三

By using multi-dimensional nuclear magnetic resonance method we have studied the folding mechanism of staphylococcal nuclease in vitro; the tertiary interactions for folding of SNase fragments into native-like conformation; the interaction between SNase N- and C-terminal subunits; the relationship of enzyme activity with folding and dynamic states of SNase; the structural properties of enzyme protein while exert its function. We have studied the internal motions of thermophilic Archaea protein Ssh10b and mechanism of its heat-resistance using the NMR 1H-15N relaxation and H/D exchange methods. We have determined the 3D solution structure of human translationally controlled tumor protein TCTP and the Ca2+-binding site; determined the 3D crystal structure of human mitoNEET, a novel protein from distinct groups of iron-sulfur proteins; determined the 3D solution structure of a novel chromatin protein Cren7. Determination of SNase-DNA and Archaea protein-DNA complex structures are in progress.

运用异核多维核磁共振方法研究了金黄色葡萄球菌酶体外折叠机制，酶蛋白片段体外折叠成类天然溶液三维构象的三级相互作用力，酶蛋白亚基间的相互作用，酶蛋白的折叠以及内运动状态与酶活力的关系，酶蛋白发挥功能时的结构特性；运用NMR的1H-15N 驰豫和H/D交换方法研究了嗜热古菌蛋白质Ssh10b双体结构内运动特性，热稳定性机制；确定了人翻译控制的肿瘤蛋白TCTP蛋白的溶液三维结构及其钙离子的结合部位；确定了一类新的铁硫蛋白家族蛋白人线粒体膜上mitoNEET蛋白的晶体结构；确定了一个新型的染色质蛋白Cren7的溶液三维结构；正在研究金黄色葡萄球菌酶及嗜热古菌蛋白质与DNA复合体的溶液三维结构。

Considering the strength enhancing efficiency of phenol-formaldehyde resin modified by triethylamine and diethylene triamine in OCC pulp, the efficiency of phenol-formaldehyde resin modified by diethylene triamine was better than triethylamine.

综合考察二乙烯三胺和三乙胺改性的酚醛树脂的增强作用，二乙烯三胺作为改性剂时改性的酚醛树脂要优于三乙胺改性的酚醛树脂。

During the preresearch on the testing well location selection in the south of western depression, three kinds of process and research work have been done according to the log datum on Well Moushen:(1)Formation analysis and formation pressure evaluation which verdicts that formation under 5198.5m is not of Trias, whereas is still in Permian, and abnormal formation pressure phenomenon exists in Members 1 and 3-4 of Shahejie Formation;(2)Re-interpretation of oil and gas formation and evaluation of reserve formation;(3)Evaluation of oil source rock. Members 1 and 3-4 source rocks of Shahejie Formation have good capability of oil generation.

在东濮凹陷西洼南部探井选位的前期研究中，根据该井的测井资料情况，做了三方面处理和研究工作：①地层分析和地层压力评价，认为5198.5m以下的地层不是三叠系而仍是下第三系，沙一段和沙三段—沙四段存在高压异常；②重新解释油气层和评价储集层，在沙三段—沙四段发现6层12.87m厚可疑油层；③评价油源岩，认为沙一段和沙三段—沙四段油源岩具有较好的生油能力。

Tri-cyanurate as a excellent additional retardant was synthesized by using cyanuric chloride_3,tribromophenol as main materials and under the condition of sodium hydroxide,dichloromethane,toluene as solvent respectively.

以三聚氯氰3和三溴苯酚为主要原料，在碱性条件下，分别以二氯甲烷、甲苯作为溶剂，合成了一种性能优良的添加型阻燃剂三三聚氰酸酯。

This paper, aimed at the problem of drying aluminum fluoride trihydrate, studied the most possible binding format of crystal water, and hereby deduced the process of crystal water dehydration.

本论文针对三水氟化铝的干燥脱水问题，应用晶体结构理论、价键理论以及各种相关化学原理推测了三水氟化铝可能的结晶水结合形式，并据此推断了其结晶水的脱除过程：对氟化铝干燥特性进行了实验研究，研究了温度和升温速率对氟化铝干燥效果的影响：采用非等温TG-DTG法，对三水氟化铝进行了热分解行为和热分解动力学分析，进一步验证了三水氟化铝的脱水过程，并得出了其脱水和水解过程的动力学参数及方程。

A new production technology of high-quality trimellitic anhydride with the liquid-phase air-oxidation from 1,2,4-trimethylbenzene was developed.

偏苯三酸酐的生产方法主要有偏三甲苯气相空气氧化法、偏三甲苯液相硝酸氧化法、偏三甲苯液相空气氧化法和间二甲苯甲醛液相空气氧化法。

In this paper, the chemical equilibrium constants of the reactions in the reaction system of toluene disproportionation and trimethylbenzene transalkylation reaction system were carefully calculated , and the equilibrium compositions of the components at different temperatures and different feed mole ratios were analysed .

对甲苯歧化与三甲苯烷基转移反应体系中反应的化学平衡常数进行了详细计算，并对不同温度、不同进料组成下的平衡组成进行了分析。结果表明，随温度升高，甲苯与三甲苯的芳烃平衡转化率降低，二甲苯的平衡组成亦降低；降低进料中甲苯和三甲苯的摩尔比，甲苯和三甲苯的总芳烃平衡转化率降低，而二甲苯的平衡组成明显上升。

This thesis consists of two parts. In Chapter 1, we synthesized novel polyimides containing 1,2,4-triazole and triphenylamine groups. In Chapter 2, we synthesized polys in which main chain contains triazole group and side chain was carbazole group or triphenylamine group.

本实验共分两部分：第一章以合成含1，2，4-三氮唑和三苯胺结构的聚醯亚胺；第二章以合成三氮唑为主链，侧链分别含有咔唑与三苯胺之聚醚醯亚胺，并探讨其热性质、光学性质及应用。

TrithiocarbonatesS,S\'-bis (α,α′-dimethyl-α-acetic acid) trithiocarbonate (TTC1),3-(2-carboxyethylsulfanylthiocarbonylsulfanyl) propionic acid (TTC3),2-(2-carboxyethylsulfanylthiocarbonylsulfanyl) propionic acid (TTC4) and2-(2-carboxyethylsulfanylthiocarbonylsulfanyl)-2-methylpropionic acid (TTC5) weresynthesized by phase transfer method.

用相转移法合成了S，S′-二(α，α′-甲基-α&-乙酸)三硫代碳酸酯(TTC1)、S，S′-二丙酸三硫代碳酸酯(TTC3)、S-丙酸-S′-三硫代碳酸酯(TTC4)和S-丙酸-S′-(α，α′-甲基-α&-乙酸)三硫代碳酸酯(TTC5)。

Three primer pairs located in psbA~trnK, psbB~psbH and trnR-ACG~trnN-GUU regions were applied in phylogenetic analysis according to Maximum parsimony and Neighbor-joining methods. The consistent results between the phylogenetic analysis and taxonomy indicated the application potential of the three primer pairs in phylogenetic analysis and species identification. However, due to no sequence variation observed in amplified regions between two vegetable soybean varieties (KS5 and KS8), two cowpea subspecies (Vigna unguiculata ssp. cylindrica and Vigna unguiculata ssp. sesquipedalis), and among three rice varieties (TNG67, TK9, and TCS10), the three primer pairs are not effective in identifying variation within species.

选择其中三组引子对(基因体位置为psbA~trnK、psbB~psbH及trnR-ACG~trnN-GUU)增幅片段之序列进行亲缘分析，以最大简约法及邻接法之分群结果皆与目前植物分类相符，故三组引子对在物种间亲缘关系分析及物种鉴定上都有不错的效果，位於psbA~trnK及psbB~psbH之引子对效果尤佳，但是三组引子对在物种内变异的辨识效果不甚理想，在两个毛豆品种间(高雄5号与高雄8号)、两个豇豆亚种间及三个水稻品种间(台农67号、台稉9号与台中秈10号)的增幅片段没有明显差异存在。

According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm～150rpm时取得最大值，此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世，形体几无变化。