三苯胺

Methods Protein in blood and urine was precipitated directly by acetonitrile with acetanilide was used as the internal standard using Agilent Zorbax SB-Aq column (250 mm×4.6 mm, 5 μm). The mixed solvents of water (triethylamine 0.12%, acetic acid 0.12%) and acetonitrile were used as the mobile phase to separate cephalosporins using gradient elution method at 1 mL/min and 254 nm.

以乙酰苯胺为内标，血液和尿液用乙腈直接沉淀蛋白，采用Agilent Zorbax SB-Aq(250 mm×4.6 mm， 5 μm)色谱柱，流动相选用水（含0.12%三乙胺和0.12%乙酸）和乙腈的混合溶剂梯度洗脱，流速1 mL/min，检测波长254 nm。

And then we found that ytterbium trifluoromethethanesulfonate is a powerful catalyst for the reaction of amine and ethyl acetate.

然后研究了三氟甲磺酸镱催化的胺和乙酸乙酯的反应，从而合成了乙酰苯胺类化合物。

The 3-chloro-4-trifluoromethoxy benzonitrile was synthesized from 3-chloro-4-trifluorome- thoxy aniline by diazotization, formaldoximation ,hydrolysis and cyanation.

以3-氯-4-三氟甲氧基苯胺为原料，经重氮化、甲醛肟化、水解和腈化反应得到纯度≥99。

With the catalyst TiO2/SO(superscript 2- subscript 4), 2, 4, N-trinitroanilinoacetic acid was synthesized from chlorobenzene and glycine with yield of 71.6%.

以纳米固体酸TiO2/SO(上标 2-下标 4)为催化剂，氯苯和氨基乙酸为原料直接合成了2，4，N-三硝基苯胺基乙酸，收率为71.6%。

The ratio of snails left water in the complex group was decreased 71.9% than that of nicotinanilide group.

由此表明，3个厂家生产的氯硝柳胺与湖北三利公司生产的烟酰苯胺复配形成的3组氯烟复合物，在浸杀和喷洒灭螺的效果上是一致的。

The synthetic organic chemicals, such as phenol, m cresol, phloroglucinol, phenylamine, 3,5 xylenol, p tertiary butyl phenol, nitrobenzene, tert butanol and chloral were oxidized in supercritical water system.

研究了超临界水氧化系统中合成有机化学品，如酚、间苯三酚、对叔丁基酚、间甲酚、3 ，5-二甲酚、苯胺、硝基苯、叔丁醇、三氯乙醛等的氧化作用。

P-π conjugated polyamic acid was synthesized by the poly-condensation of benzoguanamine and pyromellitic dianhydride under microwave irradiation. Then PAA was grafted with different side-chain containing azobenzol groups through azo coupling reaction.

选取苯代三聚氰胺和均苯四酸二酐为单体进行微波辐射溶液聚合反应，所得的聚酰胺酸与对位取代基不同的苯胺重氮盐偶合接枝，从而合成了一系列新的具有三阶非线性光学活性的侧链型聚合物。

Staining observation on complex mesochondrium of marrow-derived mesenchymal stem cells-TCP: It was found with TB staining that the complex of marrow-derived mesenchymal stem cells-TCP inside the joint cavity obviously had positive staining, which indicated that there were glycosidoprotein base formed.

骨髓基质干细胞-磷酸三钙复合体软骨基质特染观察结果：甲苯胺蓝染色发现，植入关节腔的骨髓基质干细胞-磷酸三钙复合体有明显阳性染色，表明有糖蛋白基质形成。

The Mannich-type addition of O , O'-dialky phosphite to 2-fluorobenzaldehyde and 4-trifluoro- methylaniline was carried out in one pot by means of adopting three kinds of green synthetic methods, microwave irradiation, ionic liquid and free solvent-catalyst condition. According to the results, the synthetic method was optimized without catalyst and solvent at 100 ℃ and 15 min, and it was economic, convenient, high yields, timesaving and environment friendly.

采用微波辐射﹑离子液体和无溶剂无催化剂三种绿色合成方法，分别进行了以亚磷酸酯、邻氟苯甲醛和对三氟甲基苯胺为原料的类Mannich一锅法合成反应研究，经合成筛选，优选出控制反应温度100 ℃、无溶剂和无催化剂加热反应15 min的合成方法，实验结果表明该方法经济、简便、产率高、反应时间短及对环境友好。

Huapai products:pchlorophenol,ochlorophenol,2,4dichlorophenol,2,6dichlorophenol,2,4,5trichlorophenol,2,4,6trichlorophenol,4chloro2benzyl phenol,pbromophenol,2,4,6tribromophenol,1chloro4(1,1dimethyl ethyl) benzene ether,3bromoanisole,mbromofluorobenzene,2tetra hydrofuran,αbromo4chloro acetophenone,αbromo4methoxy acetophenone,4chloro benzophenone,4chloro2methylaniline,n(2hydroxyethyl)ethane diamine; n(2aminoethyl)ethanolamine,2,3dibromopropionyl chloride,4bromo benzene sulphonyl chloride,terephthaloyl chloride,isophthaloyl chloride,nchlorosuccinimide,nbromosuccinimide,pchloranil;tetrachloro1,4benzoquinone,5chloroisatin.

华派公司产品：对氯苯酚，邻氯苯酚，2，4二氯苯酚，2，6二氯苯酚，2，4，5三氯苯酚，2，4，6三氯苯酚，4氯2苄基苯酚，对溴苯酚，2，4，6三溴苯酚，对氯苯基叔丁基醚，间溴苯甲醚，间溴氟苯，α溴甲基四氢呋喃，α溴代4氯苯乙酮，α溴4甲氧基苯乙酮，4氯二苯甲酮，4氯2甲基苯胺，N(2羟乙基)乙二胺， 2，3二溴丙酰氯，对溴苯磺酰氯，对苯二甲酰氯，间苯二甲酰氯，N氯代丁二酰亚胺，N溴代丁二酰亚胺，四氯苯醌，5氯靛红。

I can not make it blossom and suits me

我不能让树为我开花

When temperatures are above approximately 80 °C discolouration of the raceways or rolling elements is a frequent feature.

当温度高于 80 °C 左右时，滚道或滚动元件褪色是很常见的特征。