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PVC resin, PTFE resin, fumaric acid, anthraquinone, nitroanthraquinone, paraaminophenol, melamine, cyanuric acid, sulfanilic acid, chemical inhibitor 168, azoic coupling component As, stearate, aniline, nitroaniline, pentaerythritol, chlorcosane, sodium calcium, triethylene diamine, sodium benzene sulphinate, m-phthalic acid, thiourea, aniline black dyestuffs, acid dyestuff, etc.

聚氯乙烯树脂、聚四氟乙烯树脂、反丁烯二酸、蒽醌、硝基蒽醌、对氨基苯酚、三聚氰胺、氰尿酸、对氨基苯磺酸、抗氧剂168、色酚As、硬脂酸盐、苯胺、硝基苯胺、双季戊四醇、氯???腊、甲酸钙、三乙烯二胺、苯亚磺酸钠、间苯二甲酸、二甲酯五磺酸钠、硫脲、油溶性苯胺黑染料、酸性黑染料等有机化工原料和中间体。

Compared with TEA,TiBA activated system produced more blocky copolymer,but the blockiness of its block fraction is lower.

与三乙基铝相比,三异丁基铝为助催化剂得到的不溶级份含量及丙烯含量都较高,但其嵌段性却较低。

Corporation Shanghai Jiao Tong University's latest research results, primarily engaged in 3 - butene -1 - alcohol, 1,2,4 - Tromethamine, six three phosphazene ring chlorine production and marketing.

公司依托上海交通大学的最新科研成果,主要从事3-丁烯-1-醇,1,2,4-丁三醇,六氯环三磷腈的生产销售。

On the basis of aerobic oxidation ofβ-ionone catalyzed by supported catalysts/butyraldehyde system,a series of cycloolefines such as cyclohexene,β-methylionone,α-ionone,andα-pinene were oxidized under the general conditions to give corresponding epoxides and allylic oxides.

将三种催化体系CMPS-Co_2/正丁醛、Co_2/SiIm-正丁醛、MoO_2_2/SiIm-正丁醛推广应用到不同环烯烃催化氧化反应,虽然各反应底物之间的转化率和氧化选择性变化很大,但对三种催化体系横向比较而言,其催化氧化情况相当。

For developing an immunoassay for multiple residues of pyrethroid pesticides, the hapten N-2- carbanmoyl-(3"-phenoxyphenyl) methyl 3-(2"-Cldoro-3",3",3"-trifluoropropenyl)-2, 2-dimethylcyclopropane- carboxylate was synthesized from cyanohydrin and 3-(2"-Chloro-3",3",3- trifluoropropenyl)-2, 2-dimethylcyclopropanecarboxylic acid via hydrolysis and esterification. The synthesis of the hapten was foundation of preparaing anti- cyhalothrin polyclonal antibodies.

为了制备对单一拟除虫菊酯高特异性的抗体,以菊酸和氰醇为起始原料,通过水解、酯化反应合成了半抗原N-2-氨甲酰-(3-苯氧基苄基)甲基-3-(2-氯-3,3,3-三氟丙烯基)-2,2-二甲基环丙烷羧酸酯,为进一步制备抗三氟氰菊酯的特异性抗体奠定基础。

They cationic monomer Acryloyloxyethyl ethyl trimethyl ammonium chloride and resource-rich, low price, low values of weathering burning coal as its main raw material, aqueous dispersion polymerization methods, through the weathered coal / cationic monomer in-situ polymerization in the international arena for the first time prepared by a high efficiency oil-bearing wastewater treatment agent; use of oil-field wastewater treatment, the waste slurry as raw material, has developed the world's first CWS dispersants and oil fields of the "three mining" using profile control plugging agent, in order to The high value of solid waste has opened up new avenues of applications; integration of related technologies, and open up for the oil field wastewater treatment, an annual output of 300 tons of sets of processes and devices for the first time realized the slop oil and drilling fluid back row of the industrialization of treatment .

他们以阳离子单体丙烯酰氧乙基三甲基氯化铵与资源丰富、价格低廉、燃烧值低的风化煤为主要原料,采用水介质分散聚合方法,通过风化煤/阳离子单体原位聚合技术,在国际上首次制备出高效含油废水处理剂;采用油田废水处理后的废弃物泥浆为原料,在国际上率先开发出水煤浆分散剂和油田"三采"用调剖堵水剂,为固体废弃物的高值化应用开辟了新途径;集成相关技术,开拓出针对油田废水处理、年产300吨的成套工艺和装置,首次实现了油田污油水和钻井返排液的工业化处理。

The comparisons of biochemistry between OP and OR rats The differences between OP and OR rats included not only body weight, but lipids metabolism and insulin sensitivity as well, characterized with insulin resistance, increasing in serum free fatty acids and ketone body, and hepatic TC and TG in OP rats. However, no significant differences were observed in serum TG, TC, LDL, HDL and fasting glucose between OP and OR rats.⑶Comparisons of metabolites in serum, urine and liver tissue between OP and OR rats①There were significant differences in amino acids concentration between OP and OR rats,especially in liver tissue, such as high concentrations in ketogenic and glucogenic amino acids in OP rats, suggesting differences in amino acids metabolism;② The different metabolites between OP and OR rats included increasing of various saturated fatty acids and decreasing of polyunsaturated fatty acids in OP rats;③The urinary metabolites analysis indicated that different structure or metabolism of gut microflora might exist between the two phenotypes, which probably influenced the regulation of body weight gain;④The end-products of catecholamines in urine and intermediates of krebs cycle in serum in OP rats were all up-regulated, suggesting that the activity of sympatheic nervous system and energy metabolism was higher in OP rats than OR rats.

胰岛素耐受实验和胰岛素敏感指数表明OP动物的胰岛素敏感性较OR动物下降,而OP大鼠血清中游离脂肪酸、酮体、肝脏总胆固醇和甘油三酯水平显著升高;但是,OP与OR大鼠血清中总胆固醇、甘油三酯、低密度脂蛋白、高密度脂蛋白和空腹血糖等的水平并无显著性差异;⑶肥胖易感与肥胖抵抗大鼠血清、尿液和肝脏组织提取物中代谢物的比较研究表明:①OP与OR大鼠的血清、尿液和肝组织提取物中多种氨基酸的含量存在显著差异,并以肝组织中的差异氨基酸数量为最多,包括各种生酮和生糖氨基酸水平在OP组的升高,说明氨基酸代谢的差异是两种体重表型大鼠之间存在的重要差异特征之一;②OP与OR动物肝脏和血清差异代谢物中包含多种饱和长链脂肪酸的升高如十四烷酸、十六烷酸、硬脂酸等和多不饱和脂肪酸的下降如亚油酸和花生四烯酸,说明两种体重表型动物的肝脏脂肪酸代谢存在明显差异;③长期高脂饮食喂养后,动物的尿液代谢物分析表明OP与OR动物体内的肠道菌群结构存在差异,这些菌群上的差别可能在动物体重增长的调节上产生影响;④与OR动物相比,OP动物尿液代谢物中儿茶酚胺类递质的代谢终产物如高香草酸、扁桃酸和4-羟基苯乙酸明显升高。

In this paper, the studies on the preparation of high pure mesitylene usingMTBE tail gas are made in both experimental and theoretical, different factorsaffecting the alkylation reaction to produce mesitylene by MTBE tail gas areinvestigated, the optimal condition of reaction is defined and the alkylationreaction kinetics of different components are studied, moreover, the comparisonbetween C4 raffinate oil and isobutene used for alkylation agent is made too.

本文对MTBE尾气烷基化法制备高纯度均三甲苯过程进行了实验研究和理论分析,确定了不同因素对烷基化反应的影响,得到了MTBE尾气制备均三甲苯的最佳反应条件,并对不同组分的烷基化反应动力学进行了研究。此外,对乙烯C4抽余油和异丁烯做为烷化剂的实验结果进行了分析和比较。

It provides a route tothe compounds which contains three functional groups, two carbon-nitrogentriple bonds and one carbon-carbon double bond. In water, metallic indiumpromotes carbon-sulfur bond coupling reaction of aromatic sulfonyl chloride withsuitable organic halides to afford sulfones. In the last chapter, metallic tin mediated allylation of aldimines with allylbromide was revealed.

第三章,我们研究了在水相介质中金属铟促进的烯丙基溴对1,1-二氰基-2-芳基乙烯的Michael加成反应,生成一个含碳碳双键和二个碳氮叁键的三官能团化合物,另外,金属铟在水介质中还可以促进芳基磺酰氯与卤代烃发生碳硫键的偶联,生成砜。

During the manufacturing of the critical intermediate cephalosporin nucleus --7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt, first the feasibility of the one-pot synthetic route of open loop, closed loop and ozonization when chlorine is passed over is qualified by experiments. Then the critical factors that will influence this reaction are studied as follows: the mol ratio of triphenyl phosphite and Diphenylmethyl 3-hydroxy-7-phenylacetaminoceph-3-em-4-carboxylate-l-oxide is four to one; the quantity of the stablizer should be at least more than two to one. The temperature of the system must be 25℃ when chlorine is passed over so that the hydrochloride can be precipitated to obtain cephalosporin nucleus of cefaclor--7-amino-3-chloro-cephalosporanic acid diphenylmethyl ester hydrochloride salt.

在制备关键中间体头孢母核7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐时,先通过实验验证把开环、闭环、臭氧化三步在通入氯气时并为一锅煮的合成路线的可行性之外,又研究了影响该反应的几个重要因素:亚磷酸三苯酯与3-羟基-7-头孢烷-5-亚砜-2-甲酸二苯甲酯的摩尔比为4:1;稳定剂2-甲基-2-丁烯的用量至少大于2:1,通入氯化氢气体时体系温度在25℃时盐酸盐则能够顺利析出,获得头孢克洛的头孢母核—7-氨基-3-氯头孢烷酸二苯甲酯盐酸盐。

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