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The encapsulated TiO〓 particles by polymer were obtained with soapless emulsion polymerization of methyl methacrylate in water in the presence of the pretreated TiO〓 particles.

一种是用偶联剂钛酸酯对亲水性TiO〓粒子进行预处理,钛酸酯与TiO〓表面羟基反应,交联到TiO〓粒子表面,使TiO〓粒子表面由亲水性转变为憎水性,改善无机粉体与有机单体的亲合性,再进行TiO〓存在下甲基丙烯酸甲酯的无皂乳液聚合,即可得到TiO〓-PMMA复合粒子:另一种方法是用表面活性剂对TiO〓进行预处理,再进行TiO〓粒子存在下甲基丙烯酸甲酯的无皂乳液聚合,TiO〓粒子表面可形成一层均匀的聚合物膜,提出了包覆机理,指出单体在无机粉体表面发生聚合的关键是预先在粒子表面形成聚合场所,即吸附一层表面活性剂。

But Norton was no Spencerian, and he, too, strove for Martin's philosophic soul, talking as much at him as to his two opponents.

但是诺尔屯并不是个斯宾塞主义者,他也在努力理解马哲学的精髓,一面对他的对手说话一面也对马说话。

A micro-monolithic column was prepared by in-situ free radical polymerization of stearyl methacrylate with ethylene glycol dimethacrylate in the presence of the initiator AIBN and a mixture of porogens including iso-amyl alcohol and 1,4-butanediol.

以甲基丙烯酸碳酰十八酯为单体,乙叉二甲基丙烯酸酯为交联剂,异戊醇和1,4-二醇为二元致孔剂,偶氮二异腈为引发剂,原位制备了具有强疏水性的SMA整体微柱,并利用此整体微柱在普通高效液相色谱仪上测定滴眼液中氧氟沙星的含量。

Second,the sterically demanding substituted magnesium alcoholates can be prepared from dialkylmagnesiums R_2Mg and alcohol.The main disadvantage of this synthesis route lies in the fact that relative expensive dialkyl magnesium compounds,such as Et_2Mg for example,have to be used as starting materials.For this problem,a convenient preparation route of pure dialkylmagnesium from a Grignard reagent.

二、烷基镁法:具有空间位阻效应的仲醇镁和叔醇镁可以直接用烷基镁R_2Mg和醇进行反应来制备,这条路线的主要缺点是烷基镁比较昂贵,为了解决这个问题,本文采用格式试剂来制备烷基镁,将制得的烷基镁与叔醇反应制得叔醇镁。

Succinic acid dehydration is one of industrial methods to produce succinic anhydride.

二酸脱水法是工业生产二酸酐的方法之一。

An improved process for producing polyisobutylene succinimide used in emulsion explosive was introduced.

介绍了一种经过改进的乳化炸药用聚异二酰亚胺的生产工艺。

A high molecular weight polyisobutenyl succinimide dispersant with high nitrogen content and good thermal and oxidative stabilities was developed.

采用氯化烃化工艺和后偶联反应技术开发了一种氮含量高、热稳定性和氧化稳定性好的高相对分子质量的聚异烯基二酰亚胺分散剂。

Poly(p-vinylbenzyl succinimide) resin,which can be abbreviated to succinimide resin,was prepared by the reaction of chloromethylated polystyrene with succinimide in the presence of base. The succinimide resin was characterized by diffuse reflectance infrared Fourier transform spectrometry and elemental analysis.

摘 要:在碱性条件下,氯甲基化聚苯乙烯与二酰亚胺反应合成了聚(对乙烯基苄基二酰亚胺)树脂,采用元素分析、红外光谱对合成树脂的组成进行了表征。

Butyl p-hydroxybenzoate was synthesized from p-hydroxybenzoic acid and butanol with sulfoacid resin as catalyst. The optimum conditions were as follow: ratio of n-butanol, p-hydroxybenzoic acid and sulfonic acid resin was 0.25 mol ∶ 0.05 mol ∶ 1.5 g, refluxing for 5 h using water separator at the reflow reaction temperature.

摘 要:以对羟基苯甲酸和醇为原料,用磺酸树脂作催化剂,催化合成了尼泊金酯,优化反应条件为:n∶ n=5 ∶ 1,催化剂磺酸树脂的用量为对羟基苯甲酸质量的21%,反应温度为回流温度,反应时间为5 h。

The p-tert-butyl calix arene (n=4,6,8) were synthesized by p-tert-butyl phenol, formaldehyde aqueous solution as raw materials. Six kinds of calixarene oligomeric surfactants were prepared by etherification of the calix arene with 1,3-propane sultone and 1,4-butane sultone.

以对叔基苯酚、甲醛为主要原料合成杯芳烃母体对叔基杯芳烃(n=4,6,8);以1,3-丙烷磺内酯、1,4-烷磺内酯为醚化试剂,经Williamson醚化反应,合成出6种杯芳烃基低聚表面活性剂。

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