甲基-2'-丁烯酯工艺复杂、异戊烯大量分解问题,研究了MBDP直接返回循环使用工艺,MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺,比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果,筛选出回收MBDP&一锅煮&最佳工艺:按照n:n:n:n=1.0:9.8:9.2:0.05物质的量比投料,74℃~78℃反应21h,MBDP转化为贲亭酸甲酯和异戊烯醇,单程转化率87.7%,用85%的磷酸中和甲醇钠,蒸出甲醇,直接用于合成贲亭酸甲酯。

Silver nanoparticles with average particle size ranging from 2 to 131nm were manipulatively synthesized starting from silver nitrate using 10 kinds of different functional group-containing organic modifiers, such as polyvinylpyrrolidone, tween-80, sodium dodecyl sulfate, sodium polyacrylate, polyethylene glycol, D-sorbitol, sodium dodecyl sulfonate, sodium dodecylbenzene sulfonate, polyvinyl alcohol, cetyltrimethylammonium bromide, at room temperature.

摘 要:选择10种含有不同官能团的有机物为表面修饰剂,如聚乙烯吡咯烷酮、吐温-80、十二烷基硫酸钠、聚丙烯酸钠、聚乙二醇、山梨醇、十二烷基磺酸钠、聚乙烯醇、十二烷基苯磺酸钠和十六烷基三甲基溴化铵等,在室温下进行了平均粒径在2~131nm范围内纳米银颗粒的控制合成研究。

The mechanism of carbonization process of aluminate solution was analyzed thermodynamically. The results show that the internal reason of precipitation of Al3 in the process is its spontaneous nucleation caused by supersaturation of aluminate solution. The behaviors of SiO2 in the process are in accordance with that from published experiment, which implies that the content of product SiO2 from carbonization depends on its solubility but is not the result of absorption. The thermodynamic calculation for forming Na2O·Al2O3·2CO2· n H2O was achieved.

摘 要:为对高浓度铝酸钠溶液碳酸化分解过程中产品杂质含量的控制提供理论依据,分析了铝酸钠溶液碳酸化分解过程的热力学,认为该过程中Al3析出的真正机理是过饱和铝酸钠溶液的自发结晶;而基于分解过程中平衡浓度的热力学计算表明,在碳酸化分解过程中SiO2的变化规律与公认的三段变化规律一致,说明该过程产品中SiO2的含量取决于它在溶液中的平衡浓度,而非吸附所致;同时还分析了丝钠铝石的形成热力学。

This article mainly divides into three parts, The first part is the albite jade characteristic, uses traditional the gemology method conducts the research to the albite jade physical property as well as the structure, carries on the electron probe analysis to its chemical composition, and the discussion of its mineral component\'s chemical composition change carries on the SPSS statistical software; uses X powder crystal diffraction to determine its lattice parameter, mineral constituent\'s crystal structure conducts the research to the albite jade, carries on the analysis to the feldspar degree of order, and carries on the discussion to the albite jade\'s origin. The above method each other confirms mutually, confirms the data reliability.

本文主要分为三部分,第一部分为钠长石玉的性质,采用常规的宝石学方法对钠长石玉的物理性质以及结构构造进行研究,利用电子探针分析对其化学成分进行分析,并运用SPSS统计软件对其矿物成分的化学成分变化进行探讨;采用X粉晶衍射测定其晶胞参数,对钠长石玉中矿物组成的晶体结构进行研究,对长石的有序度进行分析,并对钠长石玉的成因进行探讨;上述方法彼此相互验证,以证实数据的可靠性。

In the current study, anoxic dechlorinations of p, p'-DDT,γ-HCH, HCB in the Liao River sediment were studied under the following conditions: without any additional short chain carbon substrates or vitamin B〓; with the addition of short chain carbon sources (including sodium lactate, sodium propionate or sodium acetate); with the addition of vitamin B〓; with the addition of both short chain carbon substrates and vitamin B〓, with the addition of sodium dodecyl sulfate , a kind of surfactant; the coexistence of the three chlorinated compounds.

本文分别采用不外加碳源和维生素B〓外加碳源(包括乳酸钠、丙酸钠或乙酸钠)、外加维生素B〓以及同时外加碳源和维生素B〓的方法,考察了p,p'-DDT、γ-HCH和HCB三种氯代有机污染物单独或混合存在下,在辽河沉积物中缺氧脱氯降解的情况,主要得到以下结论

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What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢?

I this is at that time, the opinion with peacockish true girl is full of in a heart.

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