丁酸

Two compounds were synthesized with two methods. The two compounds can be synthesized by two steps with triethylamine as catalyst.

分别用氢氧化钠、三乙胺为缚酸剂，3-氨基-2-丁醇、2-氨基-3-戊醇、环己酮和二氯乙酰氯为原料，采用一步法和分步法合成了两种潜在除草剂安全剂。

D. of the catalyst increased, i. e. the acid volume of the catalyst increased, the conversion for isobutene and the selectivity for trimer increased also, while the selectivity for dimer decreased, and the selectivity for tetramer was almost unchanged.

D。增加时，即催化剂的酸量增加时，异丁烯的转化率和三聚物的选择性也增加，但二聚物的选择性降低，四聚物的选择性则几乎没有变化。

Urushiol can be used as the basic raw material to develop economic and practical coating with good resistance to high temperature alkaline solution. Thus the polymer precursor was prepared using the polymerization of urushiol and formaldehyde. Then the urushiol-titanium chelate polymer (urushiol-Ti resin) was synthesized by way of the reaction of tetrabutyl titanate with the polymer precursor. The prospective target product was analyzed by means of high-performance liquid chromatography and Fourier transformation infrared spectroscopy.

为开发经济实用的耐高温碱水漆酚钛清漆，以漆酚为基本原料，先通过漆酚与甲醛缩聚，再将钛酸丁酯与前期合成产物反应，从而合成出了漆酚－钛螯合高聚物，并通过高效液相色谱和傅立叶红外技术检测了预期产物的合成情况。

In this paper, urushiol-Titanium chelate polymer was synthesized through tetrabutyl titanate reacting with the product which is from polymerization between urushiol and formaldehyde, which endows urushiol and Titanium atom with macromolecular performance and functional performance, respectively.

根据其结构特点，本研究利用漆酚先后与甲醛和钛酸丁酯聚合形成高聚物，使得漆酚高分子功能化、钛原子高分子化。

The existing form of boron on the rubbing surfaces is sodium metaborate which can be dissolved in water. The hydration water of so- dium metaborate can reduce the aiitiwear function on Four-ball Machine but enhance its antiwear ability on Timken Tester. The study also revealed that sulfonate dispersant Can reduce the antiwear function of sodium metaborate while succinimide dispersant enhance its antiwear ability.

结果表明，含偏硼酸钠的白油能在摩擦表面形成含偏硼酸钠的表面膜而具有较好的抗磨性，硼在摩擦表面膜中以偏硼酸钠的形式存在，钠和钙的石油磺酸盐型分散剂会降低偏硼酸钠的抗磨性，而丁二酰亚胺类分散剂则能提高其抗磨性。

Started from D-tyrosine, we obtained the tetramic acid 96 using Jouin reaction. The assembly of the second fragment 109 was stared from 1,4-butandiol,using asymmetric alkylation reaction developed by Oppolzer as a key step. Coupling of the tetramic acid 96 with 109 provided the key intermediate 110 according to Yoshii\'s procedure. After remove protective group and Sharpless epoxidation, we obtained the key intermediate 113. Its macrocyclization to form the final product is in progress.

本论文的第二章主要对Macrocidin A开展了合成工作，我们从D构型的酪氨酸出发，经过官能团转换；利用Jouin反应生成Tetramic acid 96，另外一个片断从1，4-丁二醇开始经过多步反应生成碘化物104，利用Oppolzer发展的手性樟脑磺酰胺为辅基参与的不对称烷基化反应，引入手性甲基，生成关键中间体109，接着通过Yoshii发展的方法连接96和109生成110，经过Sharpless不对称环氧化反应建立环氧化合物，然后脱去保护基得到关环前体113，分子内的Mitsunobu反应进行关大环反应正在进行之中。

The quantitation was monitored with an Inertsil ODS-3V column using a mobile phase of methanol- 0.3%acetic acid = 64:36 for TLM and acetonitrile- methanol - 0.3%acetic = 2:64:34 for Z detector set at 254nm.

对托美丁的分析方法是用Inertsil ODS-3V管柱，移动相则采甲醇： 0.3%醋酸为64： 36 ；而对佐美酸的定量亦用相同管柱，移动相为乙晴：甲醇： 0.3%醋酸为2： 64： 34，UV侦测器则同样设定为254 nm。

The resulting polymer electrolyte possesses 1.57×10~(-3) S·cm~(-1) of ionic conductivity at room temperature when it contain 5wt% of LiBF_4 and 1wt% of zwitterion salt.

研究表明Zwitterion型离子液体1-甲基-3-磺酸正丁基咪唑盐，具有较高的熔点和热分解温度，熔点为219℃，分解温度达320℃。

Sodium(3 S,4S)-3-amino-4--2-ox-Oazetidine-1 -sulfonate is its key intermediate, a chiral zwitterion.

手性内盐(3S，4S)-3-氨基-4-氨甲酰氧甲基-2-氧代氮杂环丁酮-1-磺酸钠是卡芦莫南的关键中间体。

Yeast cell rupture conditions by zymolysis were determined with waste brewer's yeast as material and α-amino nitrogen as inspection target.

确定了以啤酒废酵母为原料，酵母酶解液中α-氨基氮含量为考察指标的蜗牛酶酶解破壁条件；并以啤酒废酵母酶解液为有机氮源，厌氧发酵制备丁二酸。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。