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The catalyst includes: supported Ziegler-Natta catalyst of titanium halide compound and organic electron donor compound supported with MgCl2 alcoholate carrier; aluminoxane prepared with trialkyl aluminum and water; and one kind of organic electron donor, such as organosilicon compound R2Si(OCH3)2, where R is phenyl, isopropyl, isobutyl or cyclopentyl.

该催化剂包括,a一种负载型的Ziegler-Natta催化剂,即将卤钛化合物和有机给电子体化合物负载在氯化镁醇合物载体上得到的固体催化剂,b一种通过三烷基铝与水反应而制备得到的铝氧烷和c一种有机电子给体,如有机硅化合物R 2 Si(OCH 3 ) 2 ,其中R为苯基、异丙基、异丁基或环戊基。

The oxydation products of some of the secondary alcohols was shown to be ketones. The conjugation of three tertiary alcohols, butyl, amyl and hexyl, was higher than that of the corresponding primary and secondary alcohols.

某些二级乙醇氧化产物表明是酮。3种三位乙醇的接合,丁基,戊基和已基,比对应初级和二级乙醇更高。

Herein, a 13C NMR study of the LHBPEs is presented. Short branches such as methyl, ethyl, propyl, butyl and amyl were assigned and quantified.

本文主要对LHBPE进行13C NMR研究,并对聚合物分子的支链如甲基、乙基、丙基、丁基和戊基等进行归属和定量研究。

The Molar conductivity indicates that all the complexes are nonelectrolyte. IR spectra show the ligand is bonded with RE ion through its oxygen atom in hydroxyl group of phenol; NO3 is coordinated as a symmetrical chelating bidentate group; the coordinated atoms of DMF and DMSO are the oxygen atoms in carbonyl and sulfoxyl groups. Fluorescence spectrum suggests that the Tb3+complexes have characteristic luminescence and its fluorescence intensity is enhanced after doping with La3+, Gd3+, Y3+, influence of doping ions and neutral ligands have also been discussed.

摩尔电导率表明,所有配合物均为非电解质;红外光谱及核磁共振氢谱表明,对叔丁基杯[8]芳烃通过酚羟基的氧原子与稀土离子配位;硝酸根为双齿螯合配位;DMF和DMSO则分别通过羰基氧和亚砜基氧与稀土离子配位;配合物的荧光光谱表明,所有Tb的配合物具有较强的特征荧光,掺杂La~(3+)、Gd~(3+)、Y~(3+)离子对Tb~(3+)的荧光有较强的增强作用。

In the synthesis process of ligands and their rare earth complexes, metal lithium is used to substitute for n-butyllithium, such as the synthesis of fluorenyl lithium, piperonal dimethyl acetal lithium, and bis (9-fluorenyl) silylene lithium.

合成配体和配合物的中间体均采用金属锂代替正丁基锂,如芴锂、溴代胡椒醛二甲基缩醛基锂盐、甲基苯基双芴基硅烷双锂盐的制备,方法简单,操作简便,副反应少,且锂盐的浓度和用量易于控制。

The charomatographic conditions of separation and direct dermination of benzophenone-4(MS40), salizyle acid sodium, salol, benzophenone-3(M40), octyl dimethyl PABA(6007), butyl methoxy dibenzoyl methane(1789), octyl methoxyl cinnamate and octyl salicylate(587) from u-Bondapak C18 Column were studied with methanol-water-THF as elution. A HPLC method for these compounds was founded.

研究了用甲醇-四氢呋喃-水作为流动相,从C18柱上分离和测定羟苯甲酮-5-磺酸(MS40)、水杨酸钠、水杨酸苯酯、羟苯甲酮(M40)、对-二甲酸氨基苯甲酸-2-乙基己酯(6007)、4-叔丁基-4-甲氧基二苯甲酸甲烷(1789)、对-甲氧基肉桂酸-2-乙基己酯、水氧酸-2-乙基己酯(587)等8种紫外线吸收剂的色谱条件,建立了用HPLC测定上述物质的方法。

The influences of temperature and scan rate on the electrochemical characteristics of nitromethane were also investigated by using cyclic voltammetry.

采用循环伏安等测试方法,以铂微盘电极为工作电极,研究了硝基甲烷在离子液体1-正丁基-3-甲基咪唑四氟硼酸盐(BMImBF4)中的电化学行为,并探讨了温度和扫描速率等因素对硝基甲烷电化学特性的影响。

As compared to isop, the coexistence of electron-donating -OH,-C(CH_3_3 or electron-withdrawing groups (-NO_2) groups in the dicarboxylate derivatives has a significant effect on the molecular self-assembly.

同间苯二甲酸相比较,含有取代基的5-羟基间苯二甲酸、5-硝基间苯二甲酸和5-叔丁基间苯二甲酸在一定程度上影响着配位聚合物的自组装。

A series of acrylic resins were synthesized by using ditertiary butyl peroxide as a free radical initiator and 2-mercaptoethanol as a chain transfer agent.

以过氧化二叔丁基为自由基引发剂、巯基乙醇为链转移剂,合成了高固体分、低粘度的羟基丙烯酸树脂,其粘度在1000mPa·s以下,固体分高达65%~70%。

Both catalytic activity and selectivity of Ru(PPh_3)_3Cl_2 were improved in ionic liquid BMImPF_6/DME medium.The conversion of hexene and selectivity ofβ-adduct for the hydrosilylation reaction of 1-hexene with triethoxysilane catalyzed by Ru(PPh_3)_3Cl_2 in ionic liquid BMImPF_6DME (V/V=1/4) medium at 90℃were 100% and 89.0%,respectively.

实验结果表明,在乙二醇二甲醚/离子液体1-丁基-3-甲基咪唑六氟磷酸盐(BMImBF_6)(V/V =1/4)介质中,于90℃下,己烯与三乙氧基硅烷反应的转化率为100%,β加成物的选择性可达89.0%,而用Rh(PPh_3)_3Cl作为反应的催化剂,在纯离子液体BMImPF_6中,就可以高效催化烯烃与三乙氧基氢硅烷的加成反应,过渡金属Rh(PPh_3)_3Cl,Ru(PPh_3)_3Cl_2催化剂/离子液体BMImPF_6催化体系,不仅解决了产物与催化剂分离困难这一难题,同时,离子液体BMImPF_6的存在提高了过渡金属Rh(PPh_3)_3Cl,Ru(PPh_3)_3Cl_2催化硅氢加成反应的活性,特别是β加成物的选择性。

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We have no common name for a mime of Sophron or Xenarchus and a Socratic Conversation; and we should still be without one even if the imitation in the two instances were in trimeters or elegiacs or some other kind of verse--though it is the way with people to tack on 'poet' to the name of a metre, and talk of elegiac-poets and epic-poets, thinking that they call them poets not by reason of the imitative nature of their work, but indiscriminately by reason of the metre they write in.

索夫农 、森那库斯和苏格拉底式的对话采用的模仿没有一个公共的名称;三音步诗、挽歌体或其他类型的诗的模仿也没有——人们把&诗人&这一名词和格律名称结合到一起,称之为挽歌体诗人或者史诗诗人,他们被称为诗人,似乎只是因为遵守格律写作,而非他们作品的模仿本质。

The relationship between communicative competence and grammar teaching should be that of the ends and the means.

交际能力和语法的关系应该是目标与途径的关系。

This is not paper type of business,it's people business,with such huge money involved.

这不是纸上谈兵式的交易,这是人与人的业务,而且涉及金额巨大。