三烯

Result:Eight compounds were elucidated as β amyrin palmitate, taraxastery acetate, luteolin 7 O α L rhamanopyranosyl (1→2)β D glucopyranoside,luteolin 7 O β D glucopyranoside, triacontanic acid,β sitosterol, stigmasterol and stigmast 7 en 3β ol.

结果 ：从全草中分离得到 5个化合物，β香树脂醇棕榈酸酯，蒲公英醇乙酸酯，木樨草素 7 O α L 鼠李糖基(1→ 2 )β D 葡萄糖苷，木樨草素 7 O β D 葡萄糖苷，三十碳酸；1个混合物，β谷甾醇、豆甾醇、豆甾 7 烯 3β醇。

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下：首先，以磺胺异噁唑和磺胺二甲嘧啶为模板，分别以4-乙烯基吡啶，甲基丙烯酸，丙烯酰胺为功能单体，以二甲基丙烯酸乙二醇酯为交联剂，偶氮二异丁腈为引发剂，采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

The synthesis of terpene hydroquinone resin with turpentine and hydroguinone was studied, with AlCl 3 as catalyst.

摘 要：研究了以无水三氯化铝为催化剂，松节油与对苯二酚聚合反应制备萜烯对苯二酚树脂的情况。

Methods Naloxone was synthesized starting from oxidation of thebaine, followed by hydrogenation, acylation, cyanidation, O-demethylation, hydrolyzation and N-allylation. The alternative method of O-demethylation, methane sulfonic acid/DL-methionine and hydrobromic acid were investigated.

在以蒂巴因为原料，经氧化、氢化、酰化、氰化、去氧甲基、水解、N-烯丙基化得到纳洛酮的合成路线中，分别采用甲磺酸／DL-甲硫氨酸和氢溴酸代替三溴化硼进行去氧甲基化和后续水解反应。

The thermolysis of the isomerized products derived from terpadiene-coordinated carbonyl iron complexes afforded the same kind of the thermolytic products.

以萜二烯三羰基铁络合物衍生出来的铁卡宾络合物及其异构化产物，热解以后都得到了同一类型的络合物。

Extensive experimentation revealed several issues, along with several corresponding solutions:(1) given that lithium metal dissolves slowly in liquid ammonia, considerable time was required to generate the dissolved metal solution (ca. 1 h);(2) the t -BuOH must be freshly distilled prior to use 21 to diminish the formation of ketone 19 (Figure 2);(3) efficient capture of the lithium enolate ( 11 ) required the use of freshly distilled TMSCl and Et 3 N; and (4) the presence of residual thiophenol upon workup was found to inhibit the subsequent Sc 3 -promoted hydroxymethylation.

大量实验揭示若干问题，随着几个对策 1鉴于锂金属溶化慢慢液氨、需要相当多的时间创造了金属溶液溶解(约占1小时)；(2) T恤使操作必须事先用新鲜蒸馏水形成酮减少2119(图2)；有效捕获的锂烯醇(11)使用新鲜蒸馏水需氯和ET三氮；含有残余硫workup经发现抑制随后推选3-羟甲晋升。

Drug therapy is the treatment of fungal corneal ulcer as an effective way to more broad-spectrum antifungal triazole drugs vinyl with local, systemic and effective combination therapy.

药物治疗是治疗真菌性角膜溃疡的一种有效方法，广谱抗真菌药物多烯类与三唑类药物局部、全身联合治疗有效。

It was shown from the results that emulsifier TP-Ⅴ which was prepared by PEG 4000 reacted with TME, in the molar ratio of TME to PEG 2:1, at about 110℃ for 1 h, catalyzed by boron trifluoride diethyl etherate, has a very good emulsifying impact for TME. Particle size distribution of the emulsion was homo-geneous and viscosity of the emulsion was small.

实验结果表明，以M相对适中的PEG4000与TME按物质的量比2： 1、在催化剂三氟化硼乙醚作用下、110℃左右反应1h合成的乳化剂TP-Ⅴ，对萜烯基环氧树脂具有很好的乳化效果，制备的乳液粒子粒径均一度较高，乳液表观黏度较小。

D. of the catalyst increased, i. e. the acid volume of the catalyst increased, the conversion for isobutene and the selectivity for trimer increased also, while the selectivity for dimer decreased, and the selectivity for tetramer was almost unchanged.

D。增加时，即催化剂的酸量增加时，异丁烯的转化率和三聚物的选择性也增加，但二聚物的选择性降低，四聚物的选择性则几乎没有变化。

The oligomerization of isoprene with titanium tetrachloride as catalyst and alkylaluminium chlorides as promotor was studied, and especially the effects of the reaction conditions on the synthetic activity and selectivity of dimer and trimer were investigated in detail.

研究了以四氯化钛为主催化剂，以烷基铝为助催化剂催化异戊二烯的低聚反应，详细考察了各种反应条件对催化合成二聚体及三聚体的活性和选择性的影响。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐