丁胺

The existing form of boron on the rubbing surfaces is sodium metaborate which can be dissolved in water. The hydration water of so- dium metaborate can reduce the aiitiwear function on Four-ball Machine but enhance its antiwear ability on Timken Tester. The study also revealed that sulfonate dispersant Can reduce the antiwear function of sodium metaborate while succinimide dispersant enhance its antiwear ability.

结果表明，含偏硼酸钠的白油能在摩擦表面形成含偏硼酸钠的表面膜而具有较好的抗磨性，硼在摩擦表面膜中以偏硼酸钠的形式存在，钠和钙的石油磺酸盐型分散剂会降低偏硼酸钠的抗磨性，而丁二酰亚胺类分散剂则能提高其抗磨性。

It can also used as material to produce suffocating reagent, pesticide, antiseptic and weedicide.

在我国多聚甲醛主要用于生产草甘磷和丁草胺等除草剂，也用于涂料、医药、合成树脂和造纸等领域。

Started from D-tyrosine, we obtained the tetramic acid 96 using Jouin reaction. The assembly of the second fragment 109 was stared from 1,4-butandiol,using asymmetric alkylation reaction developed by Oppolzer as a key step. Coupling of the tetramic acid 96 with 109 provided the key intermediate 110 according to Yoshii\'s procedure. After remove protective group and Sharpless epoxidation, we obtained the key intermediate 113. Its macrocyclization to form the final product is in progress.

本论文的第二章主要对Macrocidin A开展了合成工作，我们从D构型的酪氨酸出发，经过官能团转换；利用Jouin反应生成Tetramic acid 96，另外一个片断从1，4-丁二醇开始经过多步反应生成碘化物104，利用Oppolzer发展的手性樟脑磺酰胺为辅基参与的不对称烷基化反应，引入手性甲基，生成关键中间体109，接着通过Yoshii发展的方法连接96和109生成110，经过Sharpless不对称环氧化反应建立环氧化合物，然后脱去保护基得到关环前体113，分子内的Mitsunobu反应进行关大环反应正在进行之中。

Copolymers with the naphthoyimine chromophores were firstly obtained through Pd-catalyzed Heck reaction. The copolymers had good solubility in common solvents due to the presence of alkoxyl substituents in the molecular chains.

在钯催化下利用Heck耦合反应制备了以萘酰亚胺为发色团的共聚物，通过侧链上引入丁氧基醚链，使得聚合物具有很好的溶解度，能溶解在常用有机溶剂中。

RESULTS:In the case of ambient temperature cefoxitin with etamsylate is in compatibility steady-state both in compatible content and outward stability (P＞0.05) within 6h;cefoxitin with aminomethylbenzoic acid or adrenochromazone is in compatibility steady-state (P＞0.05) within 4h;cefoxitin with aminocaproic acid varies in compatible content (P＜0.05) after 4h.

结果：在室温条件下，头孢西丁与酚磺乙胺在0～6 h内含量(P＞0.05)和外观稳定，但pH值有变化(P＜0.05)；与氨甲苯酸、安络血在0～4 h内稳定(P＞0.05)；与氨基己酸配伍有变化(4 h后P＜0.05)。

One synthetic strategy started fromγ-butyrolactone 38, from which a cyclohexadiene intermediate 30 was prepared in an overall yield of 44% in a 7-step procedure after y-butyrolactone underwent a-bromination, dehydrobromination, Diels-Alder reaction, aminolysis, benzylation, bromination and dehydrobromination, with the key step being the Diels-Alder reaction under harsh condition.

其中一个路线从γ-丁内酯38开始，连续经过α-溴化、脱溴化氢、Diels-Alder反应、胺解、苄基化、溴化和脱溴化氢共7步反应，制备了一个环己二烯衍生物30，总产率44％，关键步骤是高温高压下Diels-Alder反应。

It pointed that along with the development of the automobile industry,more regulations related to energy economy and environment protection coming into being and the increase of execution strength of those regulations,the environment-friendly and energy-saving boracic lubricating oil additives etc.will be widely used.Particularly,the market potential of bononized succinimide is huge.

指出随着中国汽车工业的发展，环保、节能法规的不断出台与执行力度的加大，含硼等环保、节能型润滑油添加剂将得到广泛的使用，其中硼化丁二酰亚胺市场潜力巨大。

Results: Time and concentration of poison dying all had effect on the myocardial contracts dint and myocardial enzymogram of Bufo bufo gargarizans.

结果：除草剂丁草胺的染毒时间和浓度均可影响蟾蜍心肌收缩力和心肌梅谱。

NaZSM-5 zeolites were modified by impregnation with metal nitrate and their catalytic properties for gas phase reaction of γ-butyrolactone and ethanolamine to give intermediate N-hydroxylethyl pyrrolidonewere studied.

采用金属盐溶液浸渍的方法对NaZSM-5分子筛进行改性，考察了ZSM-5分子筛对γ-丁内酯与乙醇胺之间气相反应合成N-羟乙基吡咯烷酮的催化性能。

In this paper isopropyl -γ- chlorobutyrate was prepared from γ- butyrolactone by one - step. The effects of molar ratio of reactants, reaction temperature, reaction time on the yield of product were discussed, the optimum reaction condition was obtained.

一氯代丁酸异雨酯是合成新型拟除虫菊酯中间体环丙烷较酸及高效抗菌新药丙氟见酸和环丙氟院酸中间体环丙胺的重要原料［''］。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。