丁烯酸

During the reaction of alkylation, general contained 0.2%~2.0% butadiene will produce viscous heavy composite materials, which will raise final boiling point of alkylate and decrease octane, what is more, it will react with acid to produce corresponding ester, which will increase the consumption of acid, Therefore, we must remove butadiene by selective hydrogenation, at the same time, it will convert some of 1- butane to 2- butane by isomerization and raise octane of alkylate.

一般含有0.2%~2.0%的丁二烯，其在烷基化反应中，可生成一种分子量很高的粘稠重质迭合物，使烷基化油的干点升高，辛烷值降低，并且它还和酸反应生成相应的酯而加大酸耗量。因此必须经过选择性加氢除掉丁二烯，同时，将部分1-丁烯异构化为2-丁烯，以提高烷基化油的辛烷值。

In their structures, polyanions are bridged by Ln ions via the coordination of the bridging oxygen atoms and terminal oxygen atoms, forming a W–Ot′–Ln–Ob–W linkage; and through the W–Ot′–Ln–Ob–W linkage a one-dimension infinite linear chain with alternating cations and anions is formed.

在相似的合成条件下，我们向原有体系内加入顺丁烯二酸作为有机配体，合成了化合物7，其7的基本结构和化合物1-6很相似，但有一个顺丁烯二酸阴离子取代了一个NO3-离子的位置。

Utilization ofantiseptic would not be affected by temperature or pH.The antiseptics had a longperiod of validity,the effect is much better than most other antiseptics,could notarose skin hypersusceptibility,resist to metabolization,and had a wide utilizationrange.

研究中采用了本实验室自行合成的抗菌剂反丁烯二酸桂醇甲酯，测定了反丁烯二酸桂醇甲酯在不同的pH值、不同温度、不同浓度条件下的抑菌活性、抑菌谱，并与其它常用抗菌剂的抑菌效果做了比较。

Chromatography peaks were obtained by GC-MS and 56 compounds were identified. The main components were linalyl butyrate (30.212%),(1α, 3α, 4β, 6α)-4,7,7-trimethyl-bicycloheptan-3-ol (10.940%),-4-carene (1.826%), 4-methylene-1-(1-methylethyl)-bicyclo [3.1.0] hexane (1.109%),β-myrcene (1.170%), limonene (5.784%), 3, 7-dimethyl-1, 6-octadien-3-ol (5.742%), n-hexadecanoic acid (0.914%) and-9, 12-octadecadienoic acid (2.952%), etc.

用GC-MS分离出69个峰，鉴定出56种物质，主要成分为：芳樟丁酸酯(30.212%)、(1α， 3α， 4β， 6α)-4，7，7-三甲基－双环[4.1.0]庚烷－3-醇(10.940%)、-4-蒈烯(1.826%)、4-亚甲基－1-（1-甲基乙基）－双环[3.1.0]环己烷(1.109%)、β-月桂烯(1.170%)、柠檬烯(5.784%)、3，7-二甲基－1，6-辛二烯－3-醇(5.742%)、n-棕榈酸(0.914%)、-9，12-十八碳烯酸(2.952%)等。

Given the current complexity of industrial recovery of 3'-methyl-2'-butenyl 3, 3-dimethyl-pentenoate and the decomposition problems with 2-methyl-1-butene, research was conducted on a process for direct recycling of MBDP involving an ester exchange reaction of MBDP with either methanol, trimethyl orthoacetate, or solutions of methanol and trimethyl orthoacetate.

针对目前工业上回收3，3-二甲基－4-戊烯酸－3'-甲基－2'-丁烯酯工艺复杂、异戊烯大量分解问题，研究了MBDP直接返回循环使用工艺，MBDP与甲醇、原乙酸三甲酯或与甲醇原乙酸三甲酯混合溶液进行酯交换反应的回收新工艺，比较了四异丙基钛酸酯、甲醇钠、氢氧化钾用作酯交换催化剂的效果，筛选出回收MBDP&一锅煮&最佳工艺：按照n：n：n：n＝1.0：9.8：9.2：0.05物质的量比投料，74℃~78℃反应21h，MBDP转化为贲亭酸甲酯和异戊烯醇，单程转化率87.7%，用85%的磷酸中和甲醇钠，蒸出甲醇，直接用于合成贲亭酸甲酯。

Synthesis technology of cinnamyl methyl fumarate containing α,β-unsaturated carbonyl group and its antimicrobial activity was studied.

以α，β-不饱和羰基结构为母体设计合成反丁烯二酸桂醇甲酯，并对反丁烯二酸桂醇甲酯的抗菌活性进行了研究。

Applied dodecencylsuccinic acid and diethanolamine as raw materials,dodecencylsuccinic acid diethanolamide was prepared.

以十二烯基丁二酸(T746)和二乙醇胺为原料合成了十二烯基丁二酸二乙醇酰胺防锈剂，探讨了原料质量配比、反应温度、反应时间等对产品性质的影响。

Professional sales companies operating bromide products: sodium bromide, sodium bromide, potassium bromide, potassium bromate, Tetrabromobisphenol A, Deca-BDE, ten PBDEs, DBDPE, hexabromodiphenyl Central dodecane, dibromo neopentyl glycol, neopentyl bromide three alcohols, three bromine phenol, octabromodiphenyl ether, brominated polystyrene, bromide, calcium bromide, dibromo succinic acid, dibromo-D ene glycol, bromide surfactants series: Dodecyl trimethyl ammonium bromide, tetradecyl trimethyl ammonium bromide, cetyltrimethyl ammonium bromide, octadecyl trimethyl ammonium bromide dodecyl trimethyl ammonium chloride, tetradecyl trimethyl ammonium chloride, cetyl trimethyl ammonium chloride, octadecyl trimethyl ammonium chloride, tetrabutyl ammonium bromide wholesale sales: dimethylolpropionic acid, DL-malic acid, isophthalic acid PIA, glycolic acid, adipic acid.

公司专业经营销售溴化物系列产品：溴化钠、溴酸钠、溴化钾、溴酸钾、四溴双酚A、十溴二苯醚、十溴联苯醚、十溴二苯乙烷、六溴环十二烷、二溴新戊二醇、三溴新戊醇、三溴苯酚、八溴醚、溴化聚苯乙烯、溴化铵、溴化钙、二溴丁二酸、二溴丁烯二醇、溴化表面活性剂系列：十二烷基三甲基溴化铵、十四烷基三甲基溴化铵、十六烷基三甲基溴化铵、十八烷基三甲基溴化铵、十二烷基三甲基氯化铵、十四烷基三甲基氯化铵、十六烷基三甲基氯化铵、十八烷基三甲基氯化铵、四丁基溴化铵批发销售：二羟甲基丙酸、DL-苹果酸、间苯二甲酸 PIA、羟基乙酸、己二酸。

Niobic acid; catalytic synthesis; di-2-ethylhexyl phthalate; di-n-octyl phthalate; di-2-ethylhexylmaleate; di-n-octyl maleate; cyclohexene; modification of catalyst; dynamics of esterification

工程科技I，化学，有机化学铌酸；催化合成：邻苯二甲酸二辛酷；邻苯二甲酸二异辛酯；顺丁烯二酸二辛酯：顺丁烯二酸二异辛酯：环己烯；改性；动力学

Firstly, headspace solid-phase microextraction was established to determine AITC by orthogonal design. Extraction temperature, stir speed, extraction time, and desorption time were set at 40℃, 900r/min, 30min, and 5min, respectively. Under these optimal conditions, volatile flavor compounds in mustard oil, wasabi, and 'Chongcai'leaf mustard product were identified by SPME/GC/MS. In these three samples, 6,12,17 constituents were identified respectively; Allyl isothiocyanate was the main flavor compound, which accounted for 73.45%, 64.25%, 32.74% of total volatile compounds, respectively. Carbon disulfide, a hydrolysis product of AITC, accounted for 14.37% 25.40%, 51.67% of total volatile compounds respectively. There were some other isothiocycannates, such as butane, 1-isothiocyanato-, isobutyl isothiocyanate, 1-benzene, 4-isothiocyanato-, benzene (2-isothiocyanatoethyl)-, etc.

首先采用正交实验设计优化固相微萃取技术的前处理条件，结果表明，以萃取温度40℃、搅拌速度900r／min、萃取时间30min、解吸时间5min为最佳条件；在此最优条件基础上，利用SPME／GC／MS联用技术分析芥末油、青芥辣、冲菜的挥发性风味成分，分别检出6、12、17种化合物，主要风味物质均为AITC，相对丰度分别为73.45％、64.25％、32.74％；AITC的水解产物二硫化碳的相对丰度分别为14.37％、25.40％、51.67％；还检测到了其它几种异硫氰酸酯，如异硫氰酸丁酯、异硫氰酸异丁酯、异硫氰酸丁烯酯、2-苯乙基异硫氰酸酯等。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。