丁二胺

N,N,N',N'-tetrabutyl-3-oxa-pentanediamide presents excellent extraction abilities for actinides elements. The effects of hydrolysis and radiation on extraction behavior of U with TBOPDA have been investigated.

N，N，N'，N'四丁基 3 氧戊二酰胺对锕系元素具有良好的萃取性能，为了考察TBOPDA稳定性，研究了温度、酸度和吸收剂量对TBOPDA萃取性能的影响。

To study the analysis method of samples including a combination of dimethylformamide, undecane and butanone in the air of workshop.

［目的］研究工作场所环境空气中二甲基甲酰胺、十一烷和丁酮混合物一次吸附、一次分离的定量分析方法。

Some materials were synthesized in this paper at first, 1-nitro-2-pentanol was synthesized with nitromathane and butyraldehyde and the yield was 70.2%; l-nitro-2-pentanol was reduced to 1 -amino-2- pentanol with iron and the yield was 65.2%.

分别用氢氧化钠、三乙胺为缚酸剂，2-氨基-1-丁醇、1-氨基-2-戊醇、环己酮和二氯乙酰氯为原料，采用一步法和分步法合成了两种潜在除草剂安全剂。

What's more, we measure the inhibition rate of calcium carbonate and conglutination of the polymaths.

以丙烯酸、顺丁烯二酸酐和丙烯酰胺为原料，过硫酸钾为引发剂，在不同的条件下进行自由基聚合反应，生成不同分子量的共聚物，并测定了这些共聚物的粘度和对碳酸钙的阻垢率。

The influence of each condition on the reaction speed and yield was studied, and the optimal conditions were: the ratio of the amount of substance of aromatic amine and heptafluoro-isopropyl iodine was 1:1.1~1.5, the amount of substance of sodium dithionite, sodium bicarbonate, aniline compounds were respectively 1.1~1.3, the amount of substance of phase transfer catalyst TBAB and aniline compounds was 0.05~0.1, the concentration of aniline compound was 0.5~1.0 mol/L, reaction temperature was 10~20 ℃, and the solvent was aether.

最佳结果为：芳胺与七氟异丙基碘的物质的量比1：1.1~1.5，连二亚硫酸钠、碳酸氢钠与苯胺的物质的量分别为1.1~1.3，相转移催化剂四丁基溴化铵与苯胺的物质的量比在0.05~0.1，溶剂总用量使苯胺浓度在0.5~1.0 mol/L；反应温度10~20℃；溶剂采用乙醚。取代基供电子性越强，反应时间越短，产率越高；氨基的对位优先反应，氨基的邻位较难发生反应；且七氟异丙基总是优先取代在芳环电子云密度较高的位置上。

It is demonstrated that living polymerization can be achieved when the concentration of electron pair donors such as DMAB or Et3N is higher than that of trace water in the polymerization system,and that polymers with narrow molecular weight distribution can be obtained.

发现当N，N-二甲基苯胺或三乙胺的浓度稍高于质子性杂质的浓度时，即能实现异丁烯的活性聚合，得到分子量分布较窄的聚合物。

Using 2,4,6-〓 as phase-transfer catalyst, ten symmetrical azobenzene were prepared with a saturated solution of potassium ferricyanide in 2N aqueous potassium hydroxide and dichloromethane.

用2，4，6-三叔丁基苯酚为相转移催化剂，芳胺类化合物在饱和铁氰化钾的氢氧化钾溶液和二氯甲烷的两相转移催化下合成了10个对称取代偶氮苯，并对反应机理也做了合理的解释。

A GC headspace injection method for the determination of residual organic solvents such as methanol, ethanol, acetonitrile, dichloromethane, ethylacetate, 4 methyl 2 pentanone, toluene, DMF, chloroform and tetrahydrofuran in tazobactam was established.

建立了气相色谱顶空进样法测定三唑巴坦中甲醇、乙醇、乙腈、二氯甲烷、乙酸乙酯、甲基异丁基酮、甲苯、N ，N′-二甲基甲酰胺、氯仿和四氢呋喃等有机溶剂的残留量。

In addition, the new phosphine-catalyzed cyclization reactions of dimethylacetylenedicarboxylate and methyl propiolate with N-tosylimines are also described.

发展了膦催化下丁炔二酸二甲酯和丙炔酸甲酯与贫电子亚胺的环化反应，这对2-炔酸酯的反应又是一个补充，进一步丰富了膦催化下贫电子炔烃的反应化学。

A quantitative analytical method of 5% diethylmethylbenzamide in drive-worms floral-water by GC was introduced, Dibutyl Phthalate was selected as internal standard.

摘要本文介绍了以邻苯二甲酸二丁脂为内标物，对5%避蚊胺驱虫花露水进行有效成份测定的气相色谱分析法。

By the time of its fall, most of the prisoners were writers who had written against the corruptions of the government.

到它被攻陷的时候，里面多数的犯人是写了反对政府贪污文章的作家。

The most obvious variation to ovum morphological character was that the color was changed from light green to sepiaceous in embryonic development, and all the ovums were almost hatched after 96h.

在胚胎发育过程中卵的形态特征最明显的变化是颜色从淡绿到深褐色，卵在发育96h后卵基本全部孵化。