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三乙胺

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This paper presents the synthesis of three kinds of amine such as 2-(methyl- sulonyl)ethylamine,3-propylamine and 2--ethylamine via three different methods.

本文采用三种不同的方法合成了2-乙胺,3-丙胺,2-乙胺等3个含砜基伯胺;还合成了3--x-吲哚甲酸甲酯(x=5,6,7), E-4-喹啉甲醛肟,E-6-氟-2-吡啶甲醛肟等三类芳环甲醛肟,其中吲哚类和吡啶类化合物未见文献报道。

The surface hydroxyl group onto magnetic polyvinyl acetate nanoparticles can be obtained by saponification reaction on their surface.

结果表明,磁性聚苯乙烯颗粒与丁二酸酐发生Freidel-Crafts酰基化反应,可以在颗粒表面引入少量羧基;磁性聚甲基丙烯酸甲酯颗粒分别与乙二醇、二缩三乙二醇、聚乙二醇等发生醇-酯交换反应,可以在颗粒表面接枝不同分子链长度的末端羟基;磁性聚醋酸乙烯酯颗粒经过醇解或皂化反应可以获得表面羟基;磁性聚丙烯酸甲酯颗粒通过乙二胺或1,6己二胺的胺解反应可以得到表面氨基,继而与一氯乙酸反应可以引入亚胺二乙酸基团。

Catalyzed by triethyl amine , vitamin E succinate was synthesized with vitamin E and succin-ic anhydride.

三乙胺为催化剂、维生素E和琥珀酸酐为原料合成维生素E琥珀酸单酯。

The results show that Irgacure1000 is preferable in the system and the rate is highest when the amount of Irgacure1000 is 3%;the drying condition has a considerable impact on the rate ; it decreases with the increase in neutralization degree;when NaOH is used as neuralization agent,the rate at the later period is higher than that when triethyl amine used; the structure of polymer has a certain effect on the rate and it accelerates with the increase in the ratio of PBA/DMPA and HEAD/DMPA.

结果表明,本体系优选光引发剂Irgacure1000的质量分数为3%时固化速度最快;干燥条件对光固化速度有很大的影响;随着中和度的提高,固化速度下降;用NaOH作为中和剂时,后期固化速度快于用三乙胺;聚合物结构对固化速度有一定的影响,随着PBA/DMPA和HEA/DMPA比例的提高,固化速度加快。

Experimental results showed that the hydrogenation degree can be enhanced significantly by the addition of triphenylphosphine. When the molar ratio of TPP, TPPTS and Ru is 2:5:1, 89% hydrogenation degree can be achieved after 12 h under reaction conditions of 5.0 MPa and 150~C.

考察了溶剂种类、水溶液的pH值、添加助剂三乙胺、水/有机两相体积、底物浓度等对对-氯硝基苯转化率和生成对-氯苯胺选择性的影响,并在90℃、4.0MPa、反应时间为6h的条件下,进行了催化剂的循环实验。

All of the tripodal schiff base ligands and their complexes were characterized.

以三乙醇胺、巯基苯胺、巯基乙胺为初始原料,设计合成了六个三脚架结构的化合物,其合成路线如下:三乙醇胺与氯化亚砜反应得到三(2-氯乙基)胺(1),然后与巯基苯胺或巯基乙胺在碱性条件下反应生成三脚架结构的三{[2-(2-氨基苯基)硫代]乙基}胺(2)或三{[2-(2-氨基乙基)硫代]乙基}胺(3),然后再与水杨醛、2-甲酰基-8-羟基喹啉(8)、2-甲酰基-8-苄氧基喹啉(7)反应得到六种新型的含硫西佛碱化合

Methods The internal standard was diazepam, the samples were extracted by ethyl acetate after basified the plasma., the column was Hypersil C18, and the mobile phase mixed of methanol: water(75:25) containing 0.03%-triethylamine.

色谱柱为Hypersil ODS C18 4.0mm×250mm,流动相为含0.03%三乙胺的甲醇:水(75:25),流速1.0ml/min,紫外276nm波长检测。

Six carboxyl acids DEMB was produced with Michael Reaction using triethylamine as alkaline catalyst and solvent, malonic acid and itaconic acid as raw materials.

三乙胺为催化剂和溶剂,衣康酸和丙二酸为原料,采用迈克尔加成反应合成了含有6个羧基的多元羧酸DEMB。

Liq. paraffin 10.0, lanolin 2.0, beeswax 5.0, polysorbate 80 3.5 sorbitan monofatty acid esters 1.5, water and Na4GeO4 72.0 and triethylamine 0.5%.

例如,一种乳液可被制备,它含有液体石蜡10.0%;羊毛脂2.0%;蜂蜡5.0%;聚山梨糖酸酯803.5%;山梨糖醇的单脂肪酸酯1.5%;水和Na4GeO472.0%及三乙胺0.5%。

Liq. paraffin 10.0, lanolin 2.0, beeswax 5.0, polysorbate 80 3.5 sorbitan monofatty acid ester s 1.5, water and Na4GeO4 72.0 and triethylamine 0.5%.

例如,一种乳液可被制备,它含有液体石蜡10.0%;羊毛脂2.0%;蜂蜡5.0%;聚山梨糖酸酯803.5%;山梨糖醇的单脂肪酸酯1.5%;水和Na4GeO472.0%及三乙胺0.5%。

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