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SAA ligand Lh could induce asymmetric addition of terminal alkyne to aldehydes without using air-sensitive Ti4and expensive Zn2.with good result of high yield (up to 99%) and good enantioselectivities (up to 84%ee).

将SAA配体Lh应用于在无Ti_4和Zn_2的条件下促进端基炔对醛的不对称加成反应中,反应的收率普遍较高,最高达99%,对映体选择性高达84%ee。

Under such conditions the yield of allantoin is 28.75%.

这种两步法合成尿囊素的关键在

In this paper, major agronomic traits and grain quality traits affecting rice yield and grain quality were investigated in seven aromatic rice maintainer lines bred in Sichuan and one variety introduced from America. It was aimed at estimating the numbers of gene controlling aroma, the allelism of aroma genes, location of aroma gene on the chromosome, and molecular tagging of aroma gene.

本研究利用四川新育成的七个香稻保持系(D香1B、D香2B、内香2B、内香4B、绵香2B、绵香3B、宜香1B)、一个香稻引进改良品种(泸香90)和一个非香型保持系为材料,研究了香稻保持系主要农艺性状和品质性状对品质、产量的影响,并且通过杂交群体构建对香稻香味性状进行了遗传分析。

The result shows that the repeatability of the method is within the range of the allowable repeatability error. The yield of recovery of standard sample is 95%~105%, and the consistency of results is better and the different of two results is less titan 84 in comparison with ASTM D 5762-95 dilution method.

阐述方法原理,考察方法的重复性在允许重复性误差范围内;标准样品的回收率在95%~105%;与ASTM D 5762-95的稀释法比较,结果一致性较好,两种结果的差值小于84个单位。

The industrial synthesis of 1, 4-butanediol from allyl alcohol involves two steps with low yield and selectivity.

目前工业上都是采用两步法由丙烯醇生产1,4-丁二醇,效率低,选择性差。

The latter was esterified with allyl alcohol in the presence of the catalyst toluene-p-sulfonic acid to get the title compound in the yield of 87.1%.

后者在对甲苯磺酸催化下与烯丙醇经酯化反应制得标题化合物,收率为87.1%。

At first,the intermediate of sodium 3-chloro-2-hydroxy propanesulfate was synthesized from epichlorohydrin and sodium bisulfite;And then,using NaOH as a catalyst,the title compound has been synthesized from intermediate and allyl alcohol to reach the yield of about 70%.

先由环氧氯丙烷和亚硫酸氢钠合成中间体3-氯-2-羟基丙磺酸钠,然后中间体再与丙烯醇在氢氧化钠催化下生成目标产物2-羟基-3-烯丙氧基丙磺酸钠。

Sodium allylate was prepared from solid sodium hydroxide and allyl alcohol under mild conditions, and then the solid sodium allylate was reacted with epichlorohydrin in anhydrous system to produce allyl glycidyl ether in high yield and purity.

以固体NaOH和烯丙醇为原料在温和条件下制得烯丙醇钠,再以固体烯丙醇钠为原料,与环氧氯丙烷在无水条件下高产率地得到高纯度的烯丙基缩水甘油醚。

The yield of allyl glycidyl ether can reach up to 96% at 30 ℃ for 3 h at a molar ratio of 1 to 1.5 of sodium allylate to epichlorohydrin.

醚化反应中固体烯丙醇钠与环氧氯丙烷摩尔比为1:1.5,在无水条件下于30℃反应3 h,烯丙基缩水甘油醚的收率达96%以上。

Chiral N,P ligand 5 was examined for the asymmetric allylic alkylation of 1,3-diphenyl-2-propenyl acetate with up to 89% yield and up to 81.6% ee.

化合物5用于钯催化的1,3-二苯基-2-烯丙基乙酸酯的不对称烯丙基烷基化反应,产率为89%,对映体过量最高为81.6% ee。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

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