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The use of LEDbased portable device for the colorimetric determination of triterpenoid alcohol ketones in Alisma orientalis has been established.

建立了利用便携式小型光谱仪测定中药泽泻中三萜醇酮类化合物总量的比色测定方法。

Results① The hemostasis drugs used for these patients were totally 13 kinds, among which adrenobazone, aminocaproic acid, pituitrin, aminomethylbenzoic acid injection rendered the 1st,2nd,3rd and the 4th position repectively.

结果①病例使用止血药共计13种,肾上腺色腙、氨基己酸,垂体后叶素、氨甲苯酸针分居止血药的第一、二、三、四位。

After ethanol extracted hepaticglycogen, it was identified by indic colorific mensuration and quantified with anthrone mensuration. Finally, experimentative design was bringed forward.

采用三氯醋酸沉淀组织蛋白质,乙醇提取肝糖原后,以碘呈色法对其鉴定,再以蒽酮法进行定量,最后提出对相关物质检测的实验设计要求。

The reasons for significant error were studied by adopting TTC chromogenic method, analyzing alcohol extract of natural antimicrobic component's polarity and making sample appropriate diffusion before plate cultivated.

采用氯化三苯四氮唑对指示菌显色、分析天然产物乙醇浸膏中抗菌成分的极性、样品在平板培养前适当扩散等方法,对K-B法检测天然抗菌成分存在显著误差的原因进行了研究。

The existance of vesicles was demonstrated by negatively staining TEM, freeze-fracture TEM, bromphenol blue entrapment, and quasi-elastic lightscattering experiments.

应用电镜(负染色制样和冰冻复型制样)、凝胶色谱、DSC、激光光散射等手段,证实了十一烯酸钠与十烷基三甲基溴化铵的混合溶液,在摩尔组成比α=9∶1--1∶9时经超声皆可制得单室囊泡。

Sanjin Soft Capsulae; HPLC; ELSD; Madecassoside

三金软胶囊;高效液相色谱法;蒸发光散射检测器;羟基积雪草苷

ChamaecyparisIawsoniana ParI and picea sitchensis Carr.wood treated with BTCA:Values of weigh percentgainreached 9.05% and 8.25%.Values of antiswelling efficiencyreached57.2% and 55.45% respectively.Values of moisture excluding efficiencyreached47.95% and 44.89%.Chamaecyparis Iawsoniana ParI and picea sitchensis Carr.wood treatedwith 1,2,3,4-butanetetracarboxylic acid and glycerin:Values of weigh percent gainreached 13.12% and 12.24%.Values ofantiswelling efficiencyreached 61.11% and63.12% re.Values of moisture excluding efficiencyreached 46.91% and 48.93%.Woodsurface colour of Chamaecyparis Iawsoniana ParI and picea sitchensis Carr.were slightlyvaried from red to yellow and from dismal to bright in crosslinking reaction.

处理后美国扁柏和西特克云杉两种木材,分别达到:WPG9.05%和8.25%;ASE57.2%和55.45%;MEE47.95%和44.89%;酯化剂中加入丙三醇,酯化处理美国扁柏和西特克云杉木材,分别达到:WPG为13.12%和12.24%;ASE为61.11%和63.12%;MEE为46.91%和48.93%;在酯化反应中,美国扁柏木材材色由偏红向偏黄、由稍暗向明亮方向有些变化。

It caused aggregation of purple membrane fragments at very low concentration. This effect might be attributed to its positive charges because cationic surfactant DTAB acted the same. On the other hand, melittin seemed to have behavior similar to CHAPS which has a rigid cholane ring,both had little effect on the conformation of retinal chromporphores.In consideration of the two-dimensional crystalline structure of purple membrane,melittin may form a rigid conformation such as α-helix on the surface of the membrane.

通过与三种在结构和电荷上不同的表面活性剂与紫膜的作用相比较,可以年出蜂毒作为带正电荷的分子与同样带正电的表面活性剂DTAB在引起紫膜凝聚方面表现相同;但在对紫膜可见光区的吸收光谱和圆二色谱的影响上却与具有刚性结构的CHAPS相似,表明蜂毒可在紫膜表面以一种刚性较大的构象存在,不能进入膜蛋白流水区的深层。

The molar ratio of sulfate ions to carboxylate ions is determined by conductometric titration method and the molecular weight is tested by high performance gel permeation chromatography. The precision of these two methods is also studied. To improve the detection sensitivity, guanidine hydrochloride is used as the best derivation reagent of 911. A systematic research is done on the optimum derivatization condition of 911 and Guanidine hydrochloride. The M /G ratio of 911 has direct relation to its biological activity.

论文首先对911的基本理化性质进行了系统的分析,以电导滴定法和高效凝胶渗透色谱法分别测定了分子中硫酸根羧酸根的比值和911的分子量,并探讨了两种分析方法的精密度。911分子没有紫外吸收,为提高检测灵敏度,本文采用荧光标记法,通过对三种荧光试剂与几种寡糖和多糖衍生效果的综合比较,最终确定了盐酸胍为最佳衍生试剂,并以911为代表详细探讨了衍生化反应的最优条件。911糖链结构与褐藻胶主链结构类似,以甘露糖醛酸和古罗糖醛酸的嵌段形式存在,分子中M/G比值与911的物理化学性质和生物活性有直接关系。

Xylem: Chinese P.chinensis Bge 49.15mg/g, Atlantic Ocean 46.58mg/g, UCB 55.28mg/g. 3.In certain condition, Gas-chromatograms and Mass spectrum are use to identifie phenol. Pistacia vera L .leave contain pyrocatechol 0.7640mg/g, pyrogallol 0.0580mg/g, gallic acid 1.03024mg/g, catechin 0.1040mg/g and coumaric acid by different pre-treatment methods.

采用不同方法提取阿月浑子叶片酚类物质,气相色谱-质谱法对其进行定性与定量分析,阿月浑子叶片中含有邻苯二酚0.7640mg/g;邻苯三酚0.0580mg/g;没食子酸1.3024mg/g;儿茶素0.1040mg/g,香豆酸;确定了最佳的前处理方法。

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我的第一篇文章为屏幕力量杂志,在对这天是Jackie Chan 正式杂志,是香港actioner Gen X 警察的DVD 回顾,担任主角Nicholas Tse 和丹尼尔吴。

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