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A total of one hundred fifty three healthy male and female adults were entered into a six month,doubleblind clinical study designed to evaluate the effect of a dentifrice containing 0.3% triclosan and 2.0% PVM/MA copolymer in a 0.243% sodium fluoride/silica base, relative to a 0.243% sodium fluoride silica base control dentifrice on supragingival plaque accumulation and gingivitis.

本研究的目的是证实含0.3%三氯羟苯醚,2.0%PVM/MA及0.243%氟化钠以二氧化硅磨料牙膏在减少菌斑积聚和牙龈炎形成方面对中国成年人群的效果。153名健康男女分为实验组及对照组,用双盲法评价6月后临床效果。采用纳入和排除的评价标准后进行了基线检查,实验对象每日使用分配的牙膏和软毛牙刷早晚刷牙一次,3个月和6个月再次检查。检查结果表明,使用含有三氯羟苯醚-共聚体牙膏组与使用不含该成分的对照组相比,实验对象的牙菌斑、牙龈炎指数分别减少16.1%及24.3%,均有统计学显著性意义(P<0.001)。

Owing to phosphorous acid is produced from phosphorus trichloride in industry by hydrolysts, inspissation and crystallization, if we use phosphorus trichloride directly on synthesize N- iminodiacetic acid, not only can simplify operation, but also can red.

原工艺采用的是在酸性条件下高温时将甲醛滴加到亚磷酸与亚氨基二乙酸一钠盐混合溶液中进行反应,考虑到工业上亚磷酸的合成一般采用三氯化磷水解、提浓、结晶制得,直接将三氯化磷用于双甘膦的合成,不仅可以简化操作过程,而且对于降低生产成本和能耗有明显意义。

Originally techniques dropped formaldehyde into the mixture of phosphorous acid and monosodium of imino diacetic acid in high temperature. Owing to phosphorous acid is produced from phosphorus trichloride in industry by hydrolysis, inspissation and crystallization, if we use phosphoros trichloride directly on synthesize N- iminodiacetic acid, not only can simplify operation, but also can reduce the cost and save energy.

原工艺采用的是在酸性条件下高温时将甲醛滴加到亚磷酸与亚氨基二乙酸一钠盐混合溶液中进行反应,考虑到工业上亚磷酸的合成一般采用三氯化磷水解、提浓、结晶制得,直接将三氯化磷用于双甘膦的合成,不仅可以简化操作过程,而且对于降低生产成本和能耗有明显意义。

The method on trans fatty acids analysis in food is very important. The effects of methylate sodium, potassium hydroxide, sulfuric acid and boron trifluoride in methanol and their different concentration and dosage on TFA analysis were studied. The chromatographic condition and the influence of time and temperature on the esterifation of TFA using boron trifluoride in methanol were optimized. A method for analyzing TFA were established by GC based on boron trifluoride in methanol and RT-2560(100m×0.25mm×0.2μm) capillary column.

研究了甲醇钠-甲醇、氢氧化钾-甲醇、浓硫酸-甲醇和三氟化硼-甲醇4种甲酯化试剂的浓度、用量及甲酯化时间和温度对反式脂肪酸检测的影响,优化了色谱条件,建立了以三氟化硼-甲醇法甲酯化,RT-2560(100m×0.25mm×0.2μm)毛细管柱为基础的反式脂肪酸气相色谱检测方法,C18:1-9 t, C18:1-11 t, C18:2-9 t, 12 t和C22:1-13 t 4种反式脂肪酸的最小检出浓度在0.774.08 mg/kg之间。4种反式脂肪酸不同添标浓度回收率为98.44%101.23%,重复测定的相对标准差在0.22%1.31%之间,有较好的准确度和重现性。

For more upgrade aluminium oxide yield, optimize indices, energy conservation and save cost, it is necessity to desilicify steps reconstruction.In order to overcome the shortcoming of the desilication used in Shangdong Alumina Corpotation,three technology such as indirect heating, continious desilication,deep desilication by separation of the sodium-silicon residue.

本文通过对理论界关于烧结法生产氧化铝脱硅原理的研究,结合国内主要氧化铝生产厂家脱硅实践方面的经验,针对山东铝业公司烧结法氧化铝生产脱硅工序的现状,运用间接加热连续脱硅、钠硅渣分离深度脱硅和HCAC法高效脱硅三项科研成果,对原有的三次脱硅工艺改为二次脱硅工艺。

Originally techniques dropped formaldehyde into the mixture of phosphorous acid and monosodium of imino diacetic acid in high temperature.

原工艺采用的是在酸性条件下高温时将甲醛滴加到亚磷酸与亚氨基二乙酸一钠盐混合溶液中进行反应,考虑到工业上亚磷酸的合成一般采用三氯化磷水解、提浓、结晶制得,直接将三氯化磷用于双甘膦的合成,不仅可以简化操作过程,而且对于降低生产成本和能耗有明显意义。

RESULTS: All aromatic anesthetics inhibited I at a holding potential which produce half-maximal current V(1/2; inhibition was modest with 1,3,5-trifluorobenzene (8%+/- 2%), pentafluorobenzene (13%+/- 2%), and hexafluorobenzene (13%+/- 2%), but greater with benzene (37%+/- 2%), fluorobenzene (39%+/- 2%), 1,2-difluorobenzene (48%+/- 2%), 1,4-difluorobenzene (31 +/- 3%), and 1,2,4-trifluorobenzene (33%+/- 1%).

结果:在最高电流的一半的控制电压下所有芳香族麻醉药都阻断钠电流;均苯三酚(8%+/- 2%)、戊苯(13%+/- 2%)、戌苯(13%+/- 2%)的抑制是适度的比苯(37%+/- 2%)、氟苯(39%+/- 2%),1.2-二氟二苯(48%+/- 2%),1,4-二氟二苯(31 +/- 3%),和1,2,4三氟苯(33%+/- 1%)明显。

The micelle shape transformation of tert-octylpheny phenol polyethylene glycol ether (TX-100), sodium dodecyl benzene sulfonate and tetradecyl trimethyl ammonium bromide in heavy water solutions was studied by 1H nuclear magnetic resonance spectroscopy, including an NMR self-diffusion experiment. These experiments showed that the surfactants formed several shapes of micelles (spherical, ellipsoidal, and rodlike) at the respective concentrations which were far above their critical micelle concentration.

运用核磁共振一维氢谱和自扩散实验方法研究了聚乙烯乙二醇异辛酚醚(TX-100)、十二烷基苯磺酸钠和十四烷基三甲基溴化铵三种不同类型的表面活性剂在重水溶液中的胶束形状转变,发现它们在临界胶束浓度以上的各自相应浓度都有胶束形状的变化(由球状转变为椭球状或棒状)。

The CFD software STAR-CD is used to simulate the normal operating conditions of cold and hot plenums in China Experimental Fast Reator. Complex 3-dimension model is established by using porous medium method. The temperature and velocity distributions of cold and hot plenums are given. These results are compared with the data of the thermal designs of CEFR which have been completed. Meanwhile, the influence of the buoyancy forces is analyzed.

应用计算软件STAR-CD对中国实验快堆正常运行工况中的额定工况进行了三维数值分析,使用多孔介质模型对屏蔽柱的影响进行了模拟,给出了冷热钠池的三维温度场和流场,与已有热工设计进行了比较,并著重分析了浮升力在数值模拟计算中的影响,为事故工况下的设备动态分析及相应的设备力学分析提供了数据。

The CFD software STAR-CD is used to simulate the normal operating conditions of cold and hot plenums in China Experimental Fast Reator. Complex 3-dimension model is established by using porous medium method. The temperature and velocity distributions of cold and hot plenums are given. These results are compared with the data of the thermal designs of CEFR which have been completed. Meanwhile, the influence of the buoyancy forces is analyzed.

应用计算软件STAR CD对中国实验快堆正常运行工况中的额定工况进行了三维数值分析,使用多孔介质模型对屏蔽柱的影响进行了模拟,给出了冷热钠池的三维温度场和流场,与已有热工设计进行了比较,并着重分析了浮升力在数值模拟计算中的影响,为事故工况下的设备动态分析及相应的设备力学分析提供了数据。

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