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After esterification, the ethyl-2-chloro-3-phenylpropionate reacts with diethyl malonate under the catalysis of sodium ethylate, and we obtain the corresponding triethyl ester. The-benzylsuccinic acid is formed by the triethyl ester reacting with concentrate hydrochloric acid and taking place hydrolyzation and decarboxylation reaction at the same time. In order to avoid the formation of cinnamic acid, the sodium ethylate and diethyl malonate must be react sufficiently. The course has simple operation, inexpensive materials and better yield.

具体制备工艺为:首先以L-苯丙氨酸为原料采用重氮化方法得到-2-氯-3-苯基丙酸,再经酯化得到-2-氯-3-苯基丙酸乙酯后在乙醇钠催化作用下和丙二酸二乙酯缩合,发生SN2反应,得到相应的三乙酯,然后经水解和脱羧,得到-苄基丁二酸;在实验中乙醇钠要和丙二酸二乙酯充分反应,避免生成肉桂酸乙酯;该过程操作简单,原料便宜,产率较高,总收率可达到26.8%。

Of others elsewhere in other times who, kneeling on one knee or on two, had kindled fires for him, of Brother Michael in the infirmary of the college of the Society of Jesus at Clongowes Wood, Sallins, in the county of Kildare: of his father, Simon Dedalus, in an unfurnished room of his first residence in Dublin, number thirteen Fitzgibbon street: of his godmother Miss Kate Morkan in the house of her dying sister Miss Julia Morkan at 15 Usher's Island: of his aunt Sara, wife of Richie Goulding, in the kitchen of their lodgings at 62 Clanbrassil street: of his mother Mary, wife of Simon Dedalus, in the kitchen of number twelve North Richmond street on the morning of the feast of Saint Francis Xavier 1898: of the dean of studies, Father Butt, in the physics' theatre of university College, 16 Stephen's Green, north: of his sister Dilly in his father's house in Cabra.

40他联想到旁的时候在旁的地方跪着单膝或双膝曾经替他生火的其他那些人;迈克尔修士,在坐落于基尔代尔郡塞林斯的耶稣会克朗戈伍斯公学校医院的病房里。他父亲西蒙。迪达勒斯,在菲茨吉本街门牌十五号那间没有家具等设备的屋子里,而那是他在都柏林的头一个住所。他的教母凯特。莫坎小姐--住在厄谢尔岛她那奄奄一息的姐姐朱莉姬。莫坎小姐家里。他的舅妈萨拉--里奇。古尔丁的妻子,在他们那坐落于克兰布拉西尔街门牌六十二号寓所的厨房里。他的母亲玛丽--西蒙。迪达勒斯的妻子,那是在北里奇蒙街门牌十二号的厨房里,时间是一八九八年圣方济各。沙勿略节日的早晨。副教导主任巴特神父,在"斯蒂芬草地"北区门牌十六号的大学物理实验室里。他的妹妹迪丽,在他父亲那坐落于卡布拉的家里。

In Moss Landing, a huge natural gas power plant owned by Dynegy spews dirty gray smoke, called flue ( a pipe or tube that takes smoke, gas or hot air away from a fire, a heater or an oven ) gas.

在加州摩斯兰丁,「戴那基」公司拥有的一座巨大天然气电厂喷出污浊,名为烟道废气的灰烟。

According to several years practice, comprehensively sum up measures of forcing culture technology of scale and dwarf on potted Bougainvillea as: a propagation of cuttage, which choose a mixture of 50%peat, 33% vermiculite and 17 sharp sand as cutting soil, and choose a semi-wooden shoot cut into 5~10cm length with 2~3 leaves as cuttings then touch 1% AA root powder, is lower cost and higher survival rate than that of tissue culture; Bougainvillea growth can be efficaciously regulated by pruning and using 2~5g/L PP333; bougainvillea can be induced to flowers by spraying 2.5~4.0g/L B9 and administering no more 11 hours daylight every day continuously; the florescence can be more prolonged about 20 days by spraying 50mg/L NAA while selling; and prevention and cure of pest and disease, etc.

根据多年的生产实践,从科学育苗、栽培管理、售前处理和病虫害防治等方面综合总结了叶子花的规模化矮化促成生产技术措施:选择泥炭土、蛭石和黄沙按3:2:1比例混合均匀的扦插基质,采用半木质化当年生枝条,剪成5~10cm长的2~3叶节一段,沾染1%自制生根粉的扦插育苗较组培育苗成本低,成活率高;结合修剪用2~5g/L的多效唑进行叶面喷洒能有效控制生长,矮化植株;选择2.5~4.0的丁酰肼叶面喷洒和每天保持不多于11h的短日照处理,能有效促进开花;销售前全株喷洒脱50mg/L NAA可延长花期20天左右;整个生产过程加强肥水管理、温湿度控制和环境清洁能有效防治病虫害发生。

This phrase, together with several differences in musical text between the four-hand reduction of 1875 and the full score, led the French critic M.

这段话以及1875年两人的缩编本与完整的总谱在很多地方的不同使得法国批评家卡沃雷西指责里姆斯基—科萨耶夫和格拉祖诺夫在鲍罗丁死后非法改写他的作品。

Some authors whose books are available in full text online include Jane Austen, Charles Dickens, and Fyodor Dostoevsky.

有的作家的书可在网上全文包括奥斯丁、狄更斯、fyodor杜斯妥也夫斯基。

Second, among the seven yeast strains investigated, Rhodotorula gracilis AS 2.499 exhibited the highest activity and stereo-selectivity to tert-butyl-6-chloro-5-hydroxy-3-oxohexanoate.

其次,从实验室保藏的七株酵母菌株中筛选出对-6-氯-5-羟基-3-羰基己酸叔丁酯具有较高还原能力的菌株——Rhodotorula gracilis AS 2.499。

Joel, who was Kim Grant's second signing, started his career at Southend United before going on loan to Gravesend and Northfleet in the 2006/07 season, where he made some half a dozen starts. In the summer of 200, Jim Smith took him to Oxford United on a two-year deal, where he played alongside the Cards' Assistant Coach, Phil Gilchrist. In February 2008, Joel went on loan to Hayes and Yeading and left Oxford by mutual consent at the end of last season.

1987年9月29日出生,吉姆-格兰特签入的第二名球员,在索森德联队开始职业生涯,随后在2006/07赛季被租借到格拉维森和诺斯福利特,有6次左右的首发出场。2007年夏天吉姆-史密斯将他带到了牛津联队,并签订了2年合同,在那里与现任沃金队助理教练菲尔-基尔克莱斯特是队友。2008年1月,乔尔被租借到海耶斯和耶丁,并在赛季结束后在双方同意的情况下离开了牛津联队。

The Venetians received 3/8 of Constantinople and important commercial and naval stations throughout the empire: the ports of the Marmora and Hellespont, most of the Aegean, Crete, Koroni, Modon, Dyrrachium, the Ionian Islands, etc.

威尼斯人接收了3/8的君士坦丁堡城区,以及整个帝国重要的商业和海军据点:马尔马拉海和赫勒斯滂海峡、绝大部分的爱琴海域、克里特岛、克罗尼、摩顿和底拉基乌姆。

In view of rising feedstock and energy costs, BASF will further increase prices for its acrylic acid and acrylic esters (glacial acrylic acid; methyl acrylate, ethyl acrylate, n-butyl acrylate, 2-ethyl hexyl acrylate), as contracts permit.

在原料和能源成本,巴斯夫公司将进一步提高其丙烯酸和丙烯酸酯(冰丙烯酸,丙烯酸甲酯,丙烯酸乙酯,丁酯丙烯酸2乙基己基丙烯酸酯),价格为合同许可。

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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。

This is not paper type of business,it's people business,with such huge money involved.

这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。