丁二酸

Through the coupling of cyclen and homoserine deriva-tive, we have firstly synthesized a cyclen-functionalized ?α-amino acid,-2-amino-4[1 (1, 4, 7, 10 –tetraazacyclo-dodecane)] butanoic acid.

我们通过1，4，7，10-四氮杂十二烷与高丝氨酸衍生物反应，首先合成了一个非天然α-氨基酸：-2-氨基-4[1(1，4，7，10-四氮杂环十二烷)]丁酸。

They were eucalyptol, bicyclo［2.2.1］heptan-2-one,1,7,7-trimethyl-,(1R)-, borneol, 1-methyl-2-(1-methyl ethenyl)-(1R-cis)-cyclobutaneethanol, limonene, 1-hydroxymethyl-7,7-dimethy lbicyclo［2.2.1］heptan-2-one,-spathulenol, 3,7,11,15-Tetramethyl-2-hexadecen-1-ol, isocitronellol,-9-Octadecenoic acid, heneicosane, respectively.

阿给中共有11个阿给炭没有检测出的成分，包括桉油精、D-樟脑、冰片、(1R-cis)- 1-甲基-2-(1-甲基乙烯基)环丁基乙醇、二戊烯、1-羟甲基-7，7-二甲基-双环［2.2.1］庚-2-酮、-匙叶桉油烯醇、3，7，11，15-四甲基-2-十六碳烯-1-醇、异香茅醇、-9-十八碳烯酸和廿一烷。

Using dichloropinacolone as starting material, ruthenium dioxide/celite as catalyst and sodium hypochlorite as oxidant, 3,3-dimethyl-2-oxo-butyric acid is prepared through hydrolization and oxidation two reaction steps.

以二氯频哪酮为起始原料， RuO2/Celite 为催化剂， NaOCl 作氧化剂，经水解、氧化两步反应制得3，3-二甲基-2-氧代丁酸。

In this Ph. D. dissertation, reverse microemulsion method was fully used infabricating and modifying polyacrylamide with functional and high-relative moleculeweight. The copolymerization of 2-acrylamide-2-methylpxopanesulfonic acid, fluorescent monomer 4-methoxy-N-(2-N\', N\'-dimethylamino ethyl)naphthalimide alkyl chloride quaternary ammonium salt, fluorescentmonomer 4-(N\'-methyl-1-piperazinylallyl)-N-butyl-naphthalimide chloride quaternaryammonium salt, Cationic monomer dimethylethylammonium bromide and hydrophobical monomer octadecylacrylate with acrylamide and properties of the copolymers werestudied. The interaction between five polymers and Al_2O_3(012) crystal surface have beensimulated by Materials Studio 3.0 program package, binding energies and non-bondinteraction energies and deformation energies have also been acquired.

本文以制备具有较高相对分子质量和功能型PAM为研究目的，将反相微乳液法运用到其制备及改性的有关环节，通过反相微乳液聚合工艺，将几种改性功能单体2-丙烯酰胺基-2-甲基-丙磺酸、荧光单体2-(4-甲氧基-1，8-萘二甲酰亚胺基)-乙基二甲基烯丙基氯化铵、荧光单体4-(N'-甲基-1-哌嗪基)-N-丁基-1，8-萘烯丙氯季铵盐、阳离子单体丙烯酰氧乙基-二甲基-乙基溴化铵和疏水单体丙烯酸十八酯与AM共聚，制备AMPS改性PAM、荧光示踪型PAM、阳离子单体DMB改性PAM和OA改性PAM等四类不同功能单体改性PAM，并研究其应用性能。

In order to carry out the separation of the azeotropic mixture dipropyl ether + 1-propyl alcohol by extractive distillation, we are studied the influence on the phase equilibria behavior four different solvent: 1-pentanol [2], butyl propionate [3], N,Ndimethylformamide [4] and 2-ethoxyethanol.

为了用萃取性蒸馏法分离二丙醚和1－丙醇组成的共沸混合物，我们正在研究4种不同溶剂对相平衡行为的影响：1-戊醇[2]、丙酸丁酯[3]、N，N－二甲基甲酰胺[4]和2-乙氧基乙醇。

As can be seen in Fig. 5, dipropyl ether will be recovered in the distillate using 1-pentanol, N,N-dimethylformamide and 2-ethoxyethanol as entrainers and butyl propionate is the only entrainer studied that inverts the volatility of the azeotropic mixture.

从图 5可以看出，使用1-戊醇、N，N-二甲基甲酰胺和2-乙氧基乙醇作为共溶剂时二丙醚将在馏分中回收，丙酸丁酯是唯一与共沸混合物挥发性相反的共溶剂。

The extracted components were qualitatively and quantitatively analyzed by gas chromatography mass spectrometry.The results showed that 30,26 compounds were identified from the volatile components extracted by DSE,SDE methods resp.36 kinds of components were extracted by 2 methods in total,among them the content of hexadecanoic aci...

结果表明，从DSE、SDE法提取的挥发性成分中分别鉴定出30(总含量58.24μg/g)、26种化合物总含量(86.66μg/g，2种方法共提取出36种化合物，其中十六酸含量最高，其次为亚油酸、油酸、邻苯二甲酸二异丁酯、间甲苯甲醛、龙脑。

Isopropyl 1,3 benzodioxolane was synthesized from catechol and isobutyric aldehyde using the phosphotungstic acid supported on activated carbon as catalyst.

以邻苯二酚和异丁醛为原料，活性炭固载磷钨酸为催化剂合成了杀虫剂呋喃丹的中间体2 -异丙基- 1，3-苯并二氧五环。

This paper confirmed that the microcapsule from sodium alginate and which is used in carbonless copy paper by single cogulation process owns higher embedding ratio and better nonpermeability stableness and strength.

本文对以海藻酸钠为壁材、以结晶紫内酯的邻苯二甲酸二丁酯溶液为芯材通过单凝聚法制备无碳复写纸用微囊的工艺条件进行了研究，制定了工艺路线和流程，确定了最佳的乳化条件、絮凝条件、固化条件以及壁材浓度、芯壁比，并对成品微囊进行了应用性的对比分析。

The liquefied Japanese cedar was blended with PMDI (poly-4, 4'-diphenylmethane diisocyanate), and adding water as a blowing agent, organosiloxane as a surfactant and dibutyl tin dilaurate as a catalyst to prepare the polyurethane foams. The effects of the kind and dosage of surfactant and the molar ratio of NCO/ for PMDI to liquefied Japanese cedar on the properties of PU foams were investigated.

Don； Japanese cedar进行液化处理，所得液化柳杉进一步与异氰酸酯PMDI混合，并添加水为发泡剂，有机矽氧烷为界面活性剂，二月桂酸二丁锡为催化剂制造聚胺基甲酸酯发泡体，探讨界面活性剂种类、添加量及PMDI与液化柳杉之NCO/莫耳比对所制造PU发泡体性质之影响。

On the other hand, the more important thing is because the urban housing is a kind of heterogeneity products.

另一方面，更重要的是由于城市住房是一种异质性产品。

Climate histogram is the fall that collects place measure calm value, cent serves as cross axle for a few equal interval, the area that the frequency that the value appears according to place is accumulated and becomes will be determined inside each interval, discharge the graph that rise with post, also be called histogram.

气候直方图是将所收集的降水量测定值，分为几个相等的区间作为横轴，并将各区间内所测定值依所出现的次数累积而成的面积，用柱子排起来的图形，也叫做柱状图。