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FGD gypsum further into α-form calcium sulfate hemihydrate by heating in an aqueous solution consisting of some alkail earth metal salts and sulfuric acid or chlorhydric acid at the atmospheric pressure has been studied in this subject.

FGD残渣在碱土金属盐类的盐溶液中,在丁二酸、丙三醇等结晶改良剂的作用下,与大气压下加热脱水生成α半水石膏。

The resulting polymer electrolyte possesses 1.57×10~(-3) S·cm~(-1) of ionic conductivity at room temperature when it contain 5wt% of LiBF_4 and 1wt% of zwitterion salt.

研究表明Zwitterion型离子液体1-甲基-3-磺酸正丁基咪唑盐,具有较高的熔点和热分解温度,熔点为219℃,分解温度达320℃。

Sodium(3 S,4S)-3-amino-4--2-ox-Oazetidine-1 -sulfonate is its key intermediate, a chiral zwitterion.

手性内盐(3S,4S)-3-氨基-4-氨甲酰氧甲基-2-氧代氮杂环丁酮-1-磺酸钠是卡芦莫南的关键中间体。

The catalytic system composed of NHPI and transition metal ion can catalyze effectively ethane into acetic acid,cyclane into dicarboxylic acid,toluene into benzoic acid,alkene into epoxide,alkyne into acetylenic ketone,and amide into imide;NHPI used alone can catalyze adamantane to be carbonylated,hydrogen peroxide prepared by oxidization alcohol;NHPI combined with as...

NHPI与过渡金属离子组成的催化体系能高效地催化乙烷氧化为乙酸、环烷烃氧化为二元羧酸、甲苯氧化为苯甲酸、烯烃氧化为环氧化物、炔烃氧化为炔酮、酰胺氧化为酰亚胺;NHPI单独使用能催化金刚烷发生氧化羰基化反应、催化氧化醇制取过氧化氢;NHPI与有机助催化剂如偶氮二异丁腈、溴化季铵盐、蒽醌和醇等也能催化分子氧氧化反应。

Methods starting from dimethyl succinate and benzaldehyde, mitiglinide calcium was obtained via 7 chain steps including stobble condensation, hydrolization, anhydration, condensation with cis-hexahydroisoindoline, reduction, separation, salt formation.

方法以丁二酸二甲酯和苯甲醛为原料,经stobble缩合、水解、脱水,与顺-全氢异吲哚缩合后经还原、拆分、成盐等7步反应制得糖尿病治疗药物米格列奈钙。

Penbritin, salt, alkeran, intermediate compound, cephalothin, cephalosporium triazine, analgin, peimitidine, vitaminB, vitamin C, medical metasilicic acid, coffin, tea, flower extract, folium ginkgo, chocolate powder, amylum, corn embryo and other medicine raw materials and medical intermedia.

氨苄青霉素、邓盐、左旋苯甘氨酸及中间体、头孢氨噻、头孢三嗪、安乃近,西咪替丁、维生素B、维生素C、药用偏硅酸镁、咖啡因、茶、花提取物、银杏叶、巧克力粉、淀粉、玉米胚牙芽等原料药及医药中间体。

In this Ph. D. dissertation, reverse microemulsion method was fully used infabricating and modifying polyacrylamide with functional and high-relative moleculeweight. The copolymerization of 2-acrylamide-2-methylpxopanesulfonic acid, fluorescent monomer 4-methoxy-N-(2-N\', N\'-dimethylamino ethyl)naphthalimide alkyl chloride quaternary ammonium salt, fluorescentmonomer 4-(N\'-methyl-1-piperazinylallyl)-N-butyl-naphthalimide chloride quaternaryammonium salt, Cationic monomer dimethylethylammonium bromide and hydrophobical monomer octadecylacrylate with acrylamide and properties of the copolymers werestudied. The interaction between five polymers and Al_2O_3(012) crystal surface have beensimulated by Materials Studio 3.0 program package, binding energies and non-bondinteraction energies and deformation energies have also been acquired.

本文以制备具有较高相对分子质量和功能型PAM为研究目的,将反相微乳液法运用到其制备及改性的有关环节,通过反相微乳液聚合工艺,将几种改性功能单体2-丙烯酰胺基-2-甲基-丙磺酸、荧光单体2-(4-甲氧基-1,8-萘二甲酰亚胺基)-乙基二甲基烯丙基氯化铵、荧光单体4-(N'-甲基-1-哌嗪基)-N-丁基-1,8-萘烯丙氯季铵盐、阳离子单体丙烯酰氧乙基-二甲基-乙基溴化铵和疏水单体丙烯酸十八酯与AM共聚,制备AMPS改性PAM、荧光示踪型PAM、阳离子单体DMB改性PAM和OA改性PAM等四类不同功能单体改性PAM,并研究其应用性能。

ABSTRACT: In the presence of sodium t-butoxide and DMSO,ethyl 2-oxocyclopentanecarboxylate was subjected to C-alkylation with 2-(4-bromomethylphenyl)propanoic acid with high regioselectivity to give 2-[4-(1-ethoxycarbonyl-2-oxo-1-cyclopentanylmethyl)phenyl]propanoic acid (4) which was followed by hydrolysis,decarboxylation and salt formation to afford loxoprofen sodium in about 72% overall yield.

在叔丁醇钠和二甲基亚砜的存在下,2-丙酸对2-乙氧羰基环戊酮进行C-烷基化,再经水解脱羧,成盐即得洛索洛芬钠,以2-丙酸计算,总收率为72%。

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