丁酸

Isocyanurate was qualitatively identified by infra-red absorption spectroscopy analysis, the quantity of isocyanurate was calculated according to mass fraction of NCO measured by di-n-butylamine method, the thermal stability of prepared elastomers was characterized by thermogravimetric analysis.

用红外光谱法证实了产物中异氰脲酸酯的存在，根据用二正丁胺法测得的NCO基团的质量分数可计算出异氰脲酸酯的质量分数，用热重法分析了产物的热稳定性。

In this thesis, we describe a facile and economical synthesis of-abscisic acid from keto-isophorone and 3-butyn-2-ol through ketalization, oxidization, Witting-Horner reaction, reduction with chromium sulfate and other steps in 13% total yields. Compared to the previous routes, the starting materials are more commercially available and cheaper and the synthetic process is more easily controlled in our method, but the yield of this route is still to be improved.As to isostere principle, cyclopropyl and methyl vinyl are a couple of isostere.

本论文设计并完成了一条全新的外消旋脱落酸(1)全合成路线，从廉价的工业原料氧化异佛尔酮和丁炔醇出发，经过缩酮化反应、氧化反应、Wittig-Horner反应、CrSO_4选择性还原反应以及水解等七步反应实现了脱落酸的全合成，总产率达13％，与以往路线相比，该路线所用试剂廉价、合成路线简单，但产率有待提高。

The antioxidant activity of the lipid-soluble epigaliocatechin-3-0-gallate-4'-myristate in soybean salad oil were investigated and compared in AOM test. Results: The results demonstrated that the antioxidant activity of the single-substitution EGCG myristate was almost corresponding to TBHQ.

结果：该脂溶性的EGCG衍生物为长碳链单取代的儿茶素－表没食子儿茶素－3-0-没食子酸－4'-肉豆蔻酸酯，在大豆色拉油中的抗氧化活性与叔丁基对苯二酚相当。

The above resins are irregular transparent solid which are the products of esterification by pentaerythrite and the adducts of rosin and maleic anhydride.

马林酸树脂又名失水苹果酸树脂，由松香与顺丁烯二酸酐加成反应后并以多元醇酯化而制得的不规则透明粒片状固体。

The normally brominated Baylis-Hillman adducts were formed as the major product at low temperature. While at room temperature or heating, the α,γand β,β-dibrominated compounds were formed as the major products using 3-butyn-2-one and methyl propiolate or propynenitrile as substrate, respectively.

贫电子炔类化合物的Baylis-Hillman反应的研究在这部分工作中我们发现在用TiBr〓或BBr〓为Lewis酸催化贫电子炔类化合物和芳香醛的Baylis-Hillman反应时，温度对反应的影响很大：当反应在低温下进行时，通常生成的是正常的β-溴代的Baylis-Hillman反应产物；而在室温或加热条件下反应，以丁炔酮为底物时，主要生成的是α，γ-二溴化合物，而以丙炔酸甲酯及丙炔腈为底物时，主要生成的是β，β-二溴化合物。

The major organic acids identi-fied in skins and seeds were malic and quinic acids.

相似丁果肉，果皮和种子的主要有机酸也足苹果酸和奎尼酸。

The liner for double-based propellant was prepared from HTPB,toluene diisocyanate,diisooctyl sebacate,1,4-butanediol and mica.

以端羟基聚丁二烯、癸二酸二异辛酯、1，4 丁二醇、绢云母、甲苯二异氰酸酯等为原材料，制备了双基药柱用包覆层。

The density, binding energy and radical distribution function of HTPB/plasticizers blends and binder hydroxyl-terminated polybutadiene, and plasticizer dioctyl sebacate, dioctyl adipate, dibutyl phthalate, dioctylphthalate were calculated by molecular dynamics simulation for evaluating compatibility of HTPB and plasticizers.

为评价端羟基聚丁二烯与增塑剂相容性的优劣，采用分子动力学模拟方法对纯HTPB、增塑剂癸二酸二辛酯、己二酸二辛酯、邻苯二甲酸二丁酯、邻苯二甲酸二辛酯及HTPB与增塑剂组成的共混物的密度、结合能和径向分布函数等进行了计算。

Here, by introducing C-terminally 6xHis-tagged human Nap1 gene into Escherichia coli and exploiting the nickel-charged sepharose gel system to purify the human Nap1 protein, we show that the Nap1 enzyme function is preserved in human as in lower organisms such as bacteria and plants using succinamic acid as the substrate.

此研究中，我们将已在胺基末端接上6个组胺酸标记的Nap1基因表现在大肠杆菌中，并使用接合上镍原子的琼脂糖凝胶纯化出人类Nap1蛋白，再以丁醯胺酸作为受质，证明人类Nap1蛋白具有酵素活性。

In this study, new benzo[l,2,3]thiadiazole derivatives were designed according to relationship of structure and efficacy. The 9 novel compounds were synsthesized with following reactions. The chlorine atom in 2-chloro-3,5-dinitro-benzoic acid as beginning raw material was substituted by 2-methylpropane-2-thiol, esterified then with bromoethane, reduced by iron powder and cyclized to obtain ethyl benzo[l,2,3]thiadiazole-7 after diazonation reation.

本论文根据苯并噻二唑诱导剂的构效关系设计了新的苯并噻二唑的结构，并合成了9个未见文献报道的化合物，合成步骤如下：采用2-氯-3，5-二硝基苯甲酸为起始原料，苯环上的氯原子被叔丁基硫醇置换，羧酸由溴乙烷酯化，硝基由铁粉还原，随后经重氮化关环生成苯并[1，2，3]噻二唑-7-羧酸乙酯。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。