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Solvent dosage is 10mL/ gram epichlorohydrin. The yield of 5-chloromethyl-2-oxazolidinone was more than 65.2%. 5-Chloromethyl-2-oxazolidinone and sodium phenolate were condensated to give 5-phenoxymethyl-2-oxazolidinone after taking off the sodium chloride in yield of 63.0%~78.0%. Dimethylsulfoxide was used as the solvent, and orthogonal experiment to the reaction condition had been carried out.

用5-氯甲基-2-噁唑烷酮和酚钠缩合,脱去氯化钠后生成5-芳氧甲基-2-噁唑烷酮类化合物,选用二甲亚砜为溶剂,对反应条件进行了正交实验,最佳条件为:反应温度120℃、反应时间20h、物料配比1:1,产率为63.0%~78.0%。

Compared with HA in water-contained organic solvents, the pigment in micelle had higher pKa value and higher fluorescence quantum yield. Moreover, the quantum yield of active species produced from photosensitization, 1O2 and ·OH, increased as well. As a result, the photosensitivity of HA was enhanced.

相对于含水有机体系,HA在胶束中基态的 pKa值升高,荧光量子产率增大,光敏反应产生的活性中间体1O2 和·OH的产额增加,从而提高了其光敏活性,这在光敏损伤作用中具有重要的生物学意义。

Thus it can be seen that the suitable amount and ratio of NP or NPK application impels the formation of photosynthate, hoists the biomass, grain yield, accelerates the synthesis of starch and fat, and obtains high yield and good quality.

由此可见,适宜的氮磷和氮磷钾肥用量和比例促进光合产物形成,提高生物量、籽粒产量、加速合成淀粉和脂肪,得到高产量和好品质。

The ammonia was evaporated under decreasing pressure, and the precipitate was filtered off and the liquid was poured into hot saturated picric acid solution to get picrate with a yield of 85.0%. The optimum process starting from imidazole-4,5-dicarboxylic acid was: imidazole-4,5-dicarboxylic acid in acetic anhydride was refluxed to get imidazole-4-carboxylic acid, and the product was esterification in ethanol with a catalyzer of concentrated sulfuric acid to get ethyl imidazole-4-carboxylate, at last the compound above was reduced by LiAlH4 in ether at room temperature to get the target compound, the total yield of this route was 49.6%.

以4,5-二羧酸咪唑为原料的较佳工艺:1 脱羧反应:4,5-二羧酸咪唑40g,醋酐1200ml,回流10h,过滤并将滤液浓缩至干,所得固体加至50%的乙醇溶液回流,过滤并将滤液自然冷却过夜,过滤得固体;2 酯化反应:4(5)-羧酸咪唑50g,乙醇1000ml和浓硫酸60ml,加热回流2h,5%浓度NaOH溶液调节至pH=8,减压浓缩至干,加入少量水回流,自然冷却过夜并过滤得固体;3 还原反应:LiAlH410g,乙醚300ml和4(5)-羧酸咪唑乙酯28g,常温反应1.5h,小心滴加25ml水后过滤,滤渣溶于300ml甲醇中并过滤,收集所得乙醚和甲醇滤液浓缩至干,将所得固体溶于300ml乙醇中加热回流,后将溶液浓缩至约30ml,冷却并过滤得固体,该路线总收率为49.6%。

Through the pilot survey analysis and comparison, the Green eggplant 10-3-4-8-12 fine lines and yield better integrated characters, better than the same period in the Senate trial of Xi'an Green eggplant; performance for the specific strains of plants with strong growth potential, consistency Good, ripe fruit early, high yield, fruit-being, good color and not easily infected with zombies fruit of the advantages of production in the region is very suitable for planting.

通过试验调查分析和比较,绿茄10-3-4-8-12优良品系综合性状和产量较好,优于同期参试的西安绿茄;该品系具体表现为具有植株生长势强、一致性好、果实成熟早、产量高、果型正、色泽好、不易感染僵果病等优点,十分适合本地区生产种植。

Combining with the National Natural Science Foundation ofChina(No.50478032), following researches were done in this thesis: 1 The variation regularity of the ultimate anti-bending capacity of therectangular-sectioned beam with different corrosion has been obtained through thequalitative analysis of 48 beams (32 corroded beams and 12 comparing beams) withaccelerated corrosion; 2 The conclusion has been obtained that the strain of corroded steel bar andconcrete no longer fit in with the assumption of plane section through the analysis ofthe strain data, the strain relation of steel bar and concrete in the mid-span section ofvariously corroded beams at ultimate has been obtained. Through the building of newgeometric relation, the expression of the height of compressive area in the corrodedbeam with rectangular section has been deduced, and the formula with corrosion rateas the main variable for the anti-bending capacity of the corroded concrete beam hasbeen suggested and verified by experiment.; 3 The influence of steel bar corrosion and the concrete regression to the flexureductility coefficient of the corroded structure component has been analyzed. Based onthe relation of steel bar and concrete at yield and ultimate, the expression for theflexure at yield and ultimate of corroded reinforced concrete beam, and the model forthe calculation of the flexure ductility has been built.

本文结合国家自然科学基金项目(50478032)"既有钢筋混凝土桥梁时变可靠度研究",主要进行了以下研究工作: 1通过对48根快速锈蚀钢筋混凝土矩形截面梁(32根锈蚀梁和12根对比试验梁)数据的定性分析,得到了不同锈蚀率下,锈蚀钢筋混凝土矩形截面梁极限抗弯承载力的变化规律; 2通过对应变数据的分析,论证了锈蚀构件钢筋和混凝土的应变不再符合平截面假定的结论,并通过回归分析得出了不同锈蚀率的螺纹钢筋梁和光圆钢筋梁在极限弯矩作用下,跨中截面处钢筋应变和钢筋处混凝土应变的关系,通过构造新的几何关系,得出了锈蚀钢筋混凝土矩形截面梁计算受压区高度的表达式,既而得出了以锈蚀率为主要变量的锈蚀钢筋混凝土矩形截面梁的正截面抗弯计算建议公式,并通过试验数据加以验证; 3分析了钢筋锈蚀和混凝土劣化对锈蚀构件曲率延性系数的影响,结合钢筋屈服和极限弯矩两种状态下钢筋和混凝土的应变关系,分别得到了锈蚀钢筋混凝土矩形截面梁屈服曲率和极限曲率的计算表达式;既而推导出曲率延性系数的计算模型。

SDS-PAGE results showed that as to Mut+ recombinant highest yield was obtained after 4 days inducing and with the culturetime prolonged it reduced. Pokeweed antiviral protein gene expressed well when methanol concentration reached 10g/L. Pokeweed antiviral protein obtained high yield in thin acidic culture medium (pH6.0-6.4) and its quantity in total mass of secrete protein exceeded 30%.

SDS-PAGE分析结果表明,Mut~+组菌株在甲醇诱导第四天后PAP在培养液中积累量达到最高水平,延长培养时间会导致产量下降;在10g/L的甲醇浓度诱导下,PAP的表达量达到最高;培养基pH值在偏酸性条件下(6.0-6.4)PAP的表达量都维持在较高的水平。

Utilizing the expression of maximum deviatoric stress yield rule on π plance and the relationship betwen π plane and principal stress this paper deduces and examines the shape and position of maximum deviatoric stress yield rule on π plane and the relation to Mises circle and Tresca hexagon .

利用π平面与主应力空间的关系及最大偏应力屈服准则在π平面上的表达式,推导验证最大偏应力屈服准则在π平面上图形的形状、方位及其与Mises圆和纯拉伸Tresca六边形的关系。

Based on the description of Mohr-Coulomb and Drucker-Prager yield criteria with invariant of stress, a formula for error estimation of unit strain energy between the two stress states is established in the deviatoric plane of the principal stress space, which satisfies M-C and D-P yield criteria respectively. A general procedure to transform M-C material parameters to D-P analysis parameters is obtained.

基于应变比能的概念,在偏平面内建立了分别进入Mohr-Coulomb和Drucker-Prager屈服面时所需形状改变比能的差值公式,获得M-C材料参数向D-P计算参数等效的统一性方案。

In this paper,a probability space is introduced to describe IC yield optimization problem,and the probability measure of the feasible region is employed to indicate the yield The weighted Monte Carlo method is snitable in the early optimizzation stage,while the improved SA algorithm is more efficient in the final stage.

本文引入了一个概率空间来描述集成电路合格率优化问题,并将合格率表示为可行域的概率测度。所提出的变权重MonteCarlo法适合于合格率不太高的场合,而改进后的SA算法则适合于合格率比较高的场合。

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However, as the name(read-only memory)implies, CD disks cannot be written onorchanged in any way.

然而,正如其名字所指出的那样,CD盘不能写,也不能用任何方式改变其内容。

Galvanizes steel pallet is mainly export which suits standard packing of European Union, the North America. galvanizes steel pallet is suitable to heavy rack. Pallet surface can design plate type, corrugated and the gap form, satisfies the different requirements.

镀锌钢托盘多用于出口,替代木托盘,免薰蒸,符合欧盟、北美各国对出口货物包装材料的法令要求;喷涂钢托盘适用于重载上货架之用,托盘表面根据需要制作成平板状、波纹状及间隔形式,满足不同的使用要求。

A single payment file can be uploaded from an ERP system to effect all pan-China RMB payments and overseas payments in all currencies.

付款指令文件可从您的 ERP 系统上传到我们的电子银行系统来只是国内及对海外各种币种付款。