三烯

When the tree changes from health to weak, the main terpene compounds changed, such as the amount of 3-carene, isolimonene,β-pinene, 4-carene were significantly enhanced, and santolina triene,α-fenchene,β-myrcene,β-phellandrene were declined. It will provide a basis for Monochamus urussovi Fischer to select suitable parasitic Picea jezoensis.

鱼鳞云杉树势由健康向衰弱转变时，主要烯萜类化合物含量发生变化，3-蒈烯、异柠檬烯、β-蒎烯、4-蒈烯、α-蒎烯等含量显著上升，而神圣亚麻三烯、α-葑烯、β-月桂烯、β-水芹烯等含量下降，这些烯萜类化合物的变化，为云杉大黑天牛定位选择适宜寄生的鱼鳞云杉提供了依据。

The results showed that there are 42 kinds of matters in health trunk, among which, the biggest relative mass fraction was santolina triene (16.04%), the second was α-fenchee (14.24%), and 43 kinds of matters were found from damaged trunk, the highest was β-pinene (18.07%), the second was α-pinene (12.39%).

结果表明：健康鱼鳞云杉干部挥发性物质共42种成分，其中相对质量分数最大的是神圣亚麻三烯(16.04%)，其次是α-葑烯(14.24%)；被害鱼鳞云杉干部挥发性物质共43种，其中相对质量分数最大的成分是β-蒎烯(18.07%)，其次是α-蒎烯(12.39%)。

The results showed that the density of glandular trichome of mature leaves was lowest in lower leaves, the second in cutter leaves, and the highest was found in upper leaves.α-Duvatriene-4-ol,β-Duvatriene-4-ol,α-Duvatriene-4,6-diol and β-Duvatriene-4,6-diol were higher in cutter leaves than that in lower leaves by 282%, 240%, 48% and 80% respectively, while those in upper leaves were higher than that in lower leaves by 991%, 687%, 74% and 129%, respectively.

结果表明：不同部位成熟烟叶腺毛密度表现为下部＜中部＜上部；中部烟叶分泌物中的α-西柏三烯-4-醇、β-西柏三烯-4-醇、α-西柏三烯-4，6-二醇、β-西柏三烯-4，6-二醇的含量分别比下部烟叶增加了282%、240%、48%、80%，上部烟叶的上述四种分泌物的含量分别比下部烟叶增加了991%、687%、74%和129%。

Second, using DBU as the base for enolization of propargylic esters of unsaturated acids 18e-k, we developed a tandem Ireland-Claisen rearrangement /isomerization reactions. It has been shown that the reaction sequence affords triene molecules 42a-b and 43a-b in moderated to high yields. Interestingly, with allyl hexa-3,5-dienoates 18i-j as the substrate, the rearranged products underwent further aromatization to give uniquely substituted benzyl acids 44a-b.

其次，以含有活泼质子的烯酸炔丙酯18e-k为底物，在DBU为烯醇化碱、TMSCl为硅试剂的条件下，底物18e-h发生了Ireland-Claisen重排/异构化串联反应，得到完全共轭的三烯类化合物42a-b及43a-b；而以己二烯酸炔丙基酯18i-j为底物时，重排/异构化后的产物进一步发生电环化等反应最终得到芳构化产物——取代苯甲酸类化合物44a-b。

The separation of tocopherols and tocotrienols by using the method of adsorption chromatography on silica and on silica impregnated with silver nitrate have been discussed. Satisfactory separation could be obtained with argentation column chromatography by eluting batchwise with n-hexane containing increasing amounts of diethyl ether. More than 90% of vitamin E amount in eluate was tocotrienols.

以乙醚正己烷混合溶液为淋洗液，探讨了硅胶柱层析和硝酸银硅胶柱层析分离生育三烯酚和生育酚的效果，结果表明：通过改变淋洗液中乙醚含量可以将生育酚和生育三烯酚大部分分离：硝酸银硅胶柱层析分离生育三烯酚和生育酚的效果明显高于硅胶柱层析，其洗脱液中生育三烯酚可占V〓总量的90％以上，最高达98.47％。

ConclusionThe main components of liposoluble components are D-Limonene,-3,7-dimethyl-1,3,6-Octatriene,-2,6-dimethyl-2,4,6-Octatriene, Caryophyllene, 2,6-dimethyl-6-(4-methyl-3-pentenyl)-Bicyclo［3.1.1］hept-2-ene, alpha-Farnesene, and-2,6,10,15,19,23-hexamethyl-2,6,10,14,18,22-Tetracosahexaene.

结论蹄叶橐吾的脂溶性成分主要为D-柠檬烯（2.98%）、-3，7-二甲基-1，3，6-辛三烯（15.07%）、-2，6-二甲基-2，4，6-辛三烯（3.61%）、石竹烯（3.62%）、2，6-二甲基-6-(4-甲基-3-戊烯)-二环［3.1.1］庚-2-烯（6.20%）、α-法呢烯（4.09%）、反式角鲨烯（26.91%）等。

The 26 terpenoids in the essential oil extracted from the leaves of Phoebe faberi have been identified by GC-MS technique, such as-S--3,7,11-trimethyl-1,6,10-dodecatrien-3-ol (39.34%),β-caryophyllene (29.18%),-zingiberene (5.16%) and caryophyllene oxide (4.21%).

利用GC-MS联用技术从竹叶楠叶挥发油中鉴定了26个萜类化合物，如---3，7，11-三甲基-1，6，10-十二碳三烯-3-醇（相对含量39.34%）、β-丁香烯（29.18%）、姜烯（5.16%）和氧化丁香烯（4.21%）。

The searching result indicated that many components such as 2-Heptenal,-, Hexadecanal, Octadecanal, Megastigma-4, 6, 8-triene and Megastig-matrienone were identified the first time in studies of aroma components of Chaenomeles fruits.

检索结果表明，试验检测出的-2-庚烯醛、十六醛、十八醛、甲酸叶醇酯、辛酸环己酯、4，6，8-巨豆三烯、巨豆三烯酮等多种化合物，在木瓜果实香气成分研究中尚属首次发现。

Forbesii, monoterpenes and sesquiterpenes account for 41.30% and 32.65%, respectively, in which (1R)-α-pinene (3.98%), sabinene (2.51%),(1S)-β-pinene (5.78%), m-cymene (4.05%), limonene (3.55%), 3, 7-dimethyl-1, 3, 7-octatriene (3.98%),γ-terpinene (8.70%), anisole (1.78%) and (1S)-endo-bornyl acetate (2.62%) as the monoterpenes and its derivatives, and-β-elemene (1.17%),α-bulnesene (1.40%),-β-bisabolene (1.21%),-elemol (1.42%), guaiol (1.14%), dehydroxyisocalamendiol (1.13%),-aristolene (1.99%), bulnesol (9.48%),γ-eudesmol (1.77%), guai-1(10)-en-11-ol (1.12%) and α-bisabolol (5.35 %) as the sesquiterpenes and its derivatives are the main components.

1R-α-蒎烯(3·98 %)、桧烯(2·51 %)、(1S)-β-蒎烯(5·78 %)、m-月桂烯(4·05 %)、柠檬烯(3·55 %)、3，7-二甲基-1，3，7-庚三烯(3·98 %)、γ-萜品烯(8·70 %)、茴香醚(1·78 %)和(1S)-桥环醋酸冰片酯(2·62 %)为单萜类化合物及其衍生物中的主要成分；-β-榄香烯(1·17 %)、异愈创木烯(1·40 %)、-β-没药烯(1·21 %)、-榄香醇(1·42 %)、愈创木醇(1·14 %)、去羟基异菖蒲二醇(1·13 %)、-土青木香烯(1·99 %)、异愈创木醇(9·48 %)、γ-桉醇(1·77 %)、愈创木-1(10)-烯-11-醇(1·12 %)和α-没药醇(5·35 %)为倍半萜类化合物及其衍生物中的主要成分。

Result 16 kinds of fatty acids were separated from Anak chicken muscle and identified. Among them, 7 kinds fatty acids, including lauric acid, myristic acid, pen-tadecanoic acid, palmitic acid, margaric acid, stearic acid and eicosanoic acid, were saturated fatty acids and its content accounted for 38.55% of the total fatty acids; 9 kinds fatty acids, including 11-teteadecenoic acid, 9-hexadecenoic acid, 9-vaccenic acid, 9,12-octadecadienoic acid, 6,9,12-octadeca-trienoic acid, 11-eicosenoic acid, 10, l3-eicosenoic acid, 7,10, 13-eicosatriennoic acid and 5,8,11,14-arachidonic acid, were unsaturated fatty acids, and its content accounted for 61.45% of the total fatty acids.

结果］安卡鸡肌肉中共分离和鉴定出16种脂肪酸，其中饱和脂肪酸7种，包括月桂酸、豆蔻酸、十五烷酸、棕榈酸、十七烷酸、硬脂酸和花生酸，其含量占总脂肪酸的38.55%；不饱和脂肪酸9种，包括11-十四碳烯酸、9-十六碳烯酸、9-十八碳烯酸、9，12-十八碳二烯酸、6，9，12-十八碳三烯酸、11-二十碳烯酸、10，13-二十碳二烯酸、7，10，13-二十碳三烯酸以及5，8，11，14-二十碳四烯酸，共含量占总脂肪酸的61.45%。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。