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Simetryne is synthesized from cyanuric chloride, ethylamine and sodium methyl mercaptide in solution of the trichloroethylene.

以三聚氯氰、乙胺和甲硫醇钠为原料,以三氯乙烯为溶剂制备了西草净。

The appropriate conditions are that the mole ratio of cyanuric chloride to ethylamine, sodium hydroxide, sodium methyl mercaptide is 1:2.1:2.1:4.0, the temperature and time of first, second, third substitution reaction is respectively 0℃, 20℃, 78℃ and 10min, 30min, 480min.

适宜反应条件为三聚氯氰:乙胺:氢氧化钠:甲硫醇钠=1:2.1:2.1:4,第一、第二、第三取代反应的反应温度和反应时间分别为0,20,78℃和10,30,480min。

Simetryne was synthesized from cyanuric chloride, ethylamine, and sodium methyl mercaptide in a 50% isopropanol + water solution.

以三聚氯氰、乙胺和甲硫醇钠为原料,以50%异丙醇+50%水为溶剂制备了西草净。

Cytotoxic effect was demonstrated with nitrogen mustard, nitromin, sarcolysin, thio-TEPA and myleran at concentrations of 7, 10, 25, 35, 100, and 100μg/ml respectively.

氮芥及氧化氮芥在7—10微克/毫升,溶肉瘤素和新恩必恨于25—35微克/毫升,三乙酰硫代磷酰胺和丁二醇二甲磺酸酯在100微克/毫升,都出現了显著的細胞毒作用,使細胞很快死亡溶解;但6-巯基嘌吟和氨基喋吟未表現作用。

After centrifugation, the extracts were separated on HILIC column by using acetonitrile-water as mobile phase. The analytes were identified and quantitated by LC-tandem MS under the positive/negative electrospray ionization and multiple reaction monitormode. The calibration curves showed good linearity in the range of 25-5000 μg/kg for melamine and cyanuric acid, and 50-10000 μg/kg for ammeline and ammelide. The limits of detection and limits of quantification were in the range of 5-20 μg/kg and 50-100 μg/kg, respectively.

牛奶样品直接用乙腈超声波提取;奶粉样品先用水溶解后再加乙腈超声波提取,高速离心后以乙腈-水为流动相,采用亲水作用色谱柱分离这4种化合物,在电喷雾正、负电离切换多反应监测模式下进行定性与定量分析,三聚氰酸一酰胺与三聚氰酸二酰胺含量在50~10000μg/kg之间、三聚氰胺与三聚氰酸在25~5000μg/kg之间,均获得良好的线性。

Omeprazole racemate was resolved respectively by simulated moving bed chromatography and batch chromatography with the coated cellulose triphenylcarbamate as chiral stationary phase and ethanol containing 0.1% diethylamine as mobile phase.

用纤维素三苯基氨基甲酸酯涂敷型手性固定相和含0.1%二乙胺的乙醇溶液,研究了模拟移动床色谱和间歇色谱对奥美拉唑对映体的拆分。

The results showed that there was a more better effect of filmformation and absorbency to use poly 1788 as an adhesive and polyvinyl pyrrolidone(K:90) as a hydrophilic polymer. The silicon dioxide with particle size 0.3-1 μm as a inorganic pigment had a better absorbency. The polyethylene glycol modified with ethylenediamine had a more better characteristic of dye immobilization, absorbency and definition than the polyethylene glycol modified with diethylenetriamine, of which the polyethylene glycol of molecular weight of 400 modifiedwith ethylenediamine had more best performance.

研究结果表明:采用聚乙烯醇1788作黏合剂、聚乙烯吡咯烷酮(K值为90)作亲水性高分子可得到比较理想的成膜效果和吸墨效果;粒径分布范围在0.3-1 μm的二氧化硅作为无机颜料具有较好的吸墨性能;用乙二胺改性的聚乙二醇比用二乙三胺改性的聚乙二醇具有更好的固墨性、吸墨效果以及清晰度,其中乙二胺改性的分子量为400的聚乙二醇所得到的烷基多胺的效果为最好。

First, the geometry optimization for 1-phenyldibenzophosphole and triphenylphosphine were carried out using quantum chemical AM1 method.

用量子化学AM1方法优化了1-苯基二苯并膦和三苯基膦的几何构型,比较了两种化合物的电子结构和空间结构,发现PDBP作为羰基合成铑膦催化剂的配体要优于三苯基膦;系统研究了PDBP的合成方法,其最佳合成条件为:在无水无氧的条件下,采用二乙胺锂与溴化四苯基膦摩尔比为3,反应温度为22 ℃,反应5 h,反应后酸化, pH值为1~2,产物收率可达到85%~88%。

The duration of triple chemotherapy with isoniazid, rifampin, and ethambutol, disease seerity, operatie procedures, and outcome were analyzed.

对用异烟肼、利福平、乙胺丁醇进行三联化疗的持续时间,病变的严重程度,手术方式和治疗结果进行分析。

Approximately 30 mg of fresh algal material was extracted by homogenising it in ice-cold 5% 5-sulfosalicylic acid solution containing 6.3 mM diethylentriaminepentaacetic acid, according to De Knecht et al.

大约30毫克的淡水藻类物质提取homogenising在冰冷的5%的5-磺基水杨酸溶液的载有6.3毫米三乙四胺五乙酸,根据De Knecht等人(1994年)。

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