三偶氮的

A series of novel dendrons with 1,3,5-triazine structure were synthesized by convergent strategy using cyanuric chloride, p-hydroxyazobenzene,β-naphthol, 1-hydroxyanthraquinone, 3,5-dihydroxybenzyl. They were the first generation p-phenyl-azo-phenyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated dendron G1.0, the first generation naphthyloxy-terminated and 1-anthraquinonoxy-cored dendron G, and the second generation naphthyloxy-terminated dendron G2.0.

以对羟基偶氮苯、β-萘酚为端基，三聚氯氰、3，5-二羟基苄醇为支化单体，1-羟基蒽醌为核心，用收敛法合成了一系列新型结构的含均三嗪环的树枝块：第一代端基为偶氮苯的树枝块G1.0、端基为萘氧基的树枝块G1.0、端基为萘氧基、中心为蒽醌的树枝块G、第二代端基为萘氧基的树枝块G2.0。

By using the limulus test the plasma endotoxin of 20 cases of malignant obstructive jaundice was determined before and after different bile duct drainage.

利用鲎试剂与鲎三肽的偶氮显色法测定20例恶性梗阻性黄疸患者不同引流手术前后血浆内毒素水平。

The antitumor effects of sesquiterpene lactones scabertopin and isodexyelephantopin from the whole plant of Elephantopus scaber were studied in vitro on SMMC-7721,Hela and Caco-2 cancer cell lines.

采用四甲基偶氮唑盐比色法和琼脂糖凝胶电泳法等研究地胆草倍半萜内酯化合物scabertopin(1)和isodeoxyelephantopin(2)在体外对SMMC-7721、Hela和Caco-2三种肿瘤细胞增殖的影响。

Three methods are used to prepare molecular imprinted polymers,which include conventional bulk technique or polymerization with ultraviolet initiated in low temperature and polymerization with silica-gel as sacrificial materials. In the polymerization procedure , Sulfamethazine(SM2)and Sulfisoxazole were used as target template molecules, methacrylic acid and 4-vinylpyridine(4-VP) and acrylamide were selected as functional monomers, ethylene glycol dimethacrylate as crosslinker, azobisisobutyronitrile was used as initator.

主要工作如下：首先，以磺胺异噁唑和磺胺二甲嘧啶为模板，分别以4-乙烯基吡啶，甲基丙烯酸，丙烯酰胺为功能单体，以二甲基丙烯酸乙二醇酯为交联剂，偶氮二异丁腈为引发剂，采用了传统方法(60℃恒温水浴)、牺牲硅胶法及低温紫外光聚合法等三种方法合成了一系列的磺胺类药物印迹聚合物。

Myocardialinfarct size and the area at risk for myocardial infarctionwere measured by Evans Blue and triphenyl tetrazolium chloridestaining, respectively.

心肌梗死面积和可能发生心肌梗死的危险区分别可以用偶氮蓝与氯化三苯四唑染色测量。

The third-order optical nonlinearities and lime responses were measured by a phase conjugate forward, 3-dimensional degenerate, four-wave mixing technique. Comparing polymer's third-order NLO coefficient, it shows that the χsuperscript (3 value increasecs with the introduction of the azobenzol side-chain.

通过简并四波混频飞秒激光系统对各个接枝聚合物的三阶非线性极化率系数进行了测定，考察了偶氮侧链的引入对聚合物主链三阶非线性的影响，并考察了侧链上不同取代基的电子效应对主链三阶非线性的影响。

The experimental results from cyclic voltammetry and constant-potential electrolysis show that the mechanism of the reaction was two molecules and three steps electrochemical process with eight-electrons transferred: anion radical arose in the first step; two-electrons were transferred in the second step and accompanied with coupling reaction of radicals and protonation and dehydrate, the main product was azoxybenzene; two-electrons were transferred in the third step, and azobenzene was achieved.

研究结果表明，硝基苯在铂电极上的电还原反应为双分子八电子三步骤电化学过程：第一步反应为准可逆单电子转移步骤，产生阴离子自由基；第二步为二电子转移步骤，并伴有随后的双分子不可逆自由基偶合反应和快速质子化及脱水反应，主要产物为氧化偶氮苯；第三步是二电子转移产生偶氮苯的过程。

The process is carried out by addition reacting nitrogen benzide dye containing R group with carbimide propyl triethoxy-silane to obtain final product.

将含R基团的偶氮苯染料与异氰酸基丙基三乙氧基硅烷进行加成反应即得含偶氮苯染料的硅氧烷先驱体。

Three series of disperse dyes based on heterocyclic diazo components have been designed. The structures of the synthesized compounds were identified by MS, IR and NMR.

本文设计并合成了三个系列的含杂环重氮组分的偶氮分散染料，通过质谱、红外光谱及核磁共振谱等测试手段验证了所合成的化合物的结构。

This kind of gratings can be kept in the material for a long time. A mode of molecular reorientation was used to explain the formation mechanism of these gratings and it is well consistent with our experimental results. 3. Three kinds of azobenzene polymers P , P (MMA-co-GY7) and P (MMA-co-GO13) were synthesized by radical polymerization. High-density optical storage and the three-dimension (3D) microstructures in the azobenzene polymer films were presented. Twenty gratings have been stored on the same spot in our material. It is twice as many as the best recording that has been reported. It is the first time, a rectangular microstructure and a complicated double layers nesting six-pointed star microstructure are inscribed in it by using a simple two-wave couple setup.

采用共聚反应设计合成了单偶氮苯聚合物P、双偶氮苯聚合物P（MMA-co-GY7）和P（MMA-co-GO13）三种聚合物，研究了偶氮苯聚合物薄膜中的高密度光学存储和3维微结构，成功的将20套光栅储存在样品中同一个点上，是已有报道的两倍；并首次用简单的2波混频光路在该材料中刻写出长方格子和六角星型的微结构，在制作多重不同周期不同角度的高密度光栅结构实验过程中，发现不同周期光栅的刻写顺序对整个微结构形成的最终结果具有决定性的影响，并用相衬显微镜观察了这些微结构图像。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。