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Water-soluble air drying alkyd resin is formulated by flax oil acid,trimethylol propane,dimethyl isophthalate,benzoic acid,maleic anhydride and trimellitic anhydride.

以亚麻油酸、三羟甲基丙烷、间苯二甲酸、苯甲酸、顺丁烯二酸酐、偏苯三酸酐为原料合成水溶性醇酸树脂,中和后制得的涂料具有干性好、硬度高、耐水性和贮存稳定性优良等特性。

Using tetrabutyl titanate and methyl methacrylateor 2-Hydroxyethylmethacrylate (HEMA as materials, methacryloxylpropyl trimethoxy siliane as coupling agent, HCl as catalyst, Poly-titania(PMMA-TiO2) nanocomposites and Poly-titania(PMMA-TiO2) nanocomposites were synthesized by sol-gel process.

以盐酸作为催化剂,将钛酸四丁酯水解制备二氧化钛(TiO2)溶胶;随后将所制备溶胶与甲基丙烯酸甲酯、硅烷偶联剂(γ-甲基丙烯酰氧丙基三甲氧基硅烷)相混合,以过氧化苯甲酰作为引发剂,经过聚合、缩合和溶胶-凝胶过程,制备了均匀透明的PMMA-TiO2纳米复合材料和PHEMA-TiO2纳米复合材料。

Following resolution, the following steps are performed: reduce the isomer to an alcohol, react the alcohol with triphenylmethyl chloride, ozonalyze the resulting reaction product, reduce the ozonalyzed product to yield a diol and react the diol with a methane sulfonyl compound to form-3-2-{(methylsulfonyloxy}ethoxy-4--1-butanol methane sulfonate.

拆分后,进行下一步:将异构体还原为醇,使醇与三苯基甲基氯反应,臭氧化所得反应产物,还原臭氧化产物以得到一种二醇并使所述二醇与甲烷磺酰基化合物反应以形成-3-2-{(甲基磺酰基氧}乙氧基-4--1-丁醇甲烷磺酸酯。

In this paper tungstosilicic triethanolamine salt and tungstophoric triethanolamine salt were prepared and used as catalysts in the synthesis of n-butyl lactate ,The synthetic conditions with tungstosilicic triethanolamine salt as catalyst were also examined.

合成了硅钨三乙醇胺盐和磷钨酸三乙醇胺盐,并以它们为催化剂,合成了乳酸正丁酯。

On sand packs consisting of 100 cm~3 quartz of particle size 0.3—0.6 mm, 2 mL kerosene, 1 mL produced water and several drops of isopropyl alcohol, the formulation of LFAR sand consolidation fluid is studied on the basis of the experimental data of compression strength and permeability of the consolidated sand packs and established as follows: 5.0 g LFAR; 0.5 g paratoluene sulfonic acid as curing agent; 5.0 g butyl acet...

在由100cm3粒径0.3~0.6mm的石英砂、2mL煤油、1mL油田污水、几滴异丙醇组成的固砂模型上,根据固结砂的抗压强度和渗透率筛选出了糠醇聚合物固砂剂各组分的用量:糠醇聚合物5g,固化剂对甲苯磺酸0.5g,稀释剂醋酸丁酯5g,后固化剂NaCl+HCl溶液100mL,预冲洗液80mL,后冲洗液80mL。

EMB-resistance in 18 isolates was caused by the mutation at coden 306 in embB gene with positive rate of 62.1%. The PCR result was negative in 20 specimen from pulmonary diseases without active TB and 5 negative control strains of no MTB. The data in this study showed high specificity of 100%. Only one specimen in 7 specimen with negative result in acid-fast stain and cultivation was shown alteration in coden 306 in embB gene.

结果:130例活动性肺结核患者痰标本抗酸染色阳性38例,阳性率为29.2%(38/130);罗氏培养阳性为79例,阳性率为60.8%(79/130)。79例培养阳性痰标本中耐乙胺丁醇29例,其中有18例在embB基因met306ATG突变,基因突变率为62.1%。20例非结核肺部疾病患者痰标本和5株非结核分枝杆菌菌株经套式PCR扩增全部为阴性,特异性为100%。7例涂阴培阴PCR扩增阳性的序列中有1例在embB基因306位密码了发生突变。

Bezaldehyde was used as protective agent in first method.S-Epichloeohydrin was aminated and acidulated to give(2S)-1-Amino-3-chloro-propanol Salts.The acetylation of (2S)-1-Amino-3-chloro-propanol by acetic anhydride produced the intermediate-N-[2--3-chloropropyl]acetamide.And then at 20℃,in the presence of lithium tert-butoxide,benzyl 3-fluoro-4-morpholinophenyl carbamate react with-N-[2--3-chloropropyl]acetamide to give linezolid in total yield of 43.6%.

路线一采用苯甲醛作保护剂,使S-环氧氯丙烷氨解、酸化生成S-1-氨基-3-氯-2-丙醇盐酸盐,然后经乙酰化反应后,生成中间体-N-[2-乙酰氧基-3-氯丙基]乙酰胺,再用N-(3-氟-4-吗啉苯基)氨基甲酸苄酯和中间体在催化剂叔丁醇锂存在下25℃反应生成利奈唑酮,总产率达到43.6%。

Oil and polyol firstly hydrolyze, and then react with maleic anhydride to give semi ester, the residual maleic anhydride hydrolyzing to give maleic acid, finally are adducted with DCPD. The result of experiment shows that the synthesized resin is of perfect air drying performance and improved flexibility and anti-greening because of the use of oil, meetin...

试验结果表明,油与多元醇在210~220℃下先醇解,然后与顺酐反应形成半酯,剩余顺酐水解成顺丁烯二酸,然后与DCPD加成,合成的树脂具有优良的空干性;同时油的使用极大地提高了涂膜的柔韧性和抗绿化性,得到的树脂性能上可满足涂料用不饱和聚酯树脂的要求。

At last,in order to lighten the electrophoretic particles,0.2 g of the succinic acid modified SiO_2 particles were dispersed at 90 ℃ in 50 mL xylene solution dissolving 0.1 g polyethene,cooled and kept for 12 h,and then the particles were encapsuled by PE by means of centrifugal sedimentation at(10 000) r/min.

最后,为降低电泳颗粒密度,将0.2 g经丁二酸改性的S iO2颗粒,于90℃时加入已溶解了0.1 g 聚乙烯的50 mL二甲苯中,冷却静置12 h后,以10 000 r/m in的速度离心,使PE沉积包覆于电泳颗粒表面。

In this thesis, the method of the synthesis of the common intermediate compoundof this style has been further studied. It is confirmed a procedure for esterifying the alanine.

本论文对该类化合物的常用中间体(1)的合成方法进行了改进性试验,避免了使用苄酯或叔丁基酯进行丙氨酸酯化,减少了反应的复杂性,简化了后处理方法。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。