三烯

The main chemical constituents from dipsacaceae species were triterpenoid saponins,iridoidal glycosides,flavonoids,essential oils,etc.

该科植物主要含三萜皂苷、环烯醚萜苷、黄酮、挥发油等类型的化合物。

Twenty compounds have been isolated and structure-elucidated, ten of which were new compounds including one new skeleton diterpene malloapeltin A, 5 cembrene-type diterpenes, two dolabradane-type diterpenoids, one triterpene ester malloapeltin B and one coumarinolignoid compound 5'-demethyl aquillochin.

其中有10个是新化合物，包括一个新骨架的二萜，五个枯烯类的二萜，两个罗柏烷型的二萜，一个三萜的对苯二甲酸酯和一个香豆素木脂体类化合物。

The formation of charge transfer complex was studied in the first part. The second part includes the synthesis and characterization of the acrylated unsaturated polyester and the kinetic studies on the Ar-UPE/ triethylene divinyl ether (DVE-3) photocuring system, the rheology and properties of film after photocuring. The third part includes the synthesis and characterization of the urethane modified unsaturated polyester and the kinetic studies on the PU-UPE/DVE-3 photocuring system, the rheology and properties of film after photocuring. The fourth part includes the synthesis and characterization of the vinyl ether end capped polyurethane and the kinetic studies on the VE-PU/DVE3 photocuring system, the rheology and properties of film after photocuring.

整个研究工作分为四个部分：一是电荷转移复合物的研究；二是丙烯酰氧基化不饱和聚酯的合成，表征，Ar-UPE/二缩乙二醇二乙烯基醚（DVE-3）体系光固化动力学研究以及Ar-UPE/DVE-3体系流变性能和光固化后涂膜综合性能的研究；三是氨酯改性的不饱和聚酯的合成，表征，PU-UPE/DVE-3体系光固化动力学研究以及该体系光固化后涂膜综合性能的研究；四是乙烯基醚封端的聚氨酯的合成，表征，VE-PU/马来酸二甲酯体系光固化动力学研究以及VE-PU/DMA体系流变性能和光固化后涂膜综合性能的研究。

The process industrial synthsis of tert-dodecyl mercaptan from dodecylene and hydrogen sulfide with aluminium trichloride as catalyst was introduced, which consists of four units including the preparation of catalyst, purification of raw dodecylene, additive reaction and separation of reaction product.

介绍了以无水三氯化铝络合物为催化剂，十二烯和硫化氢直接加成法生产叔十二烷基硫醇的工业试验工艺。

In Granards' reactionof fluorinated β-ketophosphonium salts we found differentGranard reagents give different reaction mechanisms andPhMgBr realized the enolate reaction of fluorinatedβ-keto-phosphonium salts.

在研究含氟β-酮基鏻盐的β位亲核加成反应中，我们利用含氟α-烷氧基-β-酮基鏻盐与有机锂试剂的亲核加成反应一锅法高度立体选择性地合成了E式或Z式三氟甲基的烯醚类化合物。

Its mainly produced by cumene peroxidation process, which requires three steps of reactions and is limited by the market requirement of equimolar byproduct acetone.

目前工业合成苯酚的最主要方法是异丙苯法，此法经过三个步骤：以苯和丙烯为原料，在酸催化下生成异丙苯，异丙苯经氧化生成过氧化氢异丙苯，再用硫酸或树脂分解，同时得到等摩尔的苯酚和丙酮。

The leftover from bamboo processing was comminuted into bamboo fine powder, which was surface-treaded with a coupling agent of ethenyl tri (β-methoxyethoxy) silane; and then in the presence of initiator dicumyl peroxide, the powder was compounded with styrene-isoprene block copolymer/bromobutyl rubber blend to prepare a crosslinked vibration-absorbing rubber composite material.

将竹加工的边角料粉碎并用乙烯基三硅烷偶联剂处理，再与苯乙烯－异戊二烯嵌段共聚物和溴化丁基橡胶的共混物进行复合，在过氧化二异丙苯引发剂的作用下制得交联型橡胶吸振复合材料。

This paperindicated that it was good for condensation reaction when benzene-ring bearingelectron-attaching groups. It also showed that and the 6-hydroxyl group could bereacted with acyl halide, haloid ether and halo alkene, but not with halo alkane. It wasnot only the first time to find that the reaction product of D-mannitol and aromaticaldehyde is tri-condensation derivatives, but also the first time to obtain thep-phthaldehyde-sorbitol derivatives containing eight hydroxyl groups.

研究发现：苯环上有吸电子基团时对缩合反应有利；多元醇缩醛衍生物6-羟基除与酰氯反应外，也能和卤代酸酯、溴代烯反应，但不与卤代烷反应；首次发现D-甘露醇与醛反应主要得到三缩合物；首次合成了含有8个羟基的对苯二甲醛和山梨醇的缩合物。

Objective: In order to provide sensitive and reliable technique for the study of the relationship between enviromental estrogens and diseases, analytical methods for three kinds of representative environmental estrogens such as mycotoxins (zearalenone and its metabolites, aflatoxin B_1 and ochratoxin A), persistent pesticide pollutants (hexachlorocyclohexane and dichlorodiphenyltrichloroethane) and industrial chemicals (bisphenol A and 4-nonylphenol) with chromatography were to develop.

目的：选择三种有代表性的环境雌激素：真菌类毒素(玉米赤霉烯酮及其代谢物及赭曲霉毒素A、黄曲霉毒素B_1)、农药类持久性污染物(666、DDT)和化工原料类雌激素为对象，分别研究它们的检测方法，为监控环境激素和研究它们与疾病之间关系提供灵敏、可靠的分析方法和实验依据。

The alternative method of O-demethylation,methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

方法在以蒂巴因为原料，经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中，分别采用甲磺酸/DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐