丁二胺

Synthesis and Crystal Structure of One Novel Three-dimensional Supramolecular Compound [Ni(H_2O)_6] ·2·4H_2Ofum= fumarate ; hmt=hexamethylenetetramine

一种新的三维超分子化合物[Ni(H_2O)_6·]2·4H_2O的合成和晶体结构(fum=反丁烯二酸根；hmt=六次甲基四胺)英文

The baseline separation of 9 neutral compounds (thiourea, benzene, toluene, ethyl benzene, n-propylbenzene, naphthalene, n-butylbenzene, fluorene and anthracene) and 7 acidic, basic and neutral compounds (thiourea, o-aminophenol, phenol, benzene, o-methylaniline,α-naphthylamine, 2,4-dichloroaniline) can be obtained under optimized capillary electrochromatographic conditions.

在该均相硅胶基质整体柱上成功地分离了9种中性物质(硫脲、苯、甲苯、乙基苯、正丙苯、萘、正丁基苯、芴和蒽)以及7种中性、酸性和碱性物质(硫脲、邻氨基酚、苯酚、苯、邻甲苯胺、α-萘胺和2，4-二氯苯胺)。

The auxiliary can be recovered in high yield (81%) only by filtering and recrystallization. Besides, some other aldehydes have been chosen to test the enantioselectivity of N,N\'-dibenzyl tartamide, in comparison with two other allylaborates reagents developed previously by Roush and Brown, respectively. The results show that %e.e. of homoallylic alcohol is superior to that of the former, and approaches the Brown reagent.

产物经S_N2反应得瑞格列萘中间体-甲基烯丙基-2-氯苯基-叠氮甲烷(17)；同时，将筛选出的新型手性配体N-苄基酒石酸二酰胺用于其他几种醛(正丁醛，异戊醛和环己醛)的不对称烯丙基化反应，并与广泛应用的Roush配体(22)和Brown配体(27)相比较，发现其立体选择性优于Roush配体，并接近Brown配体，但明显具有可回收利用的优势。

The same is carried out in the microwave, ethanol, dichloroethane, sodium carbonate, tetrabutylammonium iodide ammonium dissolved in dimethylformamide, then access to carbon dioxide.

同样是在微波炉中进行，把乙醇，氯乙烷，碳酸钠，四丁基碘化铵溶解在二甲基甲酰胺中，再通入二氧化碳。

Objective:To evaluate the effect of dobutamine stress echocardiography teston detection of myocardial ischemia.

目的：研究大剂量多巴酚丁胺二维超声心动图诊断冠心病的价值。

Two compounds were synthesized with two methods. The two compounds can be synthesized by two steps with triethylamine as catalyst.

分别用氢氧化钠、三乙胺为缚酸剂，3-氨基-2-丁醇、2-氨基-3-戊醇、环己酮和二氯乙酰氯为原料，采用一步法和分步法合成了两种潜在除草剂安全剂。

The preparation of 2,2-dimethyl-3-hydroxy propanal from the condensation of formaldehyde and i-butyraldehyde by using triethylamine as catalyst was studied.

以异丁醛和甲醛为原料，三乙胺为催化剂，羟醛缩合法合成了2，2-二甲基－3-羟基丙醛。

One synthetic strategy started fromγ-butyrolactone 38, from which a cyclohexadiene intermediate 30 was prepared in an overall yield of 44% in a 7-step procedure after y-butyrolactone underwent a-bromination, dehydrobromination, Diels-Alder reaction, aminolysis, benzylation, bromination and dehydrobromination, with the key step being the Diels-Alder reaction under harsh condition.

其中一个路线从γ-丁内酯38开始，连续经过α-溴化、脱溴化氢、Diels-Alder反应、胺解、苄基化、溴化和脱溴化氢共7步反应，制备了一个环己二烯衍生物30，总产率44％，关键步骤是高温高压下Diels-Alder反应。

GC-MS is used to determine content of free TDI, reaction kinetics is analysed by chlorhydric acid/n-dibutyl amine titration -NCO method and DSC, so the system activation energy is calculated.

采用气相色谱-质谱法测定其游离TDI含量，用盐酸-正二丁胺滴定-NCO法和DSC法相结合，分析反应动力学规律，计算体系表观活化能。

Good thermal stability, High mechanical strength.Used as catalyst or catalyst carrier in the manufacturing of the important industrial products, such as cyanuramide, benzene anhydride, maleic acid anhydride, butadiene rubber, acrylic nitrite, etc.

用途：本产品在三聚氰胺、苯酐、顺丁烯二酸酐、顺丁橡胶、丙烯腈等重要工业品生产中用作催化剂及催化剂载体，也广泛用于石化产品的精制脱除芳烃，也可用于有机气体、液体的选择性吸附分离及离子交换脱除水中多价有害元素等。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。