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Acenaphthene was dehydrogenated to afford acenaphthylene by photochemical reaction with N bromosuccinimide in benzene with the addition of quinoline at room temperature and atmospheric pressure was studied.

在常温常压下,以苯作为溶剂,加入喹啉,使苊与N-溴代丁二酰亚胺发生光化学脱氢反应生成苊烯。

Ingredients:Water、Collagen、Palmitoyl Pentapeptide、Sodium Hyaluronate、Seamollient、Gamma-Polyglutamic Acid、Evening Primrose Oil、Squalene、Algin、Aescufos、Arbutin、Tranexamic Acid、Myoxinol、Eyeseryl、Idebenone、Olive Extract、Vitamin E、Cetyl Alcohol、Glyceryl Monostearate、1-3butylene Glycol、Glycerin、Methyl Paraben、Perfume.

产品成份:去离子水、胶原蛋白、五胜肽、玻尿酸、海藻黏多醣体、纳豆聚麸胺酸、月见草油、海鲛鲨、藻胶、七叶树、熊果素、传明酸、六胜肽、四胜肽、艾地苯橙、橄榄萃取、维他命E、棕榈醇、单硬脂酸甘油酯、丁二醇、丙三醇、羟苯丙酯、香精。

Objective To evaluate the protection of ulinastatin combined with ofloxacin to diamine oxidase of intestinal mucosa in pyemic rats.

目的 通过检测大鼠肠黏膜中的二胺氧化酶,来评价乌司他丁复合氧氟沙星对脓毒症大鼠肠黏膜的保护作用。

Technical characteristics and existing problems of cyanide-free silver plating technology were summarized through the analysis of cyanide-free silver plating systems of thiosulfate,succinimide,iodide,hydantoin,sulfite and others.

通过对硫代硫酸盐、丁二酰亚胺、碘化物、乙内酰脲、亚硫酸盐以及其它无氰镀银体系的分析,总结了当前无氰镀银工艺的技术特点及存在的问题,并阐述了无氰镀银技术的发展历程和研究现状。

Totally two formulas are designed,one using four compositions and the other including five,while butadiene imide emulsifier is applied by both of the formulas.

该系列乳化炸药包括SEM-4型四组分和SEM-5五组分两种产品,二者均采用一种以丁二酰亚胺为主要成分的高分子复合乳化剂。

Cytotoxic effect was demonstrated with nitrogen mustard, nitromin, sarcolysin, thio-TEPA and myleran at concentrations of 7, 10, 25, 35, 100, and 100μg/ml respectively.

氮芥及氧化氮芥在7—10微克/毫升,溶肉瘤素和新恩必恨于25—35微克/毫升,三乙酰硫代磷酰胺和丁二醇二甲磺酸酯在100微克/毫升,都出現了显著的細胞毒作用,使細胞很快死亡溶解;但6-巯基嘌吟和氨基喋吟未表現作用。

The effect of N-bromosuccinimide on the activity of Escherichia coli arginyltRNA synthetase was studied.

用N-溴代丁二酰亚胺对大肠杆菌精氨酰tRNA合成酶中的五个色氨酸残基进行化学修饰研究,发现酶分子所含的五个色氨酸残基中有一个可以被。。。

Interactions between zinc dialkydithiosphate and succcinimide dispersants synthesized by different feeds and processes were investigated through changes in solutions behaviors, as determined by viscometry, infrared spectrometer, mass spectrometry and chemical analysis.

借助红外光谱、紫外光谱、粘度、浊度等分析测试方法,考察了用不同的原料和工艺合成的丁二酰亚胺无灰分散剂与 ZDDP 的相互作用。

The existing form of boron on the rubbing surfaces is sodium metaborate which can be dissolved in water. The hydration water of so- dium metaborate can reduce the aiitiwear function on Four-ball Machine but enhance its antiwear ability on Timken Tester. The study also revealed that sulfonate dispersant Can reduce the antiwear function of sodium metaborate while succinimide dispersant enhance its antiwear ability.

结果表明,含偏硼酸钠的白油能在摩擦表面形成含偏硼酸钠的表面膜而具有较好的抗磨性,硼在摩擦表面膜中以偏硼酸钠的形式存在,钠和钙的石油磺酸盐型分散剂会降低偏硼酸钠的抗磨性,而丁二酰亚胺类分散剂则能提高其抗磨性。

Started from D-tyrosine, we obtained the tetramic acid 96 using Jouin reaction. The assembly of the second fragment 109 was stared from 1,4-butandiol,using asymmetric alkylation reaction developed by Oppolzer as a key step. Coupling of the tetramic acid 96 with 109 provided the key intermediate 110 according to Yoshii\'s procedure. After remove protective group and Sharpless epoxidation, we obtained the key intermediate 113. Its macrocyclization to form the final product is in progress.

本论文的第二章主要对Macrocidin A开展了合成工作,我们从D构型的酪氨酸出发,经过官能团转换;利用Jouin反应生成Tetramic acid 96,另外一个片断从1,4-丁二醇开始经过多步反应生成碘化物104,利用Oppolzer发展的手性樟脑磺酰胺为辅基参与的不对称烷基化反应,引入手性甲基,生成关键中间体109,接着通过Yoshii发展的方法连接96和109生成110,经过Sharpless不对称环氧化反应建立环氧化合物,然后脱去保护基得到关环前体113,分子内的Mitsunobu反应进行关大环反应正在进行之中。

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