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The results indicate that the precipitation rate of phosphoric acid is larger than 99% under the conditions of 2530 ℃, the mole ratio of trimeric cyanamide to phosphoric acid 21, two-step precipitation by trimeric cyanamide divided into two portions and separately stirring 60 min.

研究结果表明:在25~30 ℃、三聚氰胺与磷酸摩尔比为21、三聚氰胺分成两份进行两步沉淀、各搅拌60 min为三聚氰胺沉淀磷酸的最佳条件,在此条件下磷酸沉淀率大于99%;在磷酸三聚氰胺沉淀中夹带的氯化钙在固液质量比15、温度40 ℃和搅拌60 min下用水反复洗涤3次后可被完全去除;再将净化后的磷酸三聚氰胺与氨水反应,制得了符合GB 10205—2001标准的磷酸一铵和磷酸二铵产品。

The battle once begun, its very various changes,--the resistance of Hougomont; the tenacity of La Haie-Sainte; the killing of Bauduin; the disabling of Foy; the unexpected wall against which Soye's brigade was shattered; Guilleminot's fatal heedlessness when he had neither petard nor powder sacks; the miring of the batteries; the fifteen unescorted pieces overwhelmed in a hollow way by Uxbridge; the small effect of the bombs falling in the English lines, and there embedding themselves in the rain-soaked soil, and only succeeding in producing volcanoes of mud, so that the canister was turned into a splash; the uselessness of Pire's demonstration on Braine-l'Alleud; all that cavalry, fifteen squadrons, almost exterminated; the right wing of the English badly alarmed, the left wing badly cut into; Ney's strange mistake in massing, instead of echelonning the four divisions of the first corps; men delivered over to grape-shot, arranged in ranks twenty-seven deep and with a frontage of two hundred; the frightful holes made in these masses by the cannon-balls; attacking columns disorganized; the side-battery suddenly unmasked on their flank; Bourgeois, Donzelot, and Durutte compromised; Quiot repulsed; Lieutenant Vieux, that Hercules graduated at the Polytechnic School, wounded at the moment when he was beating in with an axe the door of La Haie-Sainte under the downright fire of the English barricade which barred the angle of the road from Genappe to Brussels; Marcognet's division caught between the infantry and the cavalry, shot down at the very muzzle of the guns amid the grain by Best and Pack, put to the sword by Ponsonby; his battery of seven pieces spiked; the Prince of Saxe-Weimar holding and guarding, in spite of the Comte d'Erlon, both Frischemont and Smohain; the flag of the 105th taken, the flag of the 45th captured; that black Prussian hussar stopped by runners of the flying column of three hundred light cavalry on the scout between Wavre and Plancenoit; the alarming things that had been said by prisoners; Grouchy's delay; fifteen hundred men killed in the orchard of Hougomont in less than an hour; eighteen hundred men overthrown in a still shorter time about La Haie-Sainte,--all these stormy incidents passing like the clouds of battle before Napoleon, had hardly troubled his gaze and had not overshadowed that face of imperial certainty.

交锋以后,战争的非常复杂惊险的变化,乌古蒙的阻力,圣拉埃的顽抗,博丹的阵亡,富瓦战斗能力的丧失,使索亚旅部受到创伤的那道意外的墙,无弹无药的吉埃米诺的那种见死不退的顽强,炮队的陷入泥淖,被阿克斯布里吉击溃在一条凹路里的那十五尊无人护卫的炮,炸弹落入英军防线效果不大,土被雨水浸透了,炸弹陷入,只能喷出一些泥土,以致开花弹全变成了烂泥泡,比雷在布兰拉勒出击无功,十五营骑兵几乎全部覆没,英军右翼应战的镇静,左翼防守的周密,内伊不把第一军的四师人散开,反把他们聚拢的那种奇怪的误会,每排二百人,前后连接二十七排,许多那样的队形齐头并进去和开花弹对抗,炮弹对那些密集队伍的骇人的射击,失去连络的先锋队,从侧面进攻的炮队突然受到拦腰的袭击,布尔热瓦、东泽洛和迪吕特被围困,吉奥被击退,来自综合工科学校的大力士维安中尉,冒着英军防守热纳普到布鲁塞尔那条路转角处的炮火,在抡起板斧去砍圣拉埃大门时受了伤,马科涅师被困在步兵和骑兵的夹击中,在麦田里受到了贝司特和派克的劈面射击和庞森比的砍斫,他炮队的七尊炮的火眼全被钉塞,戴尔隆伯爵夺不下萨克森-魏玛亲王防守的弗里谢蒙和斯莫安,第一○五联队的军旗被夺,第四十五联队的军旗被夺,那个普鲁士黑轻骑军士被三百名在瓦弗和普朗尚努瓦一带策应的狙击队所获,那俘虏所说的种种悚听的危言,格鲁希的迟迟不来,一下便倒在圣拉埃周围的那一千八百人,比在乌古蒙果园中不到一个钟头便被杀尽的那一千五百人死得更快,凡此种种迅雷疾风似的意外,有如阵阵战云,在拿破仑的眼前掠过,几乎不曾扰乱他的视线,他那副极度自信的龙颜,绝不因这些变幻而稍露忧色。

The effects of benzene, triethylamine, diethylamine and ethylene diamine on the shape, yield, N-dopping content and water-adsorption content of CN were discussed. CN materials with moderate N/C ratio (0.15) and high yield 2.2 g(gcat^(-1) were synthesized using diethylamine as the raw material.

比较了苯、三乙胺、二乙胺、乙二胺四种原料对合成CN形貌、产率、掺氮量和吸水率的影响;以二乙胺为原料合成出适中的氮碳比(N/C原子比为0.15)和较高产率2.2 g(gcat^(-1)的竹节状CN材料。

RESULTS: All aromatic anesthetics inhibited I at a holding potential which produce half-maximal current V(1/2; inhibition was modest with 1,3,5-trifluorobenzene (8%+/- 2%), pentafluorobenzene (13%+/- 2%), and hexafluorobenzene (13%+/- 2%), but greater with benzene (37%+/- 2%), fluorobenzene (39%+/- 2%), 1,2-difluorobenzene (48%+/- 2%), 1,4-difluorobenzene (31 +/- 3%), and 1,2,4-trifluorobenzene (33%+/- 1%).

结果:在最高电流的一半的控制电压下所有芳香族麻醉药都阻断钠电流;均苯三酚(8%+/- 2%)、戊苯(13%+/- 2%)、戌苯(13%+/- 2%)的抑制是适度的比苯(37%+/- 2%)、氟苯(39%+/- 2%),1.2-二氟二苯(48%+/- 2%),1,4-二氟二苯(31 +/- 3%),和1,2,4三氟苯(33%+/- 1%)明显。

In order to achieve a rapid and accurate selection for extractive distillation solvent, and to acquire 1,2,3-trimethylbenzene with high purity from solvent oil via extractive distillation, the UNIFAC model was used to calculate the relative volatility of 1,2,3-trimethylbenzene to indane (the mass ratio of 1,2,3-trimethylbenzene to indane is 4∶1) in five different solvents, acetophenone, di-2-octylhexyl phthalate, glycol, dimethyl sulfoxide,sulfolane at 17.47 kPa.

为了快速准确地选择萃取精馏溶剂,由190#溶剂油萃取精馏获取高纯度连三甲苯,运用UNIFAC模型,计算了质量比为4∶1的连三甲苯-茚满体系在苯乙酮、乙二醇、邻苯二甲酸二辛酯、二甲基亚砜和环丁砜5种溶剂中在17.47 kPa下的相对挥发度。

By use of titration analysis, the thesis investigated various factors such as isocyanate, PE molecular weight, reacting substance molecular ratio, reacting temperature and time etc. influencing upon prepolymerization step. It was found that 2, 4-tolulene diisocyanate and 4, 4'diphenylmethane diisocyanate is more rapidly reacted with PE600 than HDI. With PE molecular weight increasing, the reacting temperature or time should be raised or extended relevantly. Thus PE2000+2HDI pre-polymerization should be better carried out under some catalyst, for example, Triethylene diamine , Dibutyltin dilaurate and Tin octoate were used.

首先采用滴定分析方法对WRPU预聚反应的影响因素进行了研究:芳香族二异氰酸酯TDI、MDI比脂肪族二异氰酸酯HDI反应活性高,其中TDI在反应初始阶段的反应速率比MDI快,不过随着反应的进行,MDI比TDI反应速率加快,这主要是因为TDI分子中的两个-NCO反应活性差异大所致;二元醇分子量越大,反应速度越慢;聚醚二元醇比聚酯二元醇的反应速度快;当分子量超过2000的二元醇与HDI进行预聚反应时,需借助适当的催化剂来加快反应速度,从而使预聚反应能够顺利进行,分别选择DABCO、TOA和DBDTL三种催化剂进行催化反应,发现不同的催化剂,其催化效果相差较大。

In order to unsterdand the properties of rebound and recompression, this study carried out oedometer tests for six soft clays with three surcharge ratios to simulate surcharging. Properties analyzed in this thesis include: 1 post–surcharge secant secondary compression index; 2 amended post- surcharge secant secondary compression index in which the time starts from load application; 3 time at which secondary compression reappears; 4 post-surcharge secondary compression strain rate.

为探讨软弱粘土於超载移除后的回胀与再压缩性质,本研究利用传统单向度压密试验仪对六种土样分别进行三种超载比的超载单向度压密试验,并分析所得结果,分析方法包括:1评估后超载割线二次压缩指数;2评估修正后超载割线二次压缩指数,将后超载的时间原点改为由加载起始时起算;3评估二次压缩再现时间与超载比的关系;4评估后超载二次压缩应变速率之特性。

A synthesis method of 2-(2'-hydroxyl-4'-benzoyloxy-phenyl)-2H-benzotriazole and derivatives thereof is provided, and is characterized in that 2-(2', 4'-dihydroxyphenyl)-5-X-2H-benzotriazole and benzoyl chloride are taken as raw materials for reaction in solvent for 1-8 hours under the temperature of 50-140 DEC C with the mole ratio of 1 to 0.95-1.1, wherein, the amount of the solvent is 2 to 20 times that of the 2-(2', 4'-dihydroxyphenyl)-5-X-2H-benzotriazole and X represents H, F, Cl, Br.

一种2-(2′-羟基-4′-苯甲酸基苯基)-2H-苯并三唑及其衍生物的合成方法,其特征是,以2-(2′,4′-二羟基苯基)-5-X-2H-苯并三唑和苯甲酰氯为原料,在溶剂中进行反应,反应温度50℃~140℃,反应时间1~8小时,反应原料摩尔比2-(2′,4′-二羟基苯基)-5-X-2H-苯并三唑∶苯甲酰氯为1∶0.95~1.1,溶剂用量为2-(2′,4′-二羟基苯基)-5-X-2H-苯并三唑重量的2~20倍,其中X代表H、F、Cl、Br,具有反应条件温和、反应收率高和产物纯度高的特点。

Small signal solution of aberrated second harmonic generation is deduced from three-dimension three wave coupling functions. The numerical work gives out lot of results of different aberrations. The effects of the fundamental wave's aberrations, which will change the conversion efficiency, distribution of intensity and phase in the frequency conversion, is analyzed. It shows that when walk-off and diffraction effects could be ignored approximately estimation of the phase distribution of second-harmonic wave could be done. The far field divergent angle and second moment radius of harmonic wave will vary with the aberration of fundamental wave, but the far field divergent angle will be obviously smaller than that of fundamental wave. The phase distribution of both fundamental and harmonic wave is measured using Hartmann-Shack wave front sensor in the experiment with 1064nm and 790nm lasers, respectively. Results are given.

首次从三维三波相互作用方程组推导得到了位相畸变光束倍频的小信号解;通过建立三维数值模型,编写相应仿真程序,首次得到了位相畸变光束倍频过程的大量计算结果,深入细致地研究了位相畸变光束经非线性光学频率变换后谐波的转换效率、光强分布、位相分布以及影响它们的各种因素;得出谐波的远场发散角和光斑二阶矩的变化规律会因为基波像差的不同而不同,但谐波的远场发散角明显地比相应基波的小的结论;得到了在走离效应和衍射效应等影响许多因素可以忽略的情况下,位相畸变传递到二次谐波的估算式;举例分析了KDP三倍频方案中,基波位相畸变对二次谐波和三次谐波的影响;实验工作中,用哈特曼-夏克传感器分别对1064nm倍频过程和790飞秒超短脉冲倍频过程中的基波和谐波的位相分布进行了测量,给出了相应结果。

Each test will take notes of duration of usage, times for mistake taken and subjective fulfillment, and analyze by SPSS. The research found:(1)In the experiment of stapling papers with different thickness, sample 1 and 3 perform better for the subjects with lower muscle strength. With the same result as experts' tests, Sample 1 and 3 are much suitable for more user groups.(2)in the experiment of filling, sample 3 and 4 are easier and more effective for people with lower muscle strength. The results were concert with experts' test, and it also made fewer mistakes. The staplers which are designed in Universal Design principles still can be improved in filling.

研究发现:(1)在装订纸张堆叠厚度实验中,样本一与样本三在针对肌力的弱势族群比样本二与样本四有较佳的表现,与「专家检测」的结果一致,显示样本一与样本三的机构设计适用於较广泛的使用族群;(2)在订书针装填实验中,样本三与样本四针对肌力的弱势族群比样本一与样本二的完成度更高,结果与「专家检测」的结果一致,其失误率较低,显示经通用设计改良之订书机在订书针装填机构设计上仍有改善的空间。

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I didn't watch TV last night, because it .

昨晚我没有看电视,因为电视机坏了。

Since this year, in a lot of villages of Beijing, TV of elevator liquid crystal was removed.

今年以来,在北京的很多小区里,电梯液晶电视被撤了下来。

I'm running my simile to an extreme.

我比喻得过头了。