-甲基哌啶

Excited triplet state of [60]fullerene containing piperidinoxanthate dyad is at 690nm, which has lifetime of 23.7xs in Ar-saturated benzonitrile, whereas that ofparent C60 is at 750nm, with lifetime of 50s, indicating that excited triplet state of

富勒烯C_(60)哌啶黄原酸酯稠合体激发三线态的最大吸收峰在690nm，相对于纯C_(60)发生蓝移用532nm激光激发后，富勒烯C_(60)哌啶黄原酸酯稠合体激发三线态的最大吸收峰在690nm，相对于C_(60)的750nm发生蓝移，在氩气饱和的苯腈中寿命23.7μs，比C_(60)的55μs短，表明环加成反应连接的哌啶黄原酸酯部分具有吸电子性质。

We provide intermediates of Methylphenidate HCl: 2-Phenyl-2-(2-Piperidyl) Acetamide; 2-Phenyl-2-(2-Piperidyl) Acetic Acid; Series of Benzoic Acid、Benzonitrile; Other pharmaceutical intermediates.

提供盐酸利他林中间体：2-苯基-2-(2-哌啶基)乙酰胺；2-苯基-2-(2-哌啶基)乙酸；苯甲酸、苯甲腈系列及其他医药中间体。

The UV-Visible absorption spectra and the fluorescence emission spectra of sixteen tetra-substituted metallo-phthalocyanine complexes {R4PcM, where R=2-［4-(2-sulfonic ethyl)piperazin-1-］ ethoxyl, 2-(piperidin-1-yl)ethoxyl; substitution position at α-position and β-position of phthalocyanine ring; M=Zn, Ni, Coand Cu} were measured.

报道了16种含哌嗪或含哌啶四取代酞菁金属配合物{R4PcM， R=2-［4-(2-磺基乙基)哌嗪-1-基］乙氧基、 2-(哌啶-1-基)乙氧基；取代位置分别在α位和β位； M=Zn， Ni， Co， Cu}的UV-Vis吸收光谱和荧光发射光谱的测定，探讨了中心金属离子、取代基种类及其取代位置、溶剂等因素对酞菁金属配合物UV-Vis吸收光谱和荧光发射光谱性质的影响。

METHODS: Patients met with CCMD-Ⅲ criteria of schizophrenia were randomized into two groups: ziprasidone group (n=118) and haloperidol group (n=117) for a double dummy study. The initial doses were 40 mgd^(-1) and 8 mgd^(-1) and the high did not exceed 160 mgd^(-1) and 20 mgd^(-1) for individual of ziprasidone group and haloperidol group respectively.

将235例精神分裂症病人随机分为齐拉西酮组（118例）和氟哌啶醇组（117例），齐拉西酮和氟哌啶醇最低日剂量分别定为40mgd^(-1)，和8mgd^(-1)，最高日剂量分别限定为160mgd^(-1)，和20mgd^(-1)，每日分2次服用。

The target compounds were obtained in high yield through Michael conjugative addition of amines to methyl acrylates, cyclocondensation of the obtained diadducts in the presence of sodium methoxide,and decarboxylation of the cyclocondensation products in acid.

以胺类化合物为原料，与丙烯酸甲酯经过两次Michael加成得到N，N 二丙酸甲酯类化合物，该化合物在甲醇钠存在下进行环合，在酸性条件下脱羧，高收率得到4 哌啶酮类化合物，从而证明了这是一条合成N 取代 4 哌啶酮类化合物的普遍方法。

The preparation of grafted derivant of tertiary amine: it is prepared by the reacting of above (1) product and (2) product heated in water bath at 40℃ within 10min.

聚环氧氯丙烷乙二醇哌啶接支衍生物的制备：将上面制备的聚环氧氯丙烷乙二醇与0.25mol环氧丙基哌啶叔胺于40℃水浴条件下进行接支反应。

The preparation of esterified derivant : it is prepared by the esterifying reacting of above (3) product and 4g dodecylbenzene sulphonic acid heated in water bath at 40℃ within 30min.

聚环氧氯丙烷乙二醇哌啶接支酯化衍生物的制备：4g十二烷基苯磺酸于40℃水浴条件下聚环氧氯丙烷乙二醇哌啶接支衍生物进行酯化反应。

The study sum up a synthesized route which synthesize (2E,4E)-1,6-bis(3-aminopiperidin-1-yl)hexa -2-4-diene-1,6-dione easily.

总结出了一条反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨的一条合成路线，为国内外同行在合成反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨及其性能研究方面提供了大量得数据，为同行们在合成和更深入的研究反，反-1，6-（R-3-氨基哌啶基）粘糠酰氨提供有限的参考，以互相学习交流。

The effect of reaction temperature,reaction time,materials ratio on the synthesis of piperidine alcohol benzoate ,hindered amine light stabilizer,from piperidine alcohol and benzoyl chloride by direct condensation were studied,and the proper technological conditions were given as follows:the reaction temperature is 95℃;reaction time is 4 h; the mole ratio of reactants,n∶n is 1∶1.4,the amounts of solvent is 40 mL(based 0.1mol piperidine alcohol),the arerage yield ...

王树清，高崇，苯甲酸哌啶醇酯HALS的合成工艺研究研究了以苯甲酰氯和哌啶醇为原料直接缩合合成苯甲酸哌啶醇酯受阻胺光稳定剂时反应温度、反应时间、原料配比等条件对合成反应的影响，确定了最佳工艺条件。最适宜的工艺条件是：反应温度95℃、反应时间6h、原料摩尔比n∶n为1∶1.4，溶剂用量为70mL(相对于0.1mol哌啶醇)，苯甲酸哌啶醇酯的收率为91.05%，产品纯度98.5%。

Piperidinecarboxylic acid is used as the raw material and acetic acid as the acylating agent, followed by the addition of some acetic anhydride in the later stage to get an important organic intermediate n-acetylpiperidine-4 carboxylic acid in the yield of 92%. Toluene is used as the solvent instead of sulfinyl chloride in the acyl chlorination to produce n-acetylpiperidine-4-carbonyl chloride with the yield of 97%.

以4-哌啶甲酸为原料、醋酸为酰化剂，后期加入少量醋酸酐反应得到中间体N-乙酰基哌啶－4-甲酸，收率92%；在甲苯溶剂中进行酰氯化得目标产物N-乙酰基哌啶－4-甲酰氯，收率97%。

The basic concept of FOP can be summarized as to further optimize effective prescription according to the standard of curative effects and with the aid of modern science and technology and theories of traditional Chinese medicine.

其基本内涵可概括为：以确有疗效的中药复方为研究对象，以现代科学技术和传统中医药理论为技术支持，以该复方所治病证的药效响应为评价标准，以优化重组疗效更优的新复方为研究目的。

Ever since our world has been a world, native forests have been indiscriminately exploited by man.

自从我们的世界一直是世界原生森林被任意剥削人。