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The invention discloses a method for synthesizing acetyl tributyl citrate, which uses tributyl citrate and acetic anhydride as reaction articles, uses naphthalenesulfonic acid methylal as the catalyst during the ester synthesis process, filtering the catalyst from reacted articles after reaction, water-washing, alkaline-washing, distilling the filtrate to obatin acetyl tributyl citrate.

本发明公开了一种合成乙酰柠檬酸三丁酯的方法,它以柠檬酸三丁酯、乙酸酐为反应物,在酯合成过程中用萘磺酸甲缩醛作催化剂,反应结束后,将催化剂从反应后的物料中过滤出来,滤液经水洗、碱洗、蒸馏获得乙酰柠檬酸三丁酯。

The conditions of manufacture of phytin by ion-exchange resins are also studied,its extract rato is 88 %,but the content of suger and protein is lower,so it is more suitable for inositol preparing.

酸浸取碱中和菲丁提取率达90%~93%,离子交换法菲丁提取率稍低,为88%,但菲丁中糖类、蛋白质含量低,利于进一步制备肌醇。

They are 4-(2- hydroxy-3-butynlenoxy) benzoic acid (1, WA), 5-chloro-7, 8-dihydroxy-7-methyl- 6-oxo-3- [ -3, 4-dihydroxy-3, 5-dimethyl-l-heptylene] -1H-8, 8a-dihydrobenzo [2, 3-c] pyran (2, WB),-2-(2-methyl-2-dibutene diamido)-2-butenoic acid (3, B5262), 3, 4-dihydro-9, 10-dihydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3- c] pyran-1-one (4, A73 semi-Vioxanthin), 8, 8'-bis (6, 9-dioxo-3,4-dihydro-10- hydroxy-7-methoxy-3-methyl-1H-naphtho [2, 3-c] pyran-1-one)(5, A122 Xanthomegnin), 2, 5-dioxo-3a-hydroxymethyl-3, 3a, 6, 6a-tetrahydro-furo [2, 3-b] furan (6, 1003-2), 7-acety1-5-chloro-6, 8-dioxo-7-methyl-3- [ -3, 5-dimethyl-1, 3- diheptylene] -4aH-benzo [2, 3-c] pyran (7, M2-2 sclerotiorin), respectively.

它们分别被命名为4-(2-羟基-3-丁炔氧基)苯甲酸(1,WA)、5-氯-7,8-二羟基-7-甲基-6-氧代-3-[-3,4-二羟基-3,5-二甲基-1-庚烯基]-1H-8,8a-二氢苯并[2,3-c]吡喃(2,WB)、-2-(2-甲基-2-丁烯二酰亚胺基)-2-丁烯酸(3,B5262)、3,4-氢-9,10-二羟基-7-甲氧基-3-甲基-1H-萘并[2,3-c]吡喃-1-酮(semi-Vioxanthin,4,A73)、8,8'-双(6,9-二氧代-3,4-二氢-10-羟基-7-甲氧基-3-甲基-1H-萘并[2,3-c]吡喃-1-酮)(Xanthomegnin,5,A122)、2,5-二氧代-3a-羟甲基-3,3a,6,6a-四氢-呋喃并[2,3-b]呋喃(6,1003-2),7-乙酰基-5-氯-6,8-二氧代-7-甲基-3-[-3,5-二甲基-1,3-庚二烯基]-4aH-苯并2,3-c]吡喃(Sclerotiorin,7,M2-2)。

Water,butylene glycol,biosaccharide gum-1,ppg-26-buteth-26,panthenol,peg-40 hydrogenated caster oil,hydroxyethylcellulose,imidazolidinyl urea,saccharide isomerate,benzophenone-4,phenoxyethanol,triethanolamine,citrus aurantium dulcisoil,pentadecalactone,methylparaben,sodium hyaluronate,citric acid,butylparaben,ethylparaben,citrus aurantium amaraoil,propylparaben,methylchloroisothiazolinone,methylisothiazolinone,red 4,yellow 5,red 33,limonene,linalool

水,丁二醇,多醣物质,PPG-26-丁醇聚醚-26,维生素B5,PEG-40氢化蓖麻油,羟乙基纤维素,尿素醛,天然异构寡糖,二苯甲酮- 4,苯氧乙醇,三乙醇胺,甜橙油,环十五内酯,羟苯甲酯,透明质酸钠,柠檬酸,羟苯丁酯,羟苯乙酯,苦橙油,羟苯丙酯,甲基氯异塞唑晽酮,甲基异噻唑啉酮,红4,黄5,红33,柠檬精油,芳樟醇

In present study, a liquid-liquid extraction method was employed to extract the volatile components in mulberry fruit sparkling wine. The analysis with gas chromatography-mass spectrometry detected 69 peaks, among which 63 volatile components were identified. The first 9 volatile components with high relative content were benzyl alcohol, 2-methyl-1-butanol, mono-(2-ethylhexyl)-1, 2-benzene dicarboxylic acid, 3-methyl-1-butanol, toluene, acrylic acid butyl ester, 1H-indole-3-ethanol, isodecyl octyl phthalate and decyl octyl phthalate.

采用液-液萃取法提取桑椹汽酒中的挥发性成分,经气相色谱-质谱联机分析,共检测出69个峰,鉴定出63种挥发性化合物,其相对含量排在前9位的挥发性化合物分别是苯乙醇、2-甲基-1-丁醇、1,2-苯二酸单(2-乙基)己酯、3-甲基-1-丁醇、甲苯、丙烯酸丁酯、1H-吲哚-3-乙醇、邻苯二甲酸异癸基辛基二酯、邻苯二甲酸癸基辛基二酯。

The n-butyl lactate was synthesied by the esterification of lactic acid and n-butyl alcohol in presence of ammonium ferric sulfate dodecahydrate NH4Fe(SO4)212H2O,and the factor influencing on the yield of reaction were discussed.

摘 要:在十二水合硫酸铁铵催化下,由乳酸和正丁醇发生酯化反应合成了乳酸正丁酯。实验考察了该催化剂催化酯化合成乳酸正丁酯的醇酸比、催化剂用量、反应时间、反应温度诸因素对酯化率的影响。

In recent years, the company excellent location advantages, multi-introduction of advanced production equipment and technology to improve old products and develop new products to 12 - hydroxy acid-based rigid and at the same time the production of refined castor oil, hydrogenated castor oil, refined Gan oil, Sebacate methacrylate (annual output 1500 tons), dibutyl sebacate (annual output 1500 tons), octyl sebacate, anhydrous sodium sulfate, castor meal and other products.

近年来,公司以优越的区位优势,多方引进先进的生产设备和技术,改进旧产品,拓展新产品,以 12 -羟基硬质酸为主,又同时生产精炼蓖麻油、氢化蓖麻油,精甘油,癸二酸二甲酯(年产量 1500 吨),癸二酸二丁酯(年产量 1500 吨),癸二酸二辛酯,无水硫酸钠,蓖麻粕等产品。

The logarithm difference values of partition coefficients of the compounds in butyl ether/water and in cyclohexane/water system were used for the measurement of the Lewis acidity, while the logarithm difference values of partition coefficients in trichloromethane/water and in tetrachloromethane/water system were used for the measurement of the Lewis basicity, and they were used successfully to differentiate the relative strength of Lewis acidity and basicity for 59 benzene and its derivates.

以化合物在正丁醚/水和环己烷/水溶剂体系中分配系数的对数差作为酸性指数,以其在氯仿/水和四氯化碳/水溶剂体系分配系数的对数差作为碱性指数,提出了一种新的度量有机物Lewis酸碱性的方法,按此方法成功地区分了59种苯系物Lewis酸碱性的相对强弱;并成功地将上述酸碱性指数引入定量结构—性质/活性相关研究之中,探讨了苯系物的正辛醇/水分配系数、水溶解度和土壤有机碳吸附系数等常见理化性质与其Lewis酸碱性间的相关性并建立了相应的定量模型,发现它们之间存在良好的相关性。

A four-ball tester was used to evaluate the load carrying and antiwear properties of bismuth dibutyldithiocarbamate,bis-dibutyldithiocarbamates(V7723),sulfurized isobutylene,molybdenum ester non sulfur and phosphorus in a mineral oil respectively and their synergistic effects.

利用四球试验机评价了二丁基二硫代氨基甲酸铋与二丁基二硫代氨基甲酸酯(V7723)、硫化异丁烯和非硫磷钼酸酯添加剂的极压和抗磨性能,以及它们之间的极压和抗磨协同作用。

Cytarabine microcapsules were prepared using sodium alginate and chitosan by high-voltage electrostatic droplet generator.

采用海藻硅酸钠和几丁聚糖为原料制备海藻酸钙-几丁聚糖药物缓释微胶囊,初步考察了载阿糖胞苷微胶囊的制备以及不同分子量几丁聚糖、静/动态载药方式对阿糖胞苷释放性能的影响。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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