丁基

Objective To evaluate and compare the ability to detect tumor by bis (N-ethoxy-N-ethyl dithiocarbamato) nitrido 99mTc [ 99mTcN 2 ] and 99mTc hexakis-2- methoxyisobutyl isonitrile [ 99mTc-MIBI ].

目的 探讨99mTc-氮-二(N-乙基-N-乙氧基二硫代氨基甲酸盐)[99mTcN2]应用于肿瘤诊断的可能性并与99mTc-甲氧基异丁基异腈(99mTc-MIBI)肿瘤模型显像进行比较。

By combining resolution and protection of DBSPINOL with menthyl chloroformate, the enantiopure SPINOL and other 4,4'-derivatives have been synthesized effectively via (1S)--4,4'-dibromo-l,r-spirobiindane-7,7'-diyl bis-menthyl carbonate with n-BuLi following reacting with electrophiles of I2, MeI, CO2 and water.

在制备其它衍生物反应中，薄荷醇碳酸酯成为羟基的保护基，DBSPINOL碳酸酯用正丁基锂处理后，再和亲电试剂作用合成了其它4，4'位二碘代、二甲基取代和二羧基取代SPINOL新化合物。

The regiochemistry for the ring opening of monocyclic cyclobutylcarbinyl radicals could be easily predicted by the relative stability of the two possible carbon radical products.

单环环丁基甲基自由基重排反应的区域选择性很容易判断，只需要比较两种碳自由基产物的相对稳定性即可。

For the above purposes, using a tailored cyanometalate precursor,(1) Tp=hydrotris (pyrazolyl borate; Bu〓N〓=tetrabutylammonium cation , two trinulear complexes,〓(2),〓(3; cyclam: 1, 4, 8, 11-tetraazacyclotetradecane), two one-dimensional polymers,〓(4; dien: diethylenetriamine),〓(5), and a cluster 〓(6) have been synthesized and characterized structurally and magnetically.

基于上述研究热点，我们以修饰的氰基金属化合物(1)为构筑基元（Tp：三吡唑基氢硼烷，Bu〓N〓：四丁基铵离子），合成了两个杂三核化合物，〓(2)，〓（3；cyclam：1，4，8，11-四氮环十四烷），两个一维聚合物，〓（4；dien：二乙烯三胺），〓(5)，和一个十四核簇合物〓(6)。

Two azobenzene-containing polyethers were synthesized and their thermotropic liquid crystalline properties were investigated.

氯乙基缩水甘油醚和GCE/羟丁基乙烯基醚分别通过阳离子聚合、光引发共聚合，获得两种聚醚，然后再分别与 4-硝基-4' -羟基偶氮苯反应，制备了两种侧链含偶氮苯生色团的液晶聚合物。

In this study, new benzo[l,2,3]thiadiazole derivatives were designed according to relationship of structure and efficacy. The 9 novel compounds were synsthesized with following reactions. The chlorine atom in 2-chloro-3,5-dinitro-benzoic acid as beginning raw material was substituted by 2-methylpropane-2-thiol, esterified then with bromoethane, reduced by iron powder and cyclized to obtain ethyl benzo[l,2,3]thiadiazole-7 after diazonation reation.

本论文根据苯并噻二唑诱导剂的构效关系设计了新的苯并噻二唑的结构，并合成了9个未见文献报道的化合物，合成步骤如下：采用2-氯-3，5-二硝基苯甲酸为起始原料，苯环上的氯原子被叔丁基硫醇置换，羧酸由溴乙烷酯化，硝基由铁粉还原，随后经重氮化关环生成苯并[1，2，3]噻二唑-7-羧酸乙酯。

In order to obtain versatile ulitity of host molecules, three new chiral calix [4] crown ethers containing aza, thio atoms bearing two chiral sites provided by -cysteine ester were synthesized by the condensation of calix [4] arene diacid dichloride with oligoethylene glycol bridged bis-amino acid methyl ester. All new compounds were characterized by NMR, MS and elemental analysis.

以-半胱氨酸为手性源，利用多甘醇二氯醚在碱性条件下对半胱氨酸巯基进行烷基化反应，成功地合成了多甘醇醚链桥联的半胱氨酸衍生物，醚化反应后，在高度稀释条件下与对叔丁基杯[4]芳烃二乙酰氯进行双功能基缩合反应成功地合成了新型的手性杯[4]含氮、硫杂冠醚，并利用〓H NMR、MS等谱图手段对其结构进行了表征。

A novel lead ionselective polyvinyl chloride membrane electrode was prepared using 25,27di(2thiadiazolethiooxyethyl)26,28dihydroxyl5,11,17,23tetraptertbutylcalix[4]arene as the ionophore. The influences of the nature of plasticizers and the amounts of the incorporated ionophore and ionic additive on the response characteristics of the electrode were studied.

制备了以25，27二(2噻二唑基硫代乙氧基)26，28二羟基5，11，17，23四叔丁基杯\[4\]芳烃为载体的聚氯乙烯膜铅离子选择电极；研究了电极膜中增塑剂种类及载体和离子定域体含量对电极性能的影响。

Synthetic nitro-musks are used in the most wide area recently and industrial crystallization is the most important process to separate solid mixtures such as perfumes. In order to develop new crystallization process to separate synthetic nitro- musks, the phase equilibrium of musk ketone, musk xylene and 1,3-dimethyl-2, 4- dinitro-5-tert- butyl benzene were studied.

合成硝基麝香是用量最大的合成麝香而工业结晶是分离香料等固体产品的重要方法，为了开发麝香体系结晶分离新工艺，本文首先研究了酮麝香、二甲苯麝香和1，3-二甲基-2，4-二硝基-5-叔丁基苯的相平衡关系。

The separation of neutral macrocyclic calyx [4] pyrroles with 1-butyl-3-methylimidazolium chloride as background electrolyte in acetonitrile was carried out by nonaqueous capillary electrophoresis.

建立了以1-丁基－3-甲基咪唑氯盐离子液体为背景电解质，非水毛细管电泳分离中性大环化合物八甲基杯[4]吡咯、四环戊基杯[4]吡咯、四环己基杯[4]吡咯的方法。

We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称；三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起，称之为挽歌体诗人或者史诗诗人，他们被称为诗人，似乎只是因为遵守格律写作，而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。