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Catheterization measurements were repeated at 5,10, and 15 min after completion of ketamine load.

在七氟醚的共同作用下,氯胺酮并不增加自主呼吸的肺动脉高压儿童的肺血管阻力。

Second, among the seven yeast strains investigated, Rhodotorula gracilis AS 2.499 exhibited the highest activity and stereo-selectivity to tert-butyl-6-chloro-5-hydroxy-3-oxohexanoate.

其次,从实验室保藏的七株酵母菌株中筛选出对-6-氯-5-羟基-3-羰基己酸叔丁酯具有较高还原能力的菌株——Rhodotorula gracilis AS 2.499。

Inhibition to biological treatment process by seven naphthalene derivatives was investigated with Rank Cell respirometer, and all the test chemicals were proved to be potential inhibitors to both activated sludge process and nitrification at different level.

用Rank Cell呼吸仪研究了2-萘酚、1-萘胺、5-氨基-1-萘酚、1-氨基-4-氯萘、2-萘磺酸、2-氨基-1-萘磺酸和7-氨基-4-羟基-2-萘磺酸等七种萘系列有机化合物对生物处理过程的抑制,证明被测化合物对活性污泥过程和硝化过程均有不同程度的抑制作用。

Methyl-2,3,5,6-tetrafluoro-benzene methanol was synthesized by chlorination, acylation, fluorination, esterifica- tion, reduction, bromization, reduction from terephthalic acid. Tefluthrin was obtained from-(1RS,3RS)-3-(2-chloro-3,3,3-trifluoro-1-propenyl)-2,2-dimethyl cycolpropa-necarboxylate acid by reacting with 4-methyl-2,3,5,6-tetrafluoro-benzene methanol.

以对苯二甲酸为原料,经氯化、酰氯化、氟化、酯化、还原、溴化、还原七步反应合成了4-甲基-2,3,5,6-四氟苄醇,甲基苄醇与-(1RS,3RS)-3-(2-氯-3,3,3-三氟丙-1-丙烯基)-2,2-二甲基环丙甲酸一步酯化合成了七氟菊酯。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应,以光学纯酒石酸为原料,研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性,全文共分三部分十个章节:第一部分对当前手性药物和手性技术进行了概述,并由此展开了本文的研究背景和任务;第二部分为有机合成部分,对醛的不对称烯丙基化反应进行了深入探讨,以苯甲醛为原料对反应条件进行优化,在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选,优化配体回收实验条件,最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性,结晶回收的手性配体光学纯度保持不变。

The main contents of experiment as following:(1) Modified polymerized ferric sulphate decoloring agent is made through oxidation, hydrolyzation, polymerization with ferrous sulphate heptahydrate, sulphate acid, natrium chlorate etc.

本论文为印染废水的絮凝沉降处理方法提供了一种新型的性能优良的脱色剂,具体内容有:(1)采用七水硫酸亚铁、硫酸、氯酸钠等原料,通过氧化、水解、聚合反应,制备了改性聚合硫酸铁脱色剂。

The Queen's Hotel, Ennis, county Clare, where Rudolph Bloom died on the evening of the 27 June 1886, at some hour unstated, in consequence of an overdose of monkshood selfadministered in the form of a neuralgic liniment composed of 2 parts of aconite liniment to I of chloroform liniment purchased by him at

181克莱尔郡恩尼斯的王后饭店。一八八六年六月十七日傍晚,鲁道尔夫。布卢姆因服用过量的乌头,在此故去,时间不详。他服的是按附子搽剂二、氯仿搽剂一(系他于一八八六年六月二十七日上午十点二十分在恩尼斯教会街十七号弗朗西斯。登内希药房所购),按比例亲自配制的神经痛搽剂。

Respectively, glutamic acid derivatized β-CD has been synthesized with epoxy chloropropane as the intermediate, a water-insoluble yellow liquid was got after the acetylating of the by using acetic anhydride, which was used as a novel gas chromatographic CSP; A water-soluble β-CD polymer cross-linked with epoxy chloropropane has been synthesized, and the derivatives of β-CD polymer were synthesized by its alkylating and acetylating. The different β-CD derivatives were coated on silica capillary columns by dynamic method, the chromatographic properties and retention behaviors of the fused silica capillary columns were studied, the results showed that the β-CD derivatives had good stereoselectivity and separation results to some compounds, especially to various positional isomers and enantiomers.

本文还分别以环氧氯丙烷为中间体,合成了七{2,6-二-O-[3-(1,3-二羟基丙氨酸)]}-β-环糊精,再用醋酸酐将其乙酰化,得到了一种淡黄色粘稠液体,合成了一种新型的环糊精衍生物;以环氧氯丙烷作交联剂合成了一种水溶性的β-环糊精聚合物,再将其烷基化和酰基化,合成了β-环糊精聚合物的不同衍生物,用动态法将不同类型的β-环糊精衍生物涂渍在石英毛细管柱上,通过对所制备柱柱性能的测试和对一系列化合物的分离和保留行为的研究,结果表明所合成的β-环糊精衍生物对各类化合物,特别是对位置异构体和对映异构体具有较好的分离效果,显示了很强的立体选择性。

In chapter 7, chloride absorption or binding isotherm of concretes was investigated, linear chloride binding capacity and a non-linear coefficient were firstly proposed, based on a large amount of experimental data of concretes under the actions of single, double, or multiple factors in four typical bitterns.

第七章根据不同混凝土在4种典型盐湖的单一、双重和多重因素作用下的大量数据,研究了混凝土对氯离子的吸附/结合规律,提出了线性氯离子结合能力和非线性系数的新概念。

In the 1970s and 1980s, there was concern over the emissions of chlorinated organic substances, such as dioxins and furans, from the use of chlorine in pulp bleaching.

在七十年代和八十年代,人们对超过排放含氯的有机物质,如二恶英和呋喃,从使用氯漂白。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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