丁

The acetalization and ketalization of various aldehydes and ketones with glycols using FeCl3 as catalyst were studied. The effects of reaction time, mole ratio of reactants and amount of catalyst on the yield of acetals were investigated.

研究了在FeCl3催化下，乙二醇与环己酮、丁酮、丙酮、丙醛、丁醛、异丁醛、戊醛、异戊醛、正辛醛、二苯甲酮、苯甲醛等十余种醛的缩合反应。

The optimum initial substrate concentration for cultivation of inoculum was 8%.The optimum conditions for batch fermentation were 0.04vvm of air flow,5.8 of pH value.The fed-batch fermentation showed that the productivity of Klebsiella pneumoniae CICC 10011 was better than K.pneumoniae CGMCC 1206.The maximum concentration of 2,3-butanediol and acetoin was 103.38 g/L (90.98 g/L of 2,3-butanediol),and the yield reached 82.2%of its theoretical value.The fermentation conditions for K.pneumoniae.

确定种子培养的最适初始底物浓度为8%；间歇发酵的条件为：微氧发酵，通气量为0.04vvm，pH值为5.8；通过批式流加发酵实验表明：Klebsiella pneumoniae CICC 10011的代谢产2，3-丁二醇能力要远高于K.pneumoniaeCGMCC 1206，2，3-丁二醇最高浓度达90.98g/L，2，3-丁二醇与乙偶姻浓度之和最高达103.38g/L，转化率为理论最大值的82.2%，其发酵工艺还有待于进一步优化。

This review will summarize several aspects concerning the distribution of agmatine and NMDA receptors in the central nervous system, the binding sites of agmatine on NMDA receptors as well as the pharmacological functions closely associated with NMDA receptors.

本文就胍丁胺与NMDA受体在中枢神经系统的分布、胍丁胺在NMDA受体上的作用位点以及胍丁胺通过NMDA受体介导的药理作用等几个方面进行了综述。

The mixed collectors studied were as following: benzyl arsonic acid-sodium butyl xanthate for walframite flotation, salicylohydroxamic acid-F〓, salicylohydroxamic acid-cupferron, salicylohydroxamic acid-TBP , F〓-TBP, cupferron-benzohydroxamic acid etc. for cassiterite flotation and mixed aliphatic acid or aliphatic amine for beryl or spodumene flotation.

研究过程中，本文选用了如下具体实例：苄基胂酸与丁基黄药浮选黑钨矿，水杨羟肟酸与F〓、水杨羟肟酸与铜铁灵、水杨羟肟酸与磷酸三丁酯、F〓与磷酸三丁酯、铜铁灵与苯异羟肟酸两两结合浮选锡石，混合脂肪胺与混合脂肪酸浮选锂辉石与绿柱石。

Water,butylene glycol,biosaccharide gum-1,ppg-26-buteth-26,panthenol,peg-40 hydrogenated caster oil,hydroxyethylcellulose,imidazolidinyl urea,saccharide isomerate,benzophenone-4,phenoxyethanol,triethanolamine,citrus aurantium dulcisoil,pentadecalactone,methylparaben,sodium hyaluronate,citric acid,butylparaben,ethylparaben,citrus aurantium amaraoil,propylparaben,methylchloroisothiazolinone,methylisothiazolinone,red 4,yellow 5,red 33,limonene,linalool

水，丁二醇，多醣物质，PPG-26-丁醇聚醚-26，维生素B5，PEG-40氢化蓖麻油，羟乙基纤维素，尿素醛，天然异构寡糖，二苯甲酮- 4，苯氧乙醇，三乙醇胺，甜橙油，环十五内酯，羟苯甲酯，透明质酸钠，柠檬酸，羟苯丁酯，羟苯乙酯，苦橙油，羟苯丙酯，甲基氯异塞唑晽酮，甲基异噻唑啉酮，红4，黄5，红33，柠檬精油，芳樟醇

Water,propylene glycol,butylene glycol,glyceryl polymethacrylate,ascorbic acid,peg-7 glyceryl cocoate,biosaccharide gum-1,peg-40 hydrogenated castor oil,ppg-26-buteth-26,phenoxyethanol,hydroxyethylcellulose,xanthan gum,methylparaben,pentadecalactone,citrus aurantium dulcisoil,disodium edta,sorbic acid,tocopheryl acetate,butylparaben,retinyl palmitate,iris germanica root extract,sodium hyaluronate,ethylparaben,propylparaben,citrus aurantium amara oil,limonene,linalool

水，丙二醇，丁二醇，甘油聚甲基丙烯酸酯，维生素C衍生物，PEG-7 椰子油酸单甘酯，多醣物质，PEG-40氢化蓖麻油，PPG-26-丁醇聚醚-26，苯氧乙醇，羟乙基纤维素，山羊胶，羟苯甲酯，环十五内酯，甜橙油，乙酸乙二胺二钠，山梨酸，醋酸盐维他命E，羟苯丁酯，维他命A酯，鸢尾花根萃取，透明质酸钠，羟苯乙酯，羟苯丙酯，苦橙油，柠檬精油，芳樟醇

The experimental results show that using the feed technique of "starved state" can raise the conversion ratio of monomers, shorten the reactive time and get polymers with much more even distribution of molecular weight; the technique of adding azobisisobutyronitrile as an initiator first and then benzoperoxide as another initiator at later Stage of experiment can get higher initiating efficiency than using one initiator only.

结果表明：采用&饥饿态&聚合工艺可提高单体转化率，缩短反应时间，且所得到聚合物相对分子质量分布均匀；选用偶氮二异丁腈和过氧化笨甲酰两种引发剂进行复配，比选用单一引发剂的引发效果好；选用酯酸丁酯、正丁醇和丙二醇甲醚丙酸酯作混合溶剂，当配比为2：1：1时聚合体系稳定，聚合物的固体质量分数可达70%，且粘度适中。

Two novel soluble poly, poly [(3-butyrylpyrrole-2, 5-diyl) p-nitrobenzylidene] and poly [(3-butyrylpyrrole-2, 5-diyl)(3-hydroxy-4-methoxy) benzylidene], were synthesized firstly by condensation of 3-butyrylpyrrole with p-nitrobenzaldehyde and vanillin, respectively.

通过3-丁酰基吡咯单体分别与对硝基苯甲醛和香草醛的缩聚反应，成功合成了两种新型可溶性聚吡咯甲烯衍生物－策［（3-丁酰基吡咯－2，5-二）对硝基苯甲烯］和聚［（3-丁酰基吡咯－2，5-二）（3-羟基－4-甲氧基）苯甲烯］。

And the rapid development of China's automobile tire industry, stimulating the production of rubber additives and stimulate the rapid growth the demand for raw materials have increased tert - butylamine, tert - butylamine serious domestic demand, the majority rely on imports.China's demand for NS in 2004 about 10,400 tons of production of about 7,150 metric tons; It is expected that in 2007, the NS will add production capacity for 12,000 tons, tert - butylamine demand for raw materials will reach 7,800 tons.

我国汽车和轮胎工业快速发展，拉动和刺激了橡胶助剂产量的快速增长，对原料叔丁胺的需求也随之增加，目前国内叔丁胺严重供不应求，大部分依赖进口。2004年我国促进剂NS需求量在10400吨左右，产量约7150吨；预计到2007年，促进剂NS将新增年产能力1.2万吨，对原料叔丁胺的需求量将达到7800吨。

This item plans to construct 5 thousand t/y Tert - butylamine production equipment which uses internally developed independently isobutene cyanide process for the production of raw materials for pure isobutylene, purity of 99.5% of the domestic production of tert - butylamine.

该装置采用国内自主开发的异丁烯氰化法生产工艺，以纯异丁烯为原料，生产纯度为99.5％的叔丁胺产品。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。