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The result indicated that: the amount of the excess HF formed direct ratio to the yield of phosphorus pentafluoride and the optimum amount of the excess HF used is about 35%; the trickling rate of oleum shouldnt make the temperature of hexafluorophosphoric acid exceed 25 ℃ and the amount of oleum is 110% to 125% that of stoichiometry so that the content of phosphorus pentafluoride can be achieved 90%; the time and temperature of heating hexafluorophosphoric acid influenced both the yield and the content of phosphorus pentafluoride, and the optimum time should be about 30 minutes and the proper temperature was 148 to 153℃; when alcohol used asrefrigerant, the content of phosphorus pentafluoride was 94.03%, and the content can be up to 97.38%, provided that using liquid nitrogen as refrigerant.

通过实验发现,氟化氢用量与五氟化磷的产率成正比,最佳过量百分率宜在35%左右;发烟硫酸的滴加速度不能使中间产物温度大于25℃,发烟硫酸用量大于理论量10%~25%时,得到的五氟化磷纯度高于90%;六氟磷酸的加热温度对五氟化磷的产率和纯度均有影响,宜在148~153℃的范围内,加热时间应在30分钟左右;用工业酒精做冷凝介质得到的五氟化磷纯度最高只能到达94.03%,使用液氮做冷凝介质可以使五氟化磷的纯度达97.38%以上。

In the scorch stage, average yield of withered grass of second and third year growth prematurity type of Phleum pratense L. is 10672.5 kg/hm2, by cradling one time per year, average yield of wind hay grass is 7575 kg/hm2, the plant average height of selective colony is 160.0cm, the plant height of colony is rather equality. In the course of general nutrition composition analysis, discover that nutrition value of late-maturity type is higher than nutrition value ofprematurity type, coarse fibre and coarse protein and coarse fat of late-maturity type are 10.7%, 3.58%, 24.82% respectively, coarse fibre and coarse protein and coarse fat of prematurity type are 9.84%, 2.61%, 27.59% respectively, dry matter content of prematurity type is 92.63%, dry matter content of late-maturity type is 92.22%.

在枯黄期,第二、第三年生的早熟类猫尾草一年收割一次,枯草平均产量为10672.5 kg/hm~2,风干草平均产量为7575 kg/hm~2,选育出的群体平均高度为160.0cm,群体内植株株高较均一;在常规营养成分的分析中发现晚熟类的营养价值稍高于早熟类,晚熟类的粗蛋白是10.7%,粗脂肪是3.58%,粗纤维是24.82%,早熟类的粗蛋白是9.84%,粗脂肪是2.61%,粗纤维是27.59%,早熟类干物质含量92.63%,晚熟类干物质含量92.22%。

For understanding the yield and quality changes of spring wheat piled up in field after reaping in Qinghai province, we selected Qingchun 533, which was planted widely in Qinghai province, and Plateau 205(susceptible to preharvest sprouting), Plateau 115, Plateau 448 and Plateau 314 which were bred by our institute, piled up them as the quomodo farmer used, sampled them every nine days, and mensured yield, SDS sedimentation value and falling number value to trick the changes of wheat.

为了解青海省春小麦收割后田间堆放期间产量和品质的变化,选择近年育成的春小麦品种&高原205&、&高原115&、&高原448&和&高原314&以及曾为青海省主栽品种的&青春533&为材料,收刻后以农民常用的田间堆放方式进行堆放,每隔9d对其进行采样,测定产量、SDS沉淀位和降落数值的变化。

When introduced the ultrasound into EHD of acrylonitrile, the yield of propionitrile is increased, but the yield of hydrotrimer is decreased as compare to the silent condition.

对丙烯腈电化学氢化二聚反应生成己二腈的体系中施加超声的结果表明,对这一后置化学反应的体系,超声可以改变反应的机制,并最终对电解产物的分布产生影响。

The total yield and ee value of the enantiomer were 12% and 98.7% respectively. The total yield of the racemic one was 17%, 2.5 fold more than the previously publishable route.

整条路线具有高产率高ee值的特点,将会成为合成此类直型二氢苯并呋喃香豆素的流行方法。

The oil yield rate of sewage sludge is higher th an that of putrescible garbage,the oil yield rate of activated sewage sludge i s the highest,lacquer sludge and digested sludge in successi...

低温热解制油技术的操作条件对产油率也有不同程度的影响,产油率随着热解温度的升高而增加,随着停留时间的增加而减少。

With sodium acetate as catalyst, inosine was esterified with acetic anhydride in the yield of 92% to give 2',3',5'-triacetyl inosine, which was treated with pyridine and phosphorus oxychloride to form a pyridinium solution, followed by performing an amination at 40℃ and 0.25~0.30 MPa to achieve adenosine in the yield of 67%.

肌苷在醋酸钠存在下与醋酸酐发生酯化反应以92%的收率得到2',3',5'-三乙酰肌苷,其化合物经吡啶和三氯氧磷处理形成吡啶盐溶液,未分离直接在40℃、0.25~0.30 MPa压力下进行氨解反应以67%产率制得腺苷。

In yield capitalization, the relationship between several year's stabilized income and a reversionary value at the end of a designated period is reflected in a yield rate.

在报酬资本化法中,几年的稳定收益和某一确定期间的期末终值通过收益率予以体现。

New planted ramie often have defects of fewer efficient plant numbers, many of high-branches, difficult to peel bast, low yield, bad fiber quality and so on. Aiming at all these shortages, the cuttage breeding technology of fine varieties and high-yield and good-quality cultivating method, breeding Cutting seedling with several low-branches, planting deeply appropriately, ridging to foster rootstocks when intertilling, was brought forward.

针对苎麻新麻有效株少、高位分枝多、韧皮剥制难、原麻产量低、纤维品质差等问题,提出了培育携带多个低位分枝的扦插苗,麻苗移栽时适当深植,辅以新麻中耕时起垄培蔸的苎麻良种扦插繁殖新技术与新麻高产优质栽培方法。

Based on the field experiment data of winter wheat blending irrigation by saline water in Nanpi Ecological Agriculture Experimental Station of the Chinese Academy of Sciences from 2002 to 2005, the effects of blending irrigation with mineralization of 0.84, 3, 4 and 5 g/L on the soil salification rate, soil sodium adsorption ratio of soil saturation extract as well as winter wheat yield and yield constitute factors irrigated were studied in order to determine upper limit of irrigation mineralization suitable for the location.

根据中科院南皮生态农业试验站2002~2005年的冬小麦微咸水混灌田间试验资料,以淡水为对照研究了矿化度分别为3、4、5 g/L的微咸水混灌对土壤积盐率、土壤饱和浸提液钠吸附比、冬小麦产量和产量构成因素以及水分利用效率的影响,从而确定适宜的灌溉水矿化度上限。

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