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A developmental focus was placed upon the intermediates of the drug such as cephalosporin,antihypertensive,antilipemic,antiulcer,antineoplastic,antiviral,antineuralgic,vitamin and amino acid.

重点发展第二、三、四代头孢菌素中间体、第三、四代喹诺酮类药物中间体、新型抗高血压药物中间体、新型抗高血脂药物中间体、抗溃疡药物中间体、抗癌药及抗病毒药物的中间体、中枢神经药物中间体、手性药物中间体、维生素及各种氨基酸。

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Missirlis in article [1]. At the same time, a sufficient condition for convergence of the PSD method is given to be compared when the coefficient matrix A of the linear system Ax = b is a symmetric, positively defective matrix. In §3.2, an example is given to state that the range of our sufficient condition is wider than theorem 3.3 of article [1]. On the other hand, following a.n analogous approach of [14] and starting the functional relationshipwe have a perfect analysis for the PSD method to converge and optimum valves for the involved parameters under different conditions.Under the assumptions that A is a consistent ordered matrix with nonvanishing diagonal elements and the eigenvalues of the Jacobi matrix of A are real,we get necessary and sufficient conditions for the PSD method to convergence.The result is equal to theorem 1 of article [9].Under the same condition, we can see the optimal parameter and of corresponding spectral radius of thePSD method in [8]:(2)When A is a consistent ordered matrix with nonvanishing diagonal elements and the eigenvalues of the Jacobi matrix of A are imaginary or zero,we get necessary and sufficient conditions for the PSD method to convergence.In chapter 3, the optimal parameter and of corresponding spectral radius of the PSD method are given by table 3.3. Moreover, under the assumption 0

Missirlis在文献[1]中定理3.3的不准确,同时给出了当线性方程组Ax=b的系数矩阵A为对称正定阵时,PSD迭代法收敛的一个充分条件与之比较,并且在§2.3中用实例说明了对于一部分矩阵而言本文得到的充分条件广于[1]中定理3.3的充分条件;另一方面,按照文献[14]的方法,我们从PSD迭代法的特征值λ与其Jacobi迭代矩阵B的特征值μ的关系式:出发,在不同条件下对PSD迭代法的收敛性和最优参数以及最优谱半径进行了完整的分析:(1)在系数矩阵A为(1,1)相容次序矩阵且对角元全不为零,其Jacobi迭代矩阵B的特征值全为实数的条件下,给出了PSD迭代法收敛的充分必要条件,此结果与[9]中的定理1等价,此时最优参数及最优谱半径由[8]得:(2)第三章表3.3中给出了,当系数矩阵A为(1,1)相容次序矩阵且对角元全不为零,其Jacobi迭代矩阵B的特征值全为纯虚数或零时的PSD迭代法的收敛范围和最优参数,并且我们可以得到当0

The research is carried on from four aspects. One is, based on answering the above open problem on a finite dimensional Euclidean space by means of partially ordered theory, to research the existence of solutions, global error bounds of proximal solutions and sensitivity of parametric unique solutions and present a class of variable-parameter three-step iterative algorithms for generalized set-valued variational inclusion problems by using - resolvent operator of set-valued mapping.Two is to consider the convexity, closedness and boundedness of the solution set of general set-valued variational inclusion problems and the sensitivity of the parametric solution set by means of graphical convergence theory. Three is to discuss directly the existence of solutions by using analytical methods for set-valued mixed quasi-variational-like inequalities and suggest a class of direct variable-parameter three-stepiterative algorithms for solving generalized set-valued variational inclusions.

研究分有三个方面:一是借助于偏序理论在有限维欧氏空间中解决了上述公开问题,在此基础上利用集值映射的η-预解算子,研究了广义集值变分包含问题解的存在性、逼近解的全局误差界、参数唯一解的灵敏性,并提出了一类变参数三步迭代算法;二是借助于图收敛理论研究了一般集值变分包含问题解集的凸性、闭性和有界性以及参数解集的灵敏性;三是用分析的方法直接讨论了集值混合拟类变分不等式问题解的存在性并提出了一类求解广义集值变分包含问题的直接变参数三步迭代算法。

Section two:" Hardy, the romanticist " mainly analyzes romanticists' profound influence on Hardy's lierary creation, and thus there is a strong sense of romantic consciousness contained in Hardy's nature poetry.

第三章从三个部分切入,对哈代一些自然诗进行了剖析,比较了哈代自然诗与浪漫主义诗歌的相似之处,意在揭示浪漫主义在哈代自然诗中的体现。

Besides, the derivatives were synthesized successfully by the similar acid binding agent system, such as tris(4-nitrophenyl) thiophosphate, tris(4-toluene)thiophosphate. The derivative of maleic anhydride was synthesized by the simple method, and its yield was above 90%.

采用类似的缚酸剂体系成功地合成了硫代磷酸三(4-硝基苯)酯、硫代磷酸三(4-甲基苯)酯,并用简单的方法合成了硫代磷酸三(4-氨基苯)酯的马来酸酐衍生物——硫代磷酸三(4-马来酸氨基苯)酯,产率达90%以上。

Good thermal stability and self-extinguishing behavior was observed with the cured polybenzoxazine resins. Second, furan-containing benzoxazine monomers, P-FBz, BPA-FBz, and 4FP-FBz were prepared using furfurylamine as a raw material. Formation of furfurylamine Mannich bridge networks in the polymerizations of P-FBz and BPA-FBz increased the cross-linking densities and thermal stability of the resulting polybenzoxazines. P-FBz and BPA-FBz- based polymers also exhibited high glass transition temperatures above 300℃, high char yields, and low flammability with a limited oxygen index value of 31. The dielectric (Dk3.21–3.39) and mechanical properties (high storage modulus of 3.0–3.9 GPa and low coefficient of thermal expansion of 37.7– 45.4 ppm) of the P-FBz and BPA-FBz-based polymers were superior or comparable to other polybenzoxazines. 4FP-FBz used for polybenzo- xazine modification by means of formation of benzoxazine hybridation with P-FBz.

第二部份以2-呋喃甲胺为起始物,制备了P-FBz、4FP-FBz与BPA-FBz 三个含呋喃官能基之氧代氮代苯并环己烷的单体;BPA-FBz与P-FBz於开环聚合中形成之Mannich bridge网状结构有效地提升聚氧代氮代苯并环己烷聚合物之交联密度与热安定性;Poly与Poly具有大於300℃之玻璃转移温度、高的焦炭生成率与具有31之极限氧指数(Limited oxygen index, LOI)的难燃性特质,Poly与Poly之介电常数(Dk=3.21~3.39)与机械性质[3.0~3.9 GPa的储存模数与37.7~45.4ppm之低热膨胀系数( Low coefficient of thermal expansion, Low CTE)]均较其他聚氧代氮代苯并环己烷为优;4FP-FBz具有低之介电常数(Dk=2.7),以其作为降低介电常数之反应型改质剂,与P-FBz混成,证实可有效地降低Poly的介电常数。

Inspired by these results, in this paper, we first give the definition of a new mapping ? uniformly Lipschitz asymptotically nonexpansive mapping on a compact subset of a uniform convex Banach space, then construct three-step iterative sequences of uniformly Lipschitz asymptotically nonexpansive mapping in this subset . We proved the convergence of this three-step iterative sequences for uniformly Lipschitz asymptoticallynonexpansive mapping, Further more, we proved this three-step iterative sequences with an error member converge to fixed points.

从中得到启发,在本文我们首先定义了一致凸Banach空间某非空紧子集上的一种新的映射——一致李普希兹渐进非扩张映射,在该紧子集上构造关于一致李普希兹渐进非扩张映射的三步迭代序列以及具误差的三步迭代序列,先来讨论三步迭代序列的收敛性,进而讨论具误差的三步迭代序列的收敛性。

All of the tripodal schiff base ligands and their complexes were characterized.

以三乙醇胺、巯基苯胺、巯基乙胺为初始原料,设计合成了六个三脚架结构的化合物,其合成路线如下:三乙醇胺与氯化亚砜反应得到三(2-氯乙基)胺(1),然后与巯基苯胺或巯基乙胺在碱性条件下反应生成三脚架结构的三{[2-(2-氨基苯基)硫代]乙基}胺(2)或三{[2-(2-氨基乙基)硫代]乙基}胺(3),然后再与水杨醛、2-甲酰基-8-羟基喹啉(8)、2-甲酰基-8-苄氧基喹啉(7)反应得到六种新型的含硫西佛碱化合

With regard to the lack of corresponding entity right backing for "execute the third party" according to the procedure law in current Chinese creditor"s subrogation system;the inconsistence between the entity law and the procedure law for the conditions to exercise creditor"s subrogation;the obscure effect of the exercising of the creditor"s subrogation;the indefiniteness of right and status of the parties in the subrogation proceeding and so on,it is suggested that amend the civil code,confine the creditor"s subrogation system,coordinate the rules in entity law and procedure law related to the debtees" to exercise their subrogation,define the creditor"s subrogation,the right and obligation of related parties in the procedure,perfect the rules in procedure law in order to provide proceeding procedure security for the realization of the creditors subrogation.

并针对我国现行债权人代位权制度在程序法中&执行第三人&缺乏相应实体权利依据、实体法与程序法有关债权人代位权行使条件规定不一致、债权人行使代位权效力不清、当事人在代位权诉讼中的地位和权利不明确等诸多缺欠,提出了制定民法典确定债权人代位权制度、协调实体法和程序法中关于债权人行使代位权的规定、明确债权人代位权诉讼相关当事人的权利义务、完善程序法规定为债权人代位权实现提供诉讼程序保障的意见。

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