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Aim To study the relationship between the structures of a series of 4,4-diaryl-3-butenyl derivatives of nipecotic acid and guvacine and their inhibition activity of the γ-aminobutyric aciduptake.

目的研究3-哌啶甲酸和四氢烟酸的4,4-二芳基-3-丁烯衍生物结构和对γ-氨基丁酸摄取抑制活性之间的关系。

The conversion of isobutyraldehyde and the selectivity to 2,4,6-triisopropyl-1,3,5-trioxane were 91.1% and 99.8% respectively under optimum reaction condition isobutyraldehyde 25.0 g, [Et3NH]Cl/FeCl3 ( x (FeCl3)=0.62 1.0 g, 25 ℃ for 1 h .

在最佳的反应条件下(异丁醛25.0 g, [Et3NH]Cl/FeCl3 x (FeCl3=0.62 1.0 g, 25 °C,N2保护下反应1 h,异丁醛的转化率为91.1%,对2,4,6-三异丙基-1,3,5-三氧噁烷的选择性达99.8%。

Meanwhile the chapter made some interesting analysis of the relationship between Marx and Aeschylus, Spartacus, Martin Luther, Dante, Cervantes, Shakespeare, Balzac, Danidl Defoe, Voltaire, Rousseau, Diderot, Goethe, Schiller, Immanuel Kant, Fichte, Hegel, Feuerbach, Hess, Friedrich Engels, Saint-Simon, Fourier, Robert Owen, P. Trémaux,Comte, N.

同时本章还就埃斯库罗斯、斯巴达克、马丁·路德、但丁、塞万提斯、莎士比亚、巴尔扎克、笛福、伏尔泰、卢梭、狄德罗、歌德、席勒、康德、费希特、黑格尔、费尔巴哈、赫斯、恩格斯、圣西门、傅立叶、欧文、达尔文、比·特雷莫、孔德、弗列罗夫斯基等人与马克思的关系做了有趣的分析。

Ethyl alcohol, 3-methyl-4-oxo- pentanoic acid, acetic acid butyl ester, 2-methyl-butanoic acid ethyl ester, diethyl phthalate,-2,4-Decadienal were the same volatiles d from the 10 cultivars.

其中共有组6种,为乙醇、3-甲基-4-羰基戊酸、乙酸丁酯、2-甲基丁酸乙酯、邻苯二甲酸二乙酯、-2,4-癸二烯醛。

Results: Nine compounds were obtained from the ethyl acetate fraction of C. speciosa and were identified as methyl chlorogenate, 5-O-cafeoyl quinic acid butyl ester, quinic acid butyl ester, 5-hydroxymethyl-furan-2-carbaldehyde, triacontanoic acid,-epicatichin, 7,8-dihydroxy-coumanrin, protocatechuic acid ethyl ester, and protocatechuic acid.

结果:从皱皮木瓜的乙酸乙酯萃取部位分离鉴定了9种化合物,分别为绿原酸甲酯,5-O-咖啡酰基-奎宁酸丁酯,奎宁酸丁酯,5-羟甲基-2-糠醛,三十烷酸,-表儿茶素,7,8-二羟基香豆素,3,4-二羟基苯甲酸乙酯,原儿茶酸。

And the PLA/Chitosan/ACP barriers with additional 2 wt% chitosan still maintain 56.58 % antibacterial ability after eightieth day. The different composition of PLA/Chitosan/ACP composites was prepared by water washing solidification from NMP/water/lactic acid consolvent. After storing at room temperature for 48 hours and taking it out to obtain a shapable composites. To investigate the influence of ratio of composition with the shapable property of composites, it was analyzed by Rheometer, TGA, AFM, XRD. The result of the different APC content had different effect both water content and yield stress of composite materials. The yield stress decreased with ACP content while increases. It was derived that ions, released from ACP interact with amide groups of chitosan to form water-absorbing ionic clusters through chelating or electrostatic attraction.

另外,以聚乳酸/几丁聚醣作为基材并添加不同比例的非晶型磷酸钙,经过水洗固化后可得白色片状沉淀物,於室温下静置48小时后,复合材之体积呈现膨胀且具有可塑形之特性,以热重分析仪与流变仪分析样品之含水率与屈伏应力,结果显示不同ACP含量对复合材含水率与屈伏应力具有消长变化,而PLA/Chitosan/ACP之可塑程度与其所吸收之水份多寡有关,推测可能机制为ACP磷酸钙盐解离后之金属离子与几丁聚醣之胺基透过螯合作用或静电吸引之交互作用,形成具吸水性之离子团簇分散於疏水性之聚乳酸基材中。

A high molecular weight polyisobutenyl succinimide dispersant with high nitrogen content and good thermal and oxidative stabilities was developed.

采用氯化烃化工艺和后偶联反应技术开发了一种氮含量高、热稳定性和氧化稳定性好的高相对分子质量的聚异丁烯基丁二酰亚胺分散剂。

But the electrochemical results show that complexes exhibitcompletely irreversible redox behaviour which is different from thatfound in diiron proteins. 1.3 To obtain the diiron species which are stable to elec-trochemical reduction, a series of new tetranuclear cage ironspecies containing two 〓 cores, with using hexadentatepolybenzimidazole ligands, were synthesized and characterized by vari-ous spectroscopic methods. Their physical properties have been investi-gated. The crystal structures of 〓〓tetrakis (benzimidazol-2-ylmethyl)-1, 4-diaminobutane and 〓,〓-tetrakis ( N-ethylbenzimidazol-2-ylmethyl )-1, 4-diaminobutane were determined. They contain two 〓 cores which arelinked to each other by -〓-chain in the ligands.

1.3为了获得电化学还原稳定双核氧桥联Fe化合物,使用六齿配体合成了一系列含有两个〓单元四核笼状化合物,并用各种谱学手段表征了它们,还研究了它们的物理化学性质确定了〓L=N,N,N',N'-四(苯骈咪唑基-1,4-丁二胺和〓,〓四-1,4-丁二胺化合物的晶体结构,它们含有两个〓单元,其中两个〓单元是通过配体的〓链桥联成四核笼状结构。

In this work,the non\|aqueous carbonyl nickel slips were prepared by ball\|milling using Cyclohexanone\|butyl alcohol,Glycerol trioleate,Poly\|vinyl\|butyl and polyethylene glycol as the solvent,dispersant,binder and plasticizer,respectively.

本文以环己酮丁醇为溶剂,三油酸甘油酯为分散剂,以聚乙烯醇缩丁醛为粘结剂,聚乙烯乙二醇为增塑剂,通过球磨工艺制备了非水基羰基镍粉浆料。

The methyl pheophorbide-a (5) was oxidized with osmium oxide and sodium periodate to give chlorin 8 which was converted into aldehyde purpure-18 (9) and purpure-7 trimethyl ester (10) by air-oxidation in butanol in the presence of sodium.

选用四氧化锇和高碘酸钠将5氧化成卟吩醛(8),在丁醇中以丁醇钠作催化剂, 8的氧化和重排反应给出3-甲酰基紫红素-18酯(9)和紫红素-7三甲酯衍生物10。

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The labia have now been sutured together almost completely.The drains and the Foley catheter come out at the top.

此刻阴唇已经几乎完全的缝在一起了,排除多余淤血体液的管子和Foley导管从顶端冒出来。

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为了做成这笔生意,我建议我们在价格上大家各让一半。

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