三乙胺

Methods Protein in blood and urine was precipitated directly by acetonitrile with acetanilide was used as the internal standard using Agilent Zorbax SB-Aq column (250 mm×4.6 mm, 5 μm). The mixed solvents of water (triethylamine 0.12%, acetic acid 0.12%) and acetonitrile were used as the mobile phase to separate cephalosporins using gradient elution method at 1 mL/min and 254 nm.

以乙酰苯胺为内标，血液和尿液用乙腈直接沉淀蛋白，采用Agilent Zorbax SB-Aq(250 mm×4.6 mm， 5 μm)色谱柱，流动相选用水（含0.12%三乙胺和0.12%乙酸）和乙腈的混合溶剂梯度洗脱，流速1 mL/min，检测波长254 nm。

hydroxy-2-acetonaphthene was obtained by the hydrolysis of 6-methoxy- 2-acetonaphthene in the presence of HCl (36%) and triethylamine as a catalyst.

摘 要：采用6 甲氧基 2 乙酰萘与浓盐酸在缚酸剂三乙胺存在的条件下进行水解反应制得6 羟基 2 乙酰萘。

The taurohyodeoxycholic acid was synthesized by aminolysis of sodium taurine with carboxy-carbonate mixed anhydride prepared by reacting hyodeoxycholic acid with ethyl chloroformate at the present of triethylamine.

猪去氧胆酸与氯甲酸乙酯在三乙胺存在下反应生成羟酸－碳酸乙酯混合酐，而后将其与牛磺酸钠进行氨解反应，合成猪磺去氧胆酸。

A sample-pretreated method of ether-extraction-precolumn-derivation was established, and the chromatographic conditions, which was used for determinating the derivant of extracted UDCA, were decided to be Hypersil C_(18) column(250×4.6mm, 10μm), acetonitrile-methol-0.005mol·L~(-1) phosphoric buffer-triethylamine(50:27:42:0.25, adjusted to pH3.0±0.1 by phosphoric acid) as mobile phase with detective UV wavelength at 247nm and column temperature at 35℃.

建立了乙醚提取-柱前衍生化血浆样品预处理方法，采用Hypersil C_(18)柱(250×4.6mm，10μm)，乙腈-甲醇-0.005mol·L~(-1)NaH_2PO_4缓冲液-三乙胺(50：27：42：0.25，磷酸调节pH3.0±0.1)为流动相的HPLC法，以溴苯乙酮为衍生化试剂，在247nm处测定家兔血浆中熊去氧胆酸衍生化产物。

A novel fluorescent acrylamide monomer, N-(4-Benzooxazol-2-yl-phenyl)- acrylamide, was prepared from o-aminophenol, p-aminobenzoic acid and acryloyl chloride, with polyphosphoric acid as dehydrating agent and triethylamine as deacidification agent.

以邻氨基苯酚、对氨基苯甲酸和丙烯酰氯为原料，以多聚磷酸为脱水剂、三乙胺为脱酸剂，研制了一种新的荧光丙烯酰胺单体N-[4-（苯并噁唑-2-）苯基]丙烯酰胺。

A(C2H5)3N·HCl-induced palladium complex PdL2Cl2 and CuCl2 catalyzed cyclotrimerization reaction of Ethyl Propiolate has been reported for the first time.

报道了一类三乙胺盐酸盐存在下钯PdL2Cl2-CuCl2催化体系催化的丙炔酸乙酯(Ethyl Propiolate，简称EP)环三聚反应。

In application of modified phenol-formaldehyde resin in OCC pulp, firstly the application effictiveness of phenol-formaldehyde resin modified by triethylamine and diethylene triamine in OCC pulp was researched, and the optimum application effictiveness was gotten through mon- factor trial.

通过对改性酚醛树脂在OCC废纸浆中的应用研究，考察了二乙烯三胺和三乙胺改性酚醛树脂在OCC废纸浆中的应用效果，并通过单因素实验得到了改性酚醛树脂的最佳应用效果。

Cellulose benzoate,the degree of substitution of which was calculated from the content of C determined by element analysis,was prepared from microcrystalline celluloseand benzoyl chloride under heterogeneous condition and characterized by FT-IR and~1H-NMR.

研究了微晶纤维素和苯甲酰氯在多相条件下合成制备纤维素苯甲酸酯的反应，通过元素分析所得碳的质量百分含量计算了产物的取代度，并系统研究了吡啶与N，N-二甲基乙酰胺或与三乙胺混合反应溶剂、苯甲酰氯与纤维素羟基的摩尔比r、反应温度和反应时间对D S的影响，用FT-IR和1H-NM R对产物进行了表征。

Column: Agilent C18; mobile phase 10mol.l-1 monobasic Acetate buffer, 20 molL-1triethylamine solution adjusted to pH5.5 with Acetic acid -acetonitrile ,gradient elution, flow rate: 0.6 mLmin-1; Results:The Traditional Chinese Medicines contained Acarbose, Phenformin and Glibenclamide, and can be separated completely.

色谱柱：Agilent ZORBAX ODS C18柱(5μm，4.6×250mm， Agilent)；流动相：醋酸盐缓冲液(10molL-1醋酸胺，20 molL-1三乙胺，用醋酸调节pH5.5)与乙腈，梯度洗脱，流速：0.6 mLmin-1，色谱检测波长234nm，格列吡嗪为内标物进行定量分析。

Column: Agilent C18; mobile phase 10mol.l-1 monobasic Acetate buffer, 20 mol·L-1triethylamine solution adjusted to pH5.5 with Acetic acid -acetonitrile ,gradient elution, flow rate: 0.6 mL·min-1; Results:The Traditional Chinese Medicines contained Acarbose, Phenformin and Glibenclamide, and can be separated completely.

色谱柱：Agilent ZORBAX ODS C18柱(5μm，4.6×250mm， Agilent)；流动相：醋酸盐缓冲液(10mol·L-1醋酸胺，20 mol·L-1三乙胺，用醋酸调节pH5.5)与乙腈，梯度洗脱，流速：0.6 mL·min-1，色谱检测波长234nm，格列吡嗪为内标物进行定量分析。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。