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A novel synthesis route is developed according to the synthesis method of aminoacetic acid in the dissertation.

本文借鉴甘氨酸的合成工艺,设计了一条新的合成路线,简单、高效地制备出1-氨基环丁甲酸。

Methods starting from dimethyl succinate and benzaldehyde, mitiglinide calcium was obtained via 7 chain steps including stobble condensation, hydrolization, anhydration, condensation with cis-hexahydroisoindoline, reduction, separation, salt formation.

方法以丁二酸二甲酯和苯甲醛为原料,经stobble缩合、水解、脱水,与顺-全氢异吲哚缩合后经还原、拆分、成盐等7步反应制得糖尿病治疗药物米格列奈钙。

In the presence of ethanol- HCl solution, arylamine-HCl and w=37% aqueous formaldehyde solution or the condensation product of arylamine and formaldehyde are directly reacted with ethyl 3-oxo-2-phenylmethylenebutyrate to form l-aryl-2-phenyl-3-carbethoxy-4-piperidone.

2-苯亚甲基-3-丁酮酸乙酯与芳香胺和w=37%甲醛水溶液或芳胺和甲醛的缩合物在氯化氢-无水乙醇存在下可直接发生的Mannich反应,得到1-对位取代芳基-2-苯基-3-羰乙氧基-哌啶-4-酮。

Objective To study antioxidation ofDi-(3β-hydroxyandrost-5-en-17-one) ester, a new compound which was structure derivated from active substance from Asterias amurensis.

目的 以兔和大鼠心肌及肝组织匀浆为材料,研究一种从多棘海盘车中提取得到的活性物质经结构改造和修饰得到的丁二酸二-(3β-羟基雄甾5-烯-17-酮)酯新化合物抗脂质过氧化作用。

In 1800 Dom Augustin returned to France, and two years later resumed possession of Val-Sainte.

1800年DOM的奥古斯丁回到了法国,两年后恢复藏缬氨酸-圣。

In 1800 Dom Augustin returned to France, and two years later resumed possession of Val-Sainte.

在奥古斯丁大教堂1800年返回法国,两年后恢复占有缬氨酸圣。

The invention discloses a method for preparing novel nanometer TiO2 optical catalyst material, comprising that (1) preparing gel solution of modified lanthanide series that mixing butyl titanate, alcohol solvent, azotic acid, polyvinyl alcohol and lanthanide element,(2) using alkali liquid to treat the quartz fiber leaked from side wall,(3) using drawing membrane and high-temperature sintering to form modified TiO2 optical catalyst material on the surface of quartz fiber.

本发明公开了一种制备新型纳米TiO2光催化材料的方法,包括(1)配置镧系元素改性的溶胶溶液:将钛酸四丁酯、醇类溶剂、硝酸、聚乙烯醇和镧系元素的盐类混合搅拌;(2)利用碱液对侧壁漏光石英光纤进行处理;(3)通过提拉成膜和高温煅烧,在石英光纤表面形成改性TiO2光催化材料。

The electrochemical behavior of benzalacetophenone has been studied in MeCN.

在此条件下恒电位电解,2,4-二苯基-4-丁酮酸的产率可达88%。

The main intermediates of phenol degradation were benzoquinone and organic acids such as oxalic acid and maleic acid and the final product was carbon dioxide,therefore the technique could be used as a waste minimization process for recycling the treated water.

苯酚降解的主要产物为苯醌、丁烯二酸和草酸,最终产物为二氧化碳,因此该工艺可用于有机物污染最小化处理和处理水的回用。

The influence of microwave radiation on Ullmann reaction has been investigated by three Ullmann reactions, including triphenylamine formed by treating the diphenylamine with bromobenzene or Chlorobenzene which substitutes Iodobenzene; 4,4\'-dimethyltriphenylamine formed by treating 4,4\'-dimethyldiphenylamine with bromobenzene which substitutes Iodobenzene; 4,4\',4-trinitrotriphenylamine formed by treating 4-chloronitrobenzene with p-nitroaniline in this paper.

实验表明,在微波辐射条件下,顺式比反式迈克尔反应活性高;若在丁烯二酸的双键上引入甲基后,降低了进行迈克尔加成反应的活性;引入酯基对双键的影响比腈基有利于进行迈克尔反应,丙烯酸甲酯较丙烯腈的迈克尔反应活性高。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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