丁烯

In the paper,the essential oil of Syringa oblate Lindl var affinis Lingelsh bud from Qinghai was extracted by the method of water vapor distillation. After detected by GC-MS,47 peaks were separated from the oil. Among them,26 compounds taken up 88.7% of total peak areas were identified.

采用水蒸气蒸馏法提取了产自青海的白丁香花蕾的挥发油，应用GC/MS方法对其化学成分进行了分析，分离出47个色谱峰，鉴定了26个化合物，占总峰面积的88.7%，主要成分是丁香酚、丁香醇、石竹烯、苯乙醇等化合物。

The results showed that there were 8 kinds of aliphatic, 5 kinds of esters, 2 kinds of aldehydes, 2 kinds of nitrogen sulfur heterocyclic rings and one kind of hydrocarbon, alcoholics, ketone, lactones respectively in the analyzed 21 kinds of aroma components, and the content of furfural,β-methyl valeric acid, palmitic acid, nicotine, neohytadiene were higher, next were acetyl ethyl propionate, caleric acid, phenyl ethyl acetate, hydroxylic diethyl succinate.

结果表明，在分析出的21种香气成分中，分别有脂肪酸类8种，酯类5种，醛类2种，氮硫杂环类2种，烃类、醇类、酮类、内酯类各l种，其中相对含量较高的物质成分是糠醛、β-甲基戊酸、十六碳酸、烟碱、新植二烯，其次是乙酰丙酸乙酯、异戊酸、苯乙酸乙酯、羟基丁二酸二乙酯等。

It starts with an aldol-type condensation in which a solution of the now commercially available E -[3-(4-fluorophenyl)-1-(1-methylethyl)-1 H-indol-2-yl]-2-propenal, 4 , 5 in THF is added to the preformed sodium-lithium salt of tert -butyl acetoacetate 5 at room temperature in THF.

它从一个醛型缩合其中一个解决现在的电子商业可-[3-(4-fluorophenyl)-1-(1-methylethyl)-1吲哚-2-基]-2-丙烯醛、4，5年增加了预四氢呋喃钠-锂盐叔丁基乙酰四氢呋喃在常温5。

In this paper, the synthesis ways and applications of 4,5-dimethyl-l,3-dioxolen -2-one were introduced. An appropriate way synthesizing DMDO from acetoin via acylation, cyclization and dehydrochlorination was selected. The influences of various process conditions on the reaction were studied in detail, and the optimum process conditions were obtained by single factor experiments.

本文介绍了医药中间体4，5-二甲基-1，3-二氧杂环戊烯-2-酮的应用情况和合成路线，选择了适于工业化生产的工艺路线，即采用羟基丁酮为原料，经酰化、环合和脱氯化氢等步骤合成DMDO，并采用单因素试验法详细研究了各项工艺条件对反应结果的影响规律，确定了优化工艺条件。

A method to synthsis a - methylene - r - butyrolactones was reported by the substituted (a - carbethoxyvinyl) cuprate intermediates, generated by the addition of higer order cuprate to acetylenic ester,traping with epoxides stereoselectively.

本文报道了通过以高序铜代替低序铜对炔酸酯加成得到的取代铜与端基或环状环氧化合物的立体选择性反应，较高产率的合成α，β-取代烯酯，进而可合成α-亚烷基-γ-丁内酯类衍生物。

The catalytic system composed of NHPI and transition metal ion can catalyze effectively ethane into acetic acid,cyclane into dicarboxylic acid,toluene into benzoic acid,alkene into epoxide,alkyne into acetylenic ketone,and amide into imide;NHPI used alone can catalyze adamantane to be carbonylated,hydrogen peroxide prepared by oxidization alcohol;NHPI combined with as...

NHPI与过渡金属离子组成的催化体系能高效地催化乙烷氧化为乙酸、环烷烃氧化为二元羧酸、甲苯氧化为苯甲酸、烯烃氧化为环氧化物、炔烃氧化为炔酮、酰胺氧化为酰亚胺；NHPI单独使用能催化金刚烷发生氧化羰基化反应、催化氧化醇制取过氧化氢；NHPI与有机助催化剂如偶氮二异丁腈、溴化季铵盐、蒽醌和醇等也能催化分子氧氧化反应。

Alkenyl succinic acidas an anti-rust additive is generally used in steam turbine oil .

分别测定了含烯基丁二酸的汽轮机油/蒸馏水及汽轮机油/合成海水体系的界面张力、界面剪切粘度、油相粘度及乳状液稳定性。

One synthetic strategy started fromγ-butyrolactone 38, from which a cyclohexadiene intermediate 30 was prepared in an overall yield of 44% in a 7-step procedure after y-butyrolactone underwent a-bromination, dehydrobromination, Diels-Alder reaction, aminolysis, benzylation, bromination and dehydrobromination, with the key step being the Diels-Alder reaction under harsh condition.

其中一个路线从γ-丁内酯38开始，连续经过α-溴化、脱溴化氢、Diels-Alder反应、胺解、苄基化、溴化和脱溴化氢共7步反应，制备了一个环己二烯衍生物30，总产率44％，关键步骤是高温高压下Diels-Alder反应。

Objective To study antioxidation ofDi-(3β-hydroxyandrost-5-en-17-one) ester, a new compound which was structure derivated from active substance from Asterias amurensis.

目的 以兔和大鼠心肌及肝组织匀浆为材料，研究一种从多棘海盘车中提取得到的活性物质经结构改造和修饰得到的丁二酸二-（3β-羟基雄甾5-烯-17-酮）酯新化合物抗脂质过氧化作用。

Titanium silicalite 1(TS 1)with different crystal size s were synthesized in the system of TPABr n butylamine by adjusting the formation of gel and the method of crystallization.

在四丙基溴化铵正丁胺体系中合成不同晶粒大小的TS 1沸石，采用IR、XRD UV Vis、SEM、2 7AlMASNMR对其进行表征，并以丙烯环氧化反应为探针考察其催化性能。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新