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Chapter 3 The imine salt is formed initially by the addition of an organolithium compound to the aromatic nitrile. This type of reaction usually leads to cyclic products.such as triazines.

第三章研究发现有机锂化合物LiCH_2[SiMe(NMe_2)_2]与芳香腈(如苯腈、邻甲基苯腈、间甲基苯腈)反应,可以得到2,4,6-三取代均三嗪,这是一种该类均三嗪的简单有机合成方法。

Methods:According to the principle of random design,the conditions would be consistent with the study of 90 cases of scapulohumeral periarthritis in patients with out-patient ratio of 1:1 were randomly divided into two groups,namely the "three-needle shoulder" with the temperature of acupuncture and traditional dialectical point acupuncture treatment,the treatment group:the "three-needle shoulder" with the warm acupuncture,three-needle shoulder(jianyu,before shoulder,jianzhen points) acupuncture,moxa check each 2cm,each pin of each combustion 2 day 1,10 times as a course of treatment,a total of 2 course of treatment.

根据区组随机化设计原则,将符合研究条件的90例门诊肩关节周围炎患者按1:1比例随机分为两组,分别给予温针灸&肩三针&和针刺&肩三针&治疗,治疗组:采用温针灸&肩三针&:先针刺肩三针,艾柱取每段2cm,每针每次燃烧2段,每天1次,10次为一疗程,共2个疗程。

Tri-cyanurate as a excellent additional retardant was synthesized by using cyanuric chloride_3,tribromophenol as main materials and under the condition of sodium hydroxide,dichloromethane,toluene as solvent respectively.

以三聚氯氰3和三溴苯酚为主要原料,在碱性条件下,分别以二氯甲烷、甲苯作为溶剂,合成了一种性能优良的添加型阻燃剂三三聚氰酸酯。

Also, the type of dispersion of four gasliquid-liquid systems: air-decane-aqueous solution of sodium sulfite and surfactant, airmixture of decane and dodecene-aqueous solution of rhodium complex, ligand, and surfactant, air-mixture of decane, dodecene and tridecyl aldehyde-aqueous solution of rhodium complex, ligand and surfactant, and air-mixture of decane and dodeceneaqueous solution of trisodium salt of tri (m-sulfophenyl) phosphine, and surfactant is determined by electric conductivity.

本文采用电导率测量的方法实验研究了空气—正癸烷—亚硫酸钠和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷、1-十二碳烯和十三醛混合物—铑膦络合物催化剂和十六烷基三甲基溴化铵水溶液、空气—正癸烷和1-十二碳烯混合物—三间磺化苯基膦三钠盐和十六烷基三甲基溴化铵水溶液四个三相体系的液液分散特性。当有机相与水相体积比分别为7/3、1/1和3/7时,前三个体系均形成水包油型分散,并有稳定的乳状液生成。

A new production technology of high-quality trimellitic anhydride with the liquid-phase air-oxidation from 1,2,4-trimethylbenzene was developed.

偏苯三酸酐的生产方法主要有偏三甲苯气相空气氧化法、偏三甲苯液相硝酸氧化法、偏三甲苯液相空气氧化法和间二甲苯甲醛液相空气氧化法。

This thesis consists of two parts. In Chapter 1, we synthesized novel polyimides containing 1,2,4-triazole and triphenylamine groups. In Chapter 2, we synthesized polys in which main chain contains triazole group and side chain was carbazole group or triphenylamine group.

本实验共分两部分:第一章以合成含1,2,4-三氮唑和三苯胺结构的聚醯亚胺;第二章以合成三氮唑为主链,侧链分别含有咔唑与三苯胺之聚醚醯亚胺,并探讨其热性质、光学性质及应用。

The results were as follows:The first, there were significantly differences percent between 0.6μg/mlgroups and other three groups (0.2μg/ml groups, 0.4μg/ml groups and 0.8μg/mlgroups) in 2 hour groups; and there were significantly differences between0.4μg/ml groups and other three groups in 4 hour groups; and there weresignificantly differences between 0.6μg/ml groups and other three groups in 6hour groups; and there were significantly differences between 0.4μg/ml groupsand other three groups in 8 hour groups on the metaphases (P<0.05), in theexperiment of the effect on the mouse 4- cell embryo stage single blastomere ofcolchicine with different concentrations and duration, by x~2 statistical analysis.

实验结果如下:1、在确定秋水仙素不同处理浓度和时间对小鼠4-细胞期胚胎单卵裂球中期分裂相数影响的实验中,经统计分析,阻断培养2小时组中0.6μg/ml浓度组与其他三组差异显著(0.2μg/ml组、0.4μg/ml组和0.8μg/ml组);阻断培养4小时组中0.4μg/ml浓度组与其他三组差异显著;阻断培养6小时组中0.6μg/ml浓度组与其他三组差异显著;阻断培养8小时组中0.4μg/ml浓度组与其他三组差异显著(P<0.05)。

It is separated into three large vertical pilasters; three decorative horizontal band again it is divided into three parts, of which the bottom three concave openings.

它被壁柱纵向分隔为三大块;三条装饰带又将它横向划分为三部分,其中,最下面有三个内凹的门洞。

It was pilasters vertical separation of three large; 3 decorative horizontal band again it is divided into three parts, of which lowermost of three concave openings.

它被壁柱纵向分隔为三大块;三条装饰带又将它横向划分为三部分,其中,最下面有三个内凹的门洞。

Experimental results show that the 3D SPEZBC algorithm has the same rate-distortion performances of three-dimensional embedded zero block coding (3D EZBC) algorithm, obviously outperforms three-dimensional set partitioned embedded block (3D SPECK) algorithm, three-dimensional set partitioning in hierarchical trees(3D SPIHT) algorithm and (AT-3D SPIHT) algorithm, and is slightly better than JPEG2000 multi-component (JPEG2000-MC) algorithm at different bit rate in the compression performances.

实验结果表明,3D SPEZBC算法具有与三维嵌入式零块编码(3D EZBC)算法相同的压缩编码性能,在各比特率下编码性能均明显优于三维集合分裂嵌入式块编码(3D SPECK)、三维等级树集合分裂(3D SPIHT)和非对称三维等级树集合分裂(AT-3D SPIHT)算法,并且略好于多分量JPEG2000编码(JPEG2000-MC)算法。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。

There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。