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The results show that complexing agent greatly effects on film's density. For the double complexing agents solution system based on citric acid, the solution with lactic acid and citric acid produced most compact film with lowest porosity; and for the double complexing agents solution system based on butane diacid, the solution with butane diacid and malic acid made most compact film with lowest porosity.

研究结果表明:络合剂对镀层的致密度影响显著,对于以柠檬酸为基的双络合剂体系镀液来讲,乳酸-柠檬酸双络合剂体系镀液获得的镀层致密度最好,具有最低的气孔率;而对于以二酸为基的双络合剂体系镀液来讲,二酸-苹果酸双络合剂体系镀液获得的镀层致密度最好,具有最低的气孔率。

Two estolide are that the ester melts an agent take amylum as raw material , with smooth butylene , the ester carrying out the solid room's spends reaction under the situation of there being no menstruum,ester composing smooth amylum butylene diacid Shan, and by having optimized reaction condition , having improved reaction efficiency.

以淀粉为原料,以顺烯二酸酐为酯化剂,在无溶剂的情况下,进行固体间的酯化反应,合成淀粉顺烯二酸单酯,并通过优化反应条件,提高了反应效率。

Synthesis of dibutyrate nylon acids from nylon acids and butanol by the reaction of direct esterification and distillation under reduced pressure, using solid acid as catalyst.

尼龙酸在固体酸催化下,与醇直接酯化、减压蒸馏制得合格的尼龙酸二酯。

Applied dodecencylsuccinic acid and diethanolamine as raw materials,dodecencylsuccinic acid diethanolamide was prepared.

以十二烯基二酸(T746)和二乙醇胺为原料合成了十二烯基二酸二乙醇酰胺防锈剂,探讨了原料质量配比、反应温度、反应时间等对产品性质的影响。

Spiral Spirobifluorene acetylated is oxidated by m-chloroperoxybenzoic acid and hydrolyzed by sodium hydroxide ,obtaining 2,2 '- dihydroxy -9,9'- spiral Spirobifluorene .Through nitrification,Reduced by hydrazine hydrate, we may get the 2,2 '- diamino -9,9'- spiral Spirobifluorene which are characterizated by IR, 1H-NMR !

L-酒石酸和乙醇酯化得到酒石酸二乙酯,将保护羧基保护起来,然后用碘甲烷在2,3-位上两个甲基,得到2,3-二甲氧基-酒石酸二乙酯,再用氢氧化钠将其水解,得到2,3-二甲氧基-酒石酸,用五氯化磷将羧基酰化,得到2,3-二甲氧基- 1,4-二酰氯,经过与二环己胺反应,得到拆分配体2,3-二甲氧基–N,N,N',N'-四环己二酰胺。

Treatment of dials with N-tert-butanesulfinamide, all biaryl dials were successfully converted into the corresponding bis-imines which were then treated with samarium diiodide to afford diamine products. The absolute configurations of all the intramolecular coupling products were determined by X-ray crystallography.

轴手性二醛与N-叔基亚磺酰胺缩合得到相应的亚胺,其为一对非对映异构体。N-叔基亚磺酰亚胺在二碘化钐条件下得到的偶联产物,经X-衍射也确定了其立体构型。

The intermediates were coupled respectively with derivatives of gallic acid to give polysubstituted diphenylmethane.

发现邻甲氧基苯甲酸甲酯中酯甲基可以被正基锂和仲基锂中烷基交换生成相应的酯,反应的机理不明确。

The polyesters with terminal hydroxyl groups were prepared by condensation polymerization of adipic acid with 1,4-butanediol or ethylene glycol and, in some cases, a little amount of propylene glycol. The polyurethane thermoplastics were then prepared with the polyester, 4,4'-diphenylmethane diisocyanate and 1,4-butanediol.

采用己二酸、乙二醇(或加入少量1,2-丙二醇)和1,4-二醇制备了端羟基聚酯,并用该聚酯和4,4'-二苯基甲烷二异氰酸酯、1,4-二醇制备了聚酯型热塑性聚氨酯;考察了NCO/OH值、聚酯分子量等因素对热塑性聚氨酯的物理机械性能的影响。

The fish samples were cleaned up by Florisil, then analyzed by GC-EI-MS to determine eight phthalic acid esters, diethyl phthalate, dipropyl phthalate, dibutyl phthalate, butyl benzyl phthalate, dipentyl phthalate, dicyclohexyl phthalate, dihexyl phthalate and diethyl hexyl phthalate.

鱼肉样品以Florisil硅藻土层析柱净化后,经气相色谱-电子轰击离子源-质谱法分析其中8种邻苯二甲酸酯含量:邻苯二甲酸二乙酯、邻苯二甲酸二丙酯、邻苯二甲酸二酯、邻苯二甲酸基苄基酯、邻苯二甲酸二戊酯、邻苯二甲酸二环己基酯、邻苯二甲酸二己酯、邻苯二甲酸二(2-乙基己基)酯。

N-Butyl stearate was synthesized in high yield by esterification of n- butyl alcohol with stearic acid in the presence of ammonium ferric sulfate dodecahydrate.

在十二水合硫酸铁铵存在下,正醇和硬脂酸发生酯化反应,高收率地合成了硬脂酸正酯。

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